CN214288167U - Reation kettle with crystallization filtering capability - Google Patents
Reation kettle with crystallization filtering capability Download PDFInfo
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- CN214288167U CN214288167U CN202022934935.0U CN202022934935U CN214288167U CN 214288167 U CN214288167 U CN 214288167U CN 202022934935 U CN202022934935 U CN 202022934935U CN 214288167 U CN214288167 U CN 214288167U
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- chamber
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- lower filter
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- 238000001914 filtration Methods 0.000 title claims abstract description 70
- 238000002425 crystallisation Methods 0.000 title claims abstract description 46
- 230000008025 crystallization Effects 0.000 title claims abstract description 46
- 238000006243 chemical reaction Methods 0.000 claims abstract description 69
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 239000007787 solid Substances 0.000 claims abstract description 25
- 239000000463 material Substances 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 16
- 238000007789 sealing Methods 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 238000007599 discharging Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
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Abstract
本实用新型公开了一种带有结晶过滤功能的反应釜，包括反应釜本体和控制装置，反应釜本体包括从上至下依次设置的反应室、上过滤室、结晶室、下过滤室，反应室内设置有搅拌轴，搅拌轴转动穿过反应室顶端中部连接有电机，上过滤室内设置有上过滤板，下过滤室内设置有下过滤板，反应室顶端上设置有加料口，反应室底壁中部设置有第一出料口，上过滤室底壁中部设置有第二出液口，上过滤室的一侧设置有第一出固口，结晶室底壁中部设置有第三出液口，下过滤室底壁中部设置有第四出液口，下过滤室的一侧设置有第二出固口。本实用新型将反应‑过滤‑结晶‑过滤一体化，使产物能够完全分离，减少产物损失，同时大大降低人力物力的消耗，提高生产效率。
The utility model discloses a reaction kettle with a function of crystallization and filtration, comprising a reaction kettle body and a control device. The reaction kettle body comprises a reaction chamber, an upper filter chamber, a crystallization chamber and a lower filter chamber which are arranged in sequence from top to bottom. A stirring shaft is arranged in the chamber, and the stirring shaft rotates through the middle of the top of the reaction chamber and is connected to a motor, an upper filter plate is arranged in the upper filter chamber, a lower filter plate is arranged in the lower filter chamber, a feeding port is arranged on the top of the reaction chamber, and the bottom wall of the reaction chamber is arranged. A first material outlet is arranged in the middle, a second liquid outlet is arranged in the middle of the bottom wall of the upper filter chamber, a first solid outlet is arranged on one side of the upper filter chamber, and a third liquid outlet is arranged in the middle of the bottom wall of the crystallization chamber, A fourth liquid outlet is arranged in the middle of the bottom wall of the lower filter chamber, and a second solid outlet is arranged on one side of the lower filter chamber. The utility model integrates reaction, filtration, crystallization and filtration, so that the product can be completely separated, the loss of the product is reduced, the consumption of manpower and material resources is greatly reduced, and the production efficiency is improved.
Description
Technical Field
The utility model relates to a reation kettle with crystallization filtering capability belongs to reation kettle technical field.
Background
The reaction kettle is a container for carrying out chemical reaction, and in order to adapt to different requirements of various working conditions, the types of the reaction kettle are more and more, so that the reaction kettle is widely applied to the fields of biology, chemical engineering, materials science and semi-conductor science. The existing reaction kettle generates various products after the raw materials are reacted, the products need to be transferred to other equipment for separation, such as processes of filtration, crystallization and the like, the product transfer process causes loss and pollution, and meanwhile, the consumption of manpower and material resources is needed.
SUMMERY OF THE UTILITY MODEL
In view of the problems existing in the prior art, the utility model provides a reaction kettle with crystallization filtering function, which integrates reaction, filtration, crystallization and filtration, so that the product can be completely separated, the product loss and the product pollution are reduced, meanwhile, the consumption of manpower and material resources is greatly reduced, and the production efficiency is improved.
