CN218529850U - Heating crystallization device for cobalt hydroxide production - Google Patents
Heating crystallization device for cobalt hydroxide production Download PDFInfo
- Publication number
- CN218529850U CN218529850U CN202222327130.9U CN202222327130U CN218529850U CN 218529850 U CN218529850 U CN 218529850U CN 202222327130 U CN202222327130 U CN 202222327130U CN 218529850 U CN218529850 U CN 218529850U
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- China
- Prior art keywords
- heating
- cauldron body
- locating
- cauldron
- mixing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000010438 heat treatment Methods 0.000 title claims abstract description 63
- 229910021503 Cobalt(II) hydroxide Inorganic materials 0.000 title claims abstract description 36
- ASKVAEGIVYSGNY-UHFFFAOYSA-L cobalt(ii) hydroxide Chemical compound [OH-].[OH-].[Co+2] ASKVAEGIVYSGNY-UHFFFAOYSA-L 0.000 title claims abstract description 36
- 238000002425 crystallisation Methods 0.000 title claims abstract description 24
- 230000008025 crystallization Effects 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 25
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 238000010992 reflux Methods 0.000 claims abstract description 5
- 241000883990 Flabellum Species 0.000 claims description 16
- 239000004744 fabric Substances 0.000 claims description 12
- 238000007599 discharging Methods 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 abstract description 11
- 230000008901 benefit Effects 0.000 abstract description 3
- SAXCKUIOAKKRAS-UHFFFAOYSA-N cobalt;hydrate Chemical compound O.[Co] SAXCKUIOAKKRAS-UHFFFAOYSA-N 0.000 abstract description 3
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 238000001035 drying Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000008187 granular material Substances 0.000 description 2
- 241000220317 Rosa Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001869 cobalt compounds Chemical class 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 239000002274 desiccant Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
The utility model discloses a cobaltous hydroxide production is with heating crystallization device, including the cauldron body with locate cauldron internal wall the hot plate, locate feeding part of cauldron body top one side, locate the motor of cauldron body top outer wall, locate the ejection of compact part of cauldron body bottom, locate the internal heated warehouses of cauldron, locate the (mixing) shaft at heated warehouses center, locate the epaxial stirring part of stirring and locate the air reflux part of cauldron internal wall one side, the hot plate is located between heated warehouses and the internal wall of cauldron, cauldron body bottom slope sets up, and ejection of compact part rises is kept away from to cauldron body bottom height orientation, motor and (mixing) shaft fixed connection. The utility model discloses possess the heating even, convenient operation's advantage has solved the unable problem of heating crystallization of current equipment preparation cobalt hydrate finished product.
Description
Technical Field
The utility model belongs to the technical field of the cobaltous hydroxide heating crystallization, especially, relate to a cobaltous hydroxide production is with heating crystallization device.
Background
Cobalt hydroxide is an inorganic compound having a chemical formula of Co (OH) 2, monoclinic or hexagonal crystal system, and is light cyan or rose colored powder. It is insoluble in water, slightly amphoteric, insoluble in strong alkali, but soluble in acid and ammonium salt solution. The density was about 3.6g/cm3. Melting point 1100-1200 deg.C, and is amphoteric hydroxide. It is mainly used as colouring agent for glass and enamel, raw material for preparing other cobalt compounds, and drying agent for varnish and paint. The cobalt hydroxide slurry is difficult to filter, is generally easy to agglomerate in the drying process, is easy to agglomerate and is difficult to dry, so that the cobalt hydroxide needs to be further purified to meet the requirement of industrial production.
For example, application number 202120248783.0 the present invention relates to the preparation of cobalt hydroxide, and in particular to
The cobalt hydroxide preparation system comprises a cobalt hydroxide preparation device, wherein the cobalt hydroxide preparation device comprises a filtering and concentrating reaction container, the filtering and concentrating reaction container comprises a reaction container for containing a cobalt hydroxide preparation raw material, a filter is arranged in the reaction container, and a solution generated by preparing the cobalt hydroxide can be in the reaction container
Filtering; and a stirrer for stirring the cobalt hydroxide preparation raw material is arranged in the reaction container. Compared with the traditional method of firstly reacting in a reaction kettle, the cobalt hydroxide preparation system has the advantages that the structure is more compact and the occupied area is smaller when the cobalt hydroxide is input to a filter or a centrifugal machine for solid-liquid separation, so that the cobalt hydroxide preparation efficiency is higher.
Based on the search of above-mentioned patent to and combine prior art equipment discovery, though cobalt hydroxide can be prepared to above-mentioned equipment during the application, cobalt hydroxide thick liquids are difficult to filter, generally easily reunite in drying process, easy caking, difficult stoving, and the demand of cobalt hydroxide heating crystallization can't be solved to this equipment.
SUMMERY OF THE UTILITY MODEL
Problem to prior art exists, the utility model provides a cobaltous hydroxide production is with heating crystallization device possesses the heating evenly, and convenient operation's advantage has solved the unable problem of heating crystallization of existing equipment preparation out cobaltous hydroxide finished product.
The utility model discloses a realize like this, a cobaltous hydroxide production is with heating crystallization device, including the cauldron body and the heating device who is used for heating crystallization cobaltous hydroxide, heating device is including the hot plate of locating cauldron internal wall, locate feeding part of cauldron body top one side, locate the motor of cauldron body top outer wall, locate the ejection of compact part of cauldron body bottom, locate the internal heated warehouses of cauldron, locate the (mixing) shaft at heated warehouses center, locate the epaxial stirring part of stirring and locate the air reflux part of cauldron internal wall one side, the hot plate is located between heated warehouses and the internal wall of cauldron, the slope of cauldron body bottom sets up, and the (mixing) shaft is gone up highly towards keeping away from to cauldron body bottom, motor and (mixing) shaft fixed connection, the heated warehouses is located between hot plate and the (mixing) shaft, the hot plate top (mixing) shaft is no longer than topmost.
As the utility model discloses it is preferred, stirring part includes three flabellum, flabellum and (mixing) shaft connection, angle 120 degrees between adjacent flabellum, the flabellum top is not higher than