CS226938B1 - N-(2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid - Google Patents
N-(2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid Download PDFInfo
- Publication number
- CS226938B1 CS226938B1 CS517982A CS517982A CS226938B1 CS 226938 B1 CS226938 B1 CS 226938B1 CS 517982 A CS517982 A CS 517982A CS 517982 A CS517982 A CS 517982A CS 226938 B1 CS226938 B1 CS 226938B1
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- tetramethylpentamethylene
- benzithiazol
- sulphenamide
- benzothiazole
- vulcanization
- Prior art date
Links
- GPNLWUFFWOYKLP-UHFFFAOYSA-N s-(1,3-benzothiazol-2-yl)thiohydroxylamine Chemical compound C1=CC=C2SC(SN)=NC2=C1 GPNLWUFFWOYKLP-UHFFFAOYSA-N 0.000 claims description 3
- RKMGAJGJIURJSJ-UHFFFAOYSA-N 2,2,6,6-tetramethylpiperidine Chemical compound CC1(C)CCCC(C)(C)N1 RKMGAJGJIURJSJ-UHFFFAOYSA-N 0.000 description 4
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 4
- 238000004073 vulcanization Methods 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- GQVPYCDCRPAHKB-UHFFFAOYSA-N 1,3-benzothiazol-2-yl thiohypochlorite Chemical compound C1=CC=C2SC(SCl)=NC2=C1 GQVPYCDCRPAHKB-UHFFFAOYSA-N 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 239000005060 rubber Substances 0.000 description 2
- 244000043261 Hevea brasiliensis Species 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 229920003052 natural elastomer Polymers 0.000 description 1
- 229920001194 natural rubber Polymers 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- QAZLUNIWYYOJPC-UHFFFAOYSA-M sulfenamide Chemical class [Cl-].COC1=C(C)C=[N+]2C3=NC4=CC=C(OC)C=C4N3SCC2=C1C QAZLUNIWYYOJPC-UHFFFAOYSA-M 0.000 description 1
Landscapes
- Hydrogenated Pyridines (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Description
(54) N- (2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid
Vynález sa týká nového derivátu sulfénamidu, ktorý je možné použiť pri vulkanizácii roznych typov kaučukov.
Sulfénamidy popři iných urýchlovačoch vulkanizácie sú účinné urýchlovače. Počas vulkanizácie okrem dobrej spracovatelskej bezpečnosti vykazujú aj dobrý urýchlovací efekt.
Tento vynález sa zaoberá zlúčeninou vzorca I
Zlúčeninu, ktorá je predmetom tohto vynálezu, je možné použiť ako urýchlovač pri vulkanizácii roznych typov kaučukov (napr. prírodný kaučuk, styrén-butadiénový kaučuk atd.).
Zlúčeninu vzorca I je možné pripraviť reakciou benztiazol-2-sulfenylchloridu s
2,2,6,6-tetrametylpiperidínom.
Příklad
N-(2,2,6,6-tetrametylpentametylén)benztiazol-2-sulfénamid
K roztoku 28 g (0,2 mol) 2,2,6,6-tetrametylpiperidínu v 200 ml chloride uhličitom sa přidá 20,2 g (0,1 mol) benztiazol-2-sulfenylchloridu. Po odpaření chloridu uhličitého sa získá 21 g (68,5 %) produktu s t. t. 133 až 135 °C (dietyléter).
Pre C16H22N2S2 (306,48) vypočítané:
9,14 % N zistené:
9,1 % N
IČ spektrum (cm-1):
vihráciu v (NH) (stéricky bráněný) nevidnoi XNMR spektrum (σ): || || + || -C-.(CH2)5-C- (6H) multi.,
1,18 CH3—C—CH3 (6H) singl., 1,35 ’ 6,88—7,85 aromatika (4H) multi.
II ·
1,35 CHs— C—CH5 (6H) singl.,
1,33—2,70
Claims (1)
- PREDMET VYNALEZUN-(2,2,6,6-tetrametylpentametylén]benztiazol-2-sulfénamid vzorce
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CS517982A CS226938B1 (cs) | 1982-07-07 | 1982-07-07 | N-(2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CS517982A CS226938B1 (cs) | 1982-07-07 | 1982-07-07 | N-(2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS226938B1 true CS226938B1 (cs) | 1984-04-16 |
Family
ID=5396181
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS517982A CS226938B1 (cs) | 1982-07-07 | 1982-07-07 | N-(2,2,6,8-tetrametylpentanmetylén) benztiazol-2-sulfénamid |
Country Status (1)
| Country | Link |
|---|---|
| CS (1) | CS226938B1 (cs) |
-
1982
- 1982-07-07 CS CS517982A patent/CS226938B1/cs unknown
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