In order to achieve the above purpose, the utility model adopts the following technical scheme: a reaction kettle with a crystallization filtering function comprises a reaction kettle body and a control device, wherein the control device is installed on one side of the reaction kettle body, the reaction kettle body comprises a reaction chamber, an upper filtering chamber, a crystallization chamber and a lower filtering chamber which are sequentially arranged from top to bottom, a stirring shaft is arranged in the reaction chamber, the stirring shaft is rotatably connected with a motor which is electrically connected with the control device through the middle part of the top end of the reaction chamber, an upper filtering plate is arranged in the upper filtering chamber, a lower filtering plate is arranged in the lower filtering chamber, a feeding hole is arranged on the top end of the reaction chamber, a first discharging hole which is arranged in the upper filtering chamber is arranged in the middle part of the bottom wall of the reaction chamber, a second liquid outlet which is arranged in the crystallization chamber is arranged in the middle part of the bottom wall of the upper filtering chamber, a first solid outlet which is arranged above the upper filtering plate is arranged on one side of the upper filtering chamber, a third liquid outlet which is arranged in the lower filtering chamber is arranged in the middle part of the bottom wall of the crystallization chamber, and a fourth liquid outlet is formed in the middle of the bottom wall of the lower filtering chamber, and a second solid outlet positioned above the lower filtering plate is formed in one side of the lower filtering chamber.
Preferably, the outer wall of the reaction chamber and the outer wall of the upper filtering chamber are respectively provided with a first heating device and a second heating device which are electrically connected with the control device, and the outer wall of the crystallization chamber and the outer wall of the lower filtering chamber are respectively provided with a first cooling device and a second cooling device which are electrically connected with the control device.
Preferably, the inner wall of the reaction chamber, the inner wall of the upper filtering chamber, the inner wall of the crystallization chamber and the inner wall of the lower filtering chamber are respectively provided with a first temperature sensor, a second temperature sensor, a third temperature sensor and a fourth temperature sensor which are electrically connected with the control device.
Preferably, the first discharge port, the second liquid outlet, the third liquid outlet and the fourth liquid outlet are respectively provided with a first electromagnetic valve, a second electromagnetic valve, a third electromagnetic valve and a fourth electromagnetic valve which are electrically connected with the control device.
Preferably, a first sealing cover, a second sealing cover and a third sealing cover are respectively arranged on the feeding port, the first solid outlet and the second solid outlet.
Preferably, go up the filter slope and arrange in last filter chamber, the angle of inclination of going up filter and horizontal plane is 1 ~ 10 degrees, first solid mouthful is located the top of last filter least significant end.
Preferably, the lower filter plate is obliquely arranged in the lower filter chamber, the inclination angle between the lower filter plate and the horizontal plane is 1-10 degrees, and the second solid outlet is positioned above the lowest end of the lower filter plate.
Preferably, the bottom wall of the reaction chamber, the bottom wall of the upper filtering chamber, the bottom wall of the crystallization chamber and the bottom wall of the lower filtering chamber are all arranged into a bucket-shaped structure.
The utility model has the advantages that: the reaction kettle body of the utility model integrates the reaction, filtration, crystallization and filtration from the top to the bottom of the reaction chamber, the upper filtration chamber, the crystallization chamber and the lower filtration chamber which are arranged in sequence, so that the products can be completely separated, the product loss and the product pollution are reduced, meanwhile, the consumption of manpower and material resources is greatly reduced, and the production efficiency is improved; the utility model discloses a this internal material of reation kettle can get into next process from a process completely, reduces the result loss, gets material convenience, swift simultaneously.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
In the figure: 1. the reaction kettle comprises a reaction kettle body, 2, a control device, 3, a reaction chamber, 4, an upper filtering chamber, 5, a crystallization chamber, 6, a lower filtering chamber, 7, a stirring shaft, 8, an upper filtering plate, 9, a lower filtering plate, 10, a first sealing cover, 11, a first electromagnetic valve, 12, a second electromagnetic valve, 13, a second sealing cover, 14, a third electromagnetic valve, 15, a fourth electromagnetic valve, 16, a third sealing cover, 17, a first heating device, 18, a second heating device, 19, a first cooling device, 20, a second cooling device, 21, a first temperature sensor, 22, a second temperature sensor, 23, a third temperature sensor, 24 and a fourth temperature sensor.
Detailed Description
The technical solutions in the implementation of the present invention will be clear from the following description and accompanying drawings, and the described embodiments are only some embodiments, not all embodiments, of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.
