DE102013018456B4 - Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung - Google Patents

Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung Download PDF

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Publication number
DE102013018456B4
DE102013018456B4 DE102013018456.8A DE102013018456A DE102013018456B4 DE 102013018456 B4 DE102013018456 B4 DE 102013018456B4 DE 102013018456 A DE102013018456 A DE 102013018456A DE 102013018456 B4 DE102013018456 B4 DE 102013018456B4
Authority
DE
Germany
Prior art keywords
acid
glycol
polyol ester
treatment
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE102013018456.8A
Other languages
German (de)
English (en)
Other versions
DE102013018456A1 (de
Inventor
Jens Kubitschke
Thorsten Kreickmann
Jörg Arnold
Heinz Strutz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxea GmbH
Original Assignee
OQ Chemicals GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DE102013018456.8A priority Critical patent/DE102013018456B4/de
Application filed by OQ Chemicals GmbH filed Critical OQ Chemicals GmbH
Priority to PCT/EP2014/002737 priority patent/WO2015062700A1/de
Priority to US14/915,915 priority patent/US9840454B2/en
Priority to EP14792386.6A priority patent/EP3063121B1/de
Priority to KR1020167011641A priority patent/KR102309656B1/ko
Priority to JP2016526303A priority patent/JP6470277B2/ja
Priority to CN201480050930.6A priority patent/CN105555750B/zh
Publication of DE102013018456A1 publication Critical patent/DE102013018456A1/de
Application granted granted Critical
Publication of DE102013018456B4 publication Critical patent/DE102013018456B4/de
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE102013018456.8A 2013-11-02 2013-11-02 Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung Expired - Fee Related DE102013018456B4 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE102013018456.8A DE102013018456B4 (de) 2013-11-02 2013-11-02 Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung
US14/915,915 US9840454B2 (en) 2013-11-02 2014-10-09 Method for obtaining polyol esters-enriched product streams from the side-streams in polyol ester production
EP14792386.6A EP3063121B1 (de) 2013-11-02 2014-10-09 Verfahren zur gewinnung von mit polyolestern angereicherten produktströmen aus den nebenströmen der polyolesterherstellung
KR1020167011641A KR102309656B1 (ko) 2013-11-02 2014-10-09 폴리올 에스테르 제조시 사이드-스트림으로부터 폴리올 에스테르-풍부 생성물 스트림을 수득하는 방법
PCT/EP2014/002737 WO2015062700A1 (de) 2013-11-02 2014-10-09 Verfahren zur gewinnung von mit polyolestern angereicherten produktströmen aus den nebenströmen der polyolesterherstellung
JP2016526303A JP6470277B2 (ja) 2013-11-02 2014-10-09 ポリオールエステル製造における副流から、ポリオールエステルが富化された生成物流を得るための方法
CN201480050930.6A CN105555750B (zh) 2013-11-02 2014-10-09 从多元醇酯制备中的侧流得到富含多元醇酯的产物流的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102013018456.8A DE102013018456B4 (de) 2013-11-02 2013-11-02 Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung

Publications (2)

Publication Number Publication Date
DE102013018456A1 DE102013018456A1 (de) 2015-05-07
DE102013018456B4 true DE102013018456B4 (de) 2019-01-24

Family

ID=51844660

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102013018456.8A Expired - Fee Related DE102013018456B4 (de) 2013-11-02 2013-11-02 Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung

Country Status (7)

Country Link
US (1) US9840454B2 (https=)
EP (1) EP3063121B1 (https=)
JP (1) JP6470277B2 (https=)
KR (1) KR102309656B1 (https=)
CN (1) CN105555750B (https=)
DE (1) DE102013018456B4 (https=)
WO (1) WO2015062700A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105330543B (zh) * 2015-10-19 2017-09-26 中国石油化工股份有限公司 一种多元醇酯的精制处理方法
KR102570952B1 (ko) * 2016-06-16 2023-08-28 주식회사 엘지생활건강 색상 물성이 우수한 다가 알코올 에스테르의 합성
DE102016008559A1 (de) * 2016-07-12 2018-01-18 Staedtler Mars Gmbh & Co. Kg Radierer
CN120623042B (zh) * 2025-08-14 2025-12-05 山东旺林新材料有限公司 一种三甘醇二异辛酸酯的制备方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2628249A (en) 1951-01-03 1953-02-10 Pittsburgh Coke & Chemical Co Esterification process
DE3737759A1 (de) 1987-11-06 1989-05-18 Henkel Kgaa Verfahren zur herstellung von estern der monochloressigsaeure mit c(pfeil abwaerts)1(pfeil abwaerts)-c(pfeil abwaerts)4(pfeil abwaerts)-alkanolen
US5324853A (en) 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
DE102009048772A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048775A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048771A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048773A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Farbaufhellung von Polyolestern
DE102009048774A1 (de) 2009-10-08 2011-04-28 Oxea Deutschland Gmbh Verfahren zur Farbaufhellung von Polyolestern

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011218321A (ja) * 2010-04-13 2011-11-04 Hitachi Plant Technologies Ltd 揮発性有機物の蒸留装置および蒸留方法
DE102010027458A1 (de) * 2010-07-17 2012-01-19 Oxea Gmbh Verfahren zur Nachbehandlung von Polyolestern

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2628249A (en) 1951-01-03 1953-02-10 Pittsburgh Coke & Chemical Co Esterification process
DE3737759A1 (de) 1987-11-06 1989-05-18 Henkel Kgaa Verfahren zur herstellung von estern der monochloressigsaeure mit c(pfeil abwaerts)1(pfeil abwaerts)-c(pfeil abwaerts)4(pfeil abwaerts)-alkanolen
US5324853A (en) 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
DE102009048772A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048775A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048771A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Herstellung von Polyolestern
DE102009048773A1 (de) 2009-10-08 2011-04-21 Oxea Deutschland Gmbh Verfahren zur Farbaufhellung von Polyolestern
DE102009048774A1 (de) 2009-10-08 2011-04-28 Oxea Deutschland Gmbh Verfahren zur Farbaufhellung von Polyolestern

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
DIN EN ISO 3682/ASTM D 1613

Also Published As

Publication number Publication date
KR102309656B1 (ko) 2021-10-12
CN105555750A (zh) 2016-05-04
DE102013018456A1 (de) 2015-05-07
EP3063121A1 (de) 2016-09-07
US9840454B2 (en) 2017-12-12
JP6470277B2 (ja) 2019-02-13
WO2015062700A1 (de) 2015-05-07
US20160229789A1 (en) 2016-08-11
EP3063121B1 (de) 2017-12-13
KR20160084381A (ko) 2016-07-13
CN105555750B (zh) 2017-07-14
JP2016535029A (ja) 2016-11-10

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R016 Response to examination communication
R079 Amendment of ipc main class

Free format text: PREVIOUS MAIN CLASS: C07C0067080000

Ipc: C07C0067540000

R018 Grant decision by examination section/examining division
R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee