CN218421112U

CN218421112U - Potassium fluotitanate refining and purifying equipment

Info

Publication number: CN218421112U
Application number: CN202222405383.3U
Authority: CN
Inventors: 周博理; 李素芬; 程天娥
Original assignee: Wuhan Xingliyuan Chemical Technology Co ltd
Current assignee: Wuhan Xingliyuan Chemical Technology Co ltd
Priority date: 2022-09-08
Filing date: 2022-09-08
Publication date: 2023-02-03
Anticipated expiration: 2032-09-08

Abstract

The utility model relates to a potassium fluotitanate purification technical field discloses a potassium fluotitanate refining and purifying device, which comprises an outer box, the inner side of the outer box is fixedly connected with a mixing box and a purifying tank, the mixing box is positioned above the purifying tank, the inner wall of one side of the mixing box is rotationally connected with a first rotating shaft, the outer wall of the first rotating shaft is fixedly connected with a first stirring rod distributed at equal distance, and the inner wall of one side of the purifying tank is rotationally connected with a second rotating shaft; the utility model discloses after the stirring is accomplished, demolish positioning screw from the outer container, after demolising, the outside pulling of baffle to the outer container is drawn with the effect of push-and-pull board, until the baffle is located the outside of outer container, liquid flows to the purification jar in through the effect of filter screen this moment, through the baffle that sets up, can play the effect that blocks to potassium fluotitanate crystal and hot water, make when mixing potassium fluotitanate crystal and hot water and stirring, the phenomenon of lou material can not appear, and is comparatively practical, and is suitable for extensive popularization and use.

Description

Potassium fluotitanate's refining purification equipment

Technical Field

The utility model belongs to the technical field of potassium fluotitanate purification, specifically speaking relates to a potassium fluotitanate's refining purification equipment.

Background

Potassium fluotitanate is a white flaky crystal, is soluble in hot water, slightly soluble in cold water and inorganic acid, and insoluble in ammonia water.

The CN210419286U discloses a potassium fluotitanate purification device, including the upper tank body of reation kettle and the lower tank body of reation kettle, the internal lateral wall of the upper tank body of reation kettle is from last to connecting with integrated into one piece's first annular fixed plate and second annular fixed plate respectively down, bolt fixed mounting has the filter bottom the first annular fixed plate, bolt fixed mounting has first baffle bottom the second annular fixed plate, first baffle bottom fixedly connected with protection casing. The utility model discloses, the solution after dissolving is filtered the back by the filter and is gone into jar internal portion under to reation kettle from the unloading pipe, and the silicon crystal of isolating then remains in the filter top, and electric heater heats the solution of second baffle top for solution boils rapidly, discharges from the blast pipe behind the evaporation of water in the solution, and the potassium fluotitanate recrystallization that remains after the evaporation stays on the second baffle, and rabbling mechanism stirs the potassium fluotitanate crystallization.

However, the inventor finds that the technical scheme still has at least the following defects: in the above device, when the stirring mechanism is started to mix and stir the potassium fluotitanate crystals and the hot water, the potassium fluotitanate crystals and the hot water leak downward from the filter plate, and the mixing effect of the potassium fluotitanate crystals and the hot water is poor.

In view of this, the present invention is provided.

Disclosure of Invention

In order to solve the technical problem, the utility model adopts the following basic concept:

the potassium fluotitanate refining and purifying equipment comprises an outer box, wherein a mixing box and a purifying tank are fixedly connected to the inner side of the outer box, the mixing box is positioned above the purifying tank, a first rotating shaft is rotatably connected to the inner wall of one side of the mixing box, a first stirring rod distributed at equal intervals is fixedly connected to the outer wall of the first rotating shaft, a second rotating shaft is rotatably connected to the inner wall of one side of the purifying tank, a second stirring rod distributed at equal intervals is fixedly connected to the outer wall of the second rotating shaft, a mounting opening is formed in the bottom of the mixing box, a filter screen is fixedly connected to the inner wall of the mounting opening, a partition plate is arranged on the inner side of the outer box, and the partition plate is contacted with the outer wall of the bottom of the mixing box;

outer container one side outer wall fixedly connected with protective housing, first axis of rotation and second axis of rotation run through respectively in the mixing box and the purification jar extends to the protective housing inboard, first axis of rotation and second axis of rotation are located the inboard one end outer wall of protective housing respectively fixedly connected with action wheel and follow the driving wheel, action wheel and follow driving wheel outer wall connection have same drive belt, protective housing one side inner wall fixedly connected with driving motor, the driving motor output shaft passes through the coupling joint in first axis of rotation.