As shown in fig. 1, a reaction kettle with crystallization filtering function provided by the embodiment of the present invention comprises a reaction kettle body 1 and a control device 22, wherein the control device 2 is installed at one side of the reaction kettle body 1, the reaction kettle body 1 comprises a reaction chamber 3, an upper filtering chamber 4, a crystallization chamber 5 and a lower filtering chamber 6 which are sequentially arranged from top to bottom, a stirring shaft 7 is arranged in the reaction chamber 3, the stirring shaft 7 is connected with a motor electrically connected with the control device 2 by rotating to penetrate through the middle part of the top end of the reaction chamber 3, an upper filtering plate 8 is arranged in the upper filtering chamber 4, a lower filtering plate 9 is arranged in the lower filtering chamber 6, a charging opening is arranged at the top end of the reaction chamber 3, a first discharging opening arranged in the upper filtering chamber 4 is arranged at the middle part of the bottom wall of the reaction chamber 3, a second liquid outlet arranged in the crystallization chamber 5 is arranged at the middle part of the bottom wall of the upper filtering chamber 4, go up one side of filter chamber 4 and be provided with the first solid mouth that goes out that is located 8 tops of last filter, 5 diapire middle parts of crystallization chamber are provided with the third liquid outlet that is located lower filter chamber 6, 6 diapire middle parts of lower filter chamber are provided with the fourth liquid outlet, one side of lower filter chamber 6 is provided with the second solid mouth that goes out that is located lower filter 9 tops.
The outer wall of the reaction chamber 3 and the outer wall of the upper filtering chamber 4 are respectively provided with a first heating device 17 and a second heating device 18 which are electrically connected with the control device 2, and the outer wall of the crystallization chamber 5 and the outer wall of the lower filtering chamber 6 are respectively provided with a first cooling device 19 and a second cooling device 20 which are electrically connected with the control device 2.
The inner wall of the reaction chamber 3, the inner wall of the upper filtering chamber 4, the inner wall of the crystallization chamber 5 and the inner wall of the lower filtering chamber 6 are respectively provided with a first temperature sensor 21, a second temperature sensor 22, a third temperature sensor 23 and a fourth temperature sensor 24 which are electrically connected with the control device 2.
The first discharge port, the second liquid outlet, the third liquid outlet and the fourth liquid outlet are respectively provided with a first electromagnetic valve 11, a second electromagnetic valve 12, a third electromagnetic valve 14 and a fourth electromagnetic valve 15 which are electrically connected with the control device 2.
And a first sealing cover 10, a second sealing cover 13 and a third sealing cover 16 are respectively arranged on the feeding port, the first solid outlet and the second solid outlet.
Go up filter 8 slope and arrange in last filter chamber 4, the angle of inclination of going up filter 8 and horizontal plane is 1 ~ 10 degrees, first solid mouth is located the top of 8 lowest ends of last filter, conveniently takes out the solid.
Lower filter 9 slope is arranged in lower filter chamber 6, the angle of inclination of lower filter 9 and horizontal plane is 1 ~ 10 degrees, the second goes out solid mouthful and is located the top of lower filter 9 least significant end, conveniently takes out the solid.
The bottom wall of the reaction chamber 3, the bottom wall of the upper filtering chamber 4, the bottom wall of the crystallization chamber 5 and the bottom wall of the lower filtering chamber 6 are all of bucket-shaped structures, so that materials can completely enter the next process from one process.