As an optimal implementation mode of the utility model, the opening that the symmetry set up is seted up at the outer container top, and two opening inner walls fixedly connected with water injection pipe and feeder hopper respectively, water injection pipe and feeder hopper all extend to the mixing box inboard.

As a preferred embodiment of the utility model, the rectangle expansion joint has been seted up to outer container one side, and baffle one end is located the rectangle expansion joint inboard, the baffle is located the one end fixedly connected with push-and-pull plate in the outer container outside.

As an embodiment of the present invention, the push-pull plate is provided with a threaded hole, and the threaded hole inner wall is screwed with a positioning screw, the positioning hole is provided on one side of the outer container, and the positioning screw is screwed on the inner wall of the positioning hole.

As a preferred embodiment of the utility model, the equal fixedly connected with limit baffle of outer container both sides inner wall, two limit baffle contacts with purification tank deck portion both sides outer wall respectively, two the limit baffle top contacts with baffle bottom both sides outer wall respectively.

As an optimal implementation mode of the utility model, the mounting groove has all been seted up to purification jar both sides, and two equal fixedly connected with installation shell of mounting groove inner wall, two the inboard equal fixedly connected with heating pipe of installation shell.

As the utility model discloses a preferred embodiment, the through-hole has been seted up at purification tank bottoms middle part, and through-hole inner wall fixedly connected with unloading pipe, the unloading bottom run through in the outer container, the outer container bottom outside is provided with the case that gathers materials, it is located under the unloading pipe to gather materials the case.

Compared with the prior art, the utility model following beneficial effect has:

the utility model discloses, with potassium fluotitanate crystal and hot water leading-in to the mixing box through the effect of feeder hopper and water injection pipe respectively, start driving motor drives first axis of rotation and rotates, first axis of rotation drives first stirring rod and stirs potassium fluotitanate crystal and hot water, make potassium fluotitanate crystal dissolve in the hot water, after the stirring is accomplished, demolish positioning screw from the outer container, after demolising, the effect through the push-and-pull board stimulates the baffle to the outside of outer container with the baffle, the outside that is located the outer container up to the baffle, liquid flows to the purification jar through the effect of filter screen this moment, through the baffle that sets up, can play the effect that blocks to potassium fluotitanate crystal and hot water, make when carrying out the mixing stirring to potassium fluotitanate crystal and hot water, the phenomenon of leaking can not appear.

The utility model discloses, after liquid flows to the purification jar in, the starting heating pipe heats liquid for reach the effect of being heated the crystallization, first axis of rotation drives the second axis of rotation through the action wheel, from the driving wheel and the effect of drive belt simultaneously and rotates, and the second axis of rotation drives second stirring rod and stirs liquid, makes to be heated more evenly, and the potassium fluotitanate crystal purity that obtains is higher.

The following describes embodiments of the present invention in further detail with reference to the accompanying drawings.

Drawings

In the drawings:

FIG. 1 is a schematic view of a front sectional structure of the outer box of the present invention;

FIG. 2 is a schematic sectional view of the mixing box of the present invention;

FIG. 3 is a schematic sectional view of the purification tank of the present invention;

fig. 4 is an enlarged schematic structural diagram of a in fig. 1 according to the present invention.

In the figure: 1. an outer box; 2. a mixing box; 3. a purification tank; 4. a water injection pipe; 5. a feed hopper; 6. a protective housing; 7. a first rotating shaft; 8. a second rotating shaft; 9. a driving wheel; 10. a driven wheel; 11. a transmission belt; 12. a drive motor; 13. a partition plate; 14. a feeding pipe; 15. a material collecting box; 16. a first stirring rod; 17. filtering with a screen; 18. a second stirring rod; 19. heating a tube; 20. a limiting baffle; 21. a push-pull plate; 22. and (5) positioning the screw rod.