When in use: opening a first sealing cover 10, adding reaction raw materials, starting a motor to drive a stirring shaft 7 to stir, heating a reaction chamber 3 by a first heating device 17, transmitting the temperature of the reaction chamber 3 to a control device 2 by a first temperature sensor 21, controlling the first heating device 17 to be heated to the temperature required by the reaction by the control device 2, standing the mixture in the reaction chamber 3 after the reaction is finished, heating an upper filtering chamber 4 by a second heating device 18, transmitting the temperature of the upper filtering chamber 4 to the control device 2 by a second temperature sensor 22, controlling the second heating device 18 to be heated to the temperature required by the filtering by the control device 2, then opening the first electromagnetic valve 11 by the control device 2, enabling the mixture to enter the upper filtering chamber 4, opening the second electromagnetic valve 12 by the control device 2, enabling the solid of the mixture to stay on the upper filtering plate 8, and enabling the mixed liquid of the mixture to enter a crystallization chamber 5, closing the first heating device 17 and the second heating device 18, cooling the crystallization tank by the first cooling device 19, receiving the temperature of the reaction chamber 3 by the third temperature sensor 23 and transmitting the temperature to the control device 2, controlling the first cooling device 19 to be cooled to the temperature required by crystallization by the control device 2, crystallizing the liquid, standing the liquid after the crystallization is completed, cooling the lower filter chamber 6 by the second cooling device 20, receiving the temperature of the lower filter chamber 6 by the fourth temperature sensor 24 and transmitting the temperature to the control device 2, controlling the second cooling device 20 to be cooled to the temperature required by filtration by the control device 2, then opening the third electromagnetic valve 14 by the control device 2, allowing the crystallized mixture to enter the lower filter chamber 6, opening the fourth electromagnetic valve 15 by the control device 2, allowing the crystal to stay on the upper filter plate 8, allowing the liquid to flow out to the recovery tank, respectively opening the second sealing cover 13 and the third sealing cover 16 to take out the filtered solid, And (3) crystallizing, and then closing the first cooling device 19 and the second cooling device 20, so that the reaction, filtration, crystallization and filtration are integrated, the product can be completely separated, the product loss is reduced, the consumption of manpower and material resources is greatly reduced, and the production efficiency is improved.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should make the description as a whole, and the embodiments may be appropriately combined to form other embodiments understood by those skilled in the art.
Claims (8)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022934935.0U CN214288167U (en) | 2020-12-09 | 2020-12-09 | Reation kettle with crystallization filtering capability |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022934935.0U CN214288167U (en) | 2020-12-09 | 2020-12-09 | Reation kettle with crystallization filtering capability |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214288167U true CN214288167U (en) | 2021-09-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022934935.0U Expired - Fee Related CN214288167U (en) | 2020-12-09 | 2020-12-09 | Reation kettle with crystallization filtering capability |
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| Country | Link |
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| CN (1) | CN214288167U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113856591A (en) * | 2021-10-12 | 2021-12-31 | 浙江帕瓦新能源股份有限公司 | High-efficient concentration reaction kettle |
| CN114515442A (en) * | 2021-11-05 | 2022-05-20 | 广州市鸿浩光电半导体有限公司 | Crystallization system and crystallization method for generating sodium fluoroaluminate crystals from fluorine-containing wastewater |
| CN114853044A (en) * | 2022-05-12 | 2022-08-05 | 广西南宁百会药业集团有限公司 | Production system of hydrotalcite |
| CN115814633A (en) * | 2022-11-19 | 2023-03-21 | 浙江国盛源实业有限公司 | Production process of sodium sarcosinate and special production equipment thereof |
| CN115845783A (en) * | 2022-11-30 | 2023-03-28 | 四川安宁铁钛股份有限公司 | Continuous synthesizer of ferric phosphate |
-
2020
- 2020-12-09 CN CN202022934935.0U patent/CN214288167U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113856591A (en) * | 2021-10-12 | 2021-12-31 | 浙江帕瓦新能源股份有限公司 | High-efficient concentration reaction kettle |
| CN114515442A (en) * | 2021-11-05 | 2022-05-20 | 广州市鸿浩光电半导体有限公司 | Crystallization system and crystallization method for generating sodium fluoroaluminate crystals from fluorine-containing wastewater |
| CN114515442B (en) * | 2021-11-05 | 2023-06-20 | 广州市鸿浩光电半导体有限公司 | Crystallization system and crystallization method for generating sodium fluoroaluminate crystals from fluorine-containing wastewater |
| CN114853044A (en) * | 2022-05-12 | 2022-08-05 | 广西南宁百会药业集团有限公司 | Production system of hydrotalcite |
| CN115814633A (en) * | 2022-11-19 | 2023-03-21 | 浙江国盛源实业有限公司 | Production process of sodium sarcosinate and special production equipment thereof |
| CN115814633B (en) * | 2022-11-19 | 2023-11-03 | 浙江国盛源实业有限公司 | Production process of sodium sarcosinate and special production equipment thereof |
| CN115845783A (en) * | 2022-11-30 | 2023-03-28 | 四川安宁铁钛股份有限公司 | Continuous synthesizer of ferric phosphate |
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Granted publication date: 20210928 |