Detailed Description

In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and the following embodiments are used to illustrate the present invention.

As shown in fig. 1 to 4

A potassium fluotitanate refining and purifying device comprises an outer box 1, wherein a mixing box 2 and a purifying tank 3 are fixedly connected to the inner side of the outer box 1, the mixing box 2 is positioned above the purifying tank 3, a first rotating shaft 7 is rotatably connected to the inner wall of one side of the mixing box 2, a first stirring rod 16 which is distributed at equal intervals is fixedly connected to the outer wall of the first rotating shaft 7, a second rotating shaft 8 is rotatably connected to the inner wall of one side of the purifying tank 3, a second stirring rod 18 which is distributed at equal intervals is fixedly connected to the outer wall of the second rotating shaft 8, a mounting opening is formed in the bottom of the mixing box 2, a filter screen 17 is fixedly connected to the inner wall of the mounting opening, a partition plate 13 is arranged on the inner side of the outer box 1, and the partition plate 13 is contacted with the outer wall of the bottom of the mixing box 2;

outer wall fixedly connected with protective housing 6 in one side of outer container 1, first axis of rotation 7 and second axis of rotation 8 run through respectively in mixing box 2 and purification jar 3 extend to protective housing 6 inboardly, first axis of rotation 7 and second axis of rotation 8 are located 6 inboard one end outer walls of protective housing and are fixedly connected with action wheel 9 respectively and follow driving wheel 10, action wheel 9 and have same drive belt 11 from driving wheel 10 outer wall connection, inner wall fixedly connected with driving motor 12 in protective housing 6 one side, driving motor 12 output shaft passes through the coupling joint on first axis of rotation 7.

In the concrete embodiment, the opening that the symmetry set up is seted up at 1 top of outer container, and two opening inner walls be fixedly connected with water injection pipe 4 and feeder hopper 5 respectively, water injection pipe 4 and feeder hopper 5 all extend to 2 inboards of mixing box, the rectangle expansion joint has been seted up to 1 one side of outer container, and 13 one end of baffle is located the rectangle expansion joint inboards, baffle 13 is located the one end fixedly connected with push-and-pull plate 21 in the 1 outside of outer container, set up threaded hole on the push-and-pull plate 21, and threaded hole inner wall spiro union has positioning screw 22, the locating hole has been seted up to 1 one side of outer container, and positioning screw 22 spiro union is on the locating hole inner wall.

Further, 1 equal fixedly connected with limit baffle 20 of both sides inner wall of outer container, two limit baffle 20 contact with 3 top both sides outer walls of purification jar respectively, two limit baffle 20 tops contact with 13 bottom both sides outer walls of baffle respectively, the mounting groove has all been seted up to 3 both sides of purification jar, and the equal fixedly connected with installation shell of two mounting groove inner walls, two inboard equal fixedly connected with heating pipes 19 of installation shell, the through-hole has been seted up at purification jar 3 bottom middle part, and through-hole inner wall fixedly connected with unloading

pipe

14, 14 bottom run through in outer container 1 of unloading pipe, 1 bottom outside of outer container is provided with the case 15 that gathers materials, the case 15 that gathers materials is located unloading pipe 14 under.

The implementation principle of the potassium fluotitanate refining and purifying equipment of the embodiment is as follows: firstly, potassium fluotitanate crystals and hot water are respectively led into a mixing box 2 under the action of a feed hopper 5 and a water injection pipe 4, a driving motor 12 is started to drive a first rotating shaft 7 to rotate, the first rotating shaft 7 drives a first stirring rod 16 to stir the potassium fluotitanate crystals and the hot water, the potassium fluotitanate crystals are dissolved in the hot water, after the stirring is completed, a positioning screw 22 is detached from an outer box 1, after the detachment, a partition plate 13 is pulled to the outer side of the outer box 1 under the action of a push-pull plate 21 until the partition plate 13 is positioned at the outer side of the outer box 1, at the moment, the liquid flows into a purification tank 3 under the action of a filter screen 17, the impurities in the liquid can be filtered under the action of the filter screen 17, after the liquid flows into the purification tank 3, a heating pipe 19 is started to heat the liquid, the heated crystal effect is achieved, meanwhile, the first rotating shaft 7 drives a second rotating shaft 8 to rotate under the action of a driving wheel 9, a driven wheel 10 and a driven wheel 11, the second rotating rod 8 drives a second rotating rod 18 to stir the liquid, the heating belt is more uniform, the obtained, the potassium fluotitanate crystals flow into a potassium fluotitanate collecting pipe 14, and the potassium fluotitanate collecting pipe 14.

Claims

1. The potassium fluotitanate refining and purifying equipment is characterized by comprising an outer box (1), wherein the inner side of the outer box (1) is fixedly connected with a mixing box (2) and a purifying tank (3), the mixing box (2) is positioned above the purifying tank (3), the inner wall of one side of the mixing box (2) is rotatably connected with a first rotating shaft (7), the outer wall of the first rotating shaft (7) is fixedly connected with a first stirring rod (16) which is distributed at equal intervals, the inner wall of one side of the purifying tank (3) is rotatably connected with a second rotating shaft (8), the outer wall of the second rotating shaft (8) is fixedly connected with a second stirring rod (18) which is distributed at equal intervals, the bottom of the mixing box (2) is provided with a mounting opening, the inner wall of the mounting opening is fixedly connected with a filter screen (17), the inner side of the outer box (1) is provided with a partition plate (13), and the partition plate (13) is contacted with the outer wall of the bottom of the mixing box (2);

outer container (1) one side outer wall fixedly connected with protecting sheathing (6), first axis of rotation (7) and second axis of rotation (8) run through respectively in mixing box (2) and purification jar (3) extend to protecting sheathing (6) inboard, first axis of rotation (7) and second axis of rotation (8) are located protecting sheathing (6) inboard one end outer wall respectively fixedly connected with action wheel (9) and follow driving wheel (10), action wheel (9) and follow driving wheel (10) outer wall connection have same drive belt (11), protecting sheathing (6) one side inner wall fixedly connected with driving motor (12), driving motor (12) output shaft passes through the coupling joint on first axis of rotation (7).

2. The potassium fluotitanate refining and purifying equipment according to claim 1, wherein the top of the outer box (1) is provided with symmetrically arranged openings, the inner walls of the two openings are fixedly connected with a water injection pipe (4) and a feed hopper (5) respectively, and the water injection pipe (4) and the feed hopper (5) both extend to the inner side of the mixing box (2).

3. The potassium fluotitanate refining and purifying equipment according to claim 1, wherein one side of the outer box (1) is provided with a rectangular movable opening, one end of the partition plate (13) is positioned at the inner side of the rectangular movable opening, and one end of the partition plate (13) positioned at the outer side of the outer box (1) is fixedly connected with a push-pull plate (21).

4. The potassium fluotitanate refining and purifying equipment according to claim 3, wherein the push-pull plate (21) is provided with a threaded hole, the inner wall of the threaded hole is in threaded connection with a positioning screw (22), one side of the outer box (1) is provided with a positioning hole, and the positioning screw (22) is in threaded connection with the inner wall of the positioning hole.

5. The potassium fluotitanate refining and purifying equipment according to claim 1, wherein the inner walls of both sides of the outer box (1) are fixedly connected with limit baffles (20), two limit baffles (20) are respectively contacted with the outer walls of both sides of the top of the purifying tank (3), and the tops of two limit baffles (20) are respectively contacted with the outer walls of both sides of the bottom of the partition plate (13).

6. The potassium fluotitanate refining and purifying equipment according to claim 1, wherein both sides of the purifying tank (3) are provided with mounting grooves, the inner walls of the two mounting grooves are fixedly connected with mounting shells, and the inner sides of the two mounting shells are fixedly connected with heating pipes (19).

7. The potassium fluotitanate refining and purifying equipment according to claim 1, wherein a through hole is formed in the middle of the bottom of the purifying tank (3), a blanking pipe (14) is fixedly connected to the inner wall of the through hole, the bottom end of the blanking pipe (14) penetrates through the outer box (1), a material collecting box (15) is arranged on the outer side of the bottom of the outer box (1), and the material collecting box (15) is located under the blanking pipe (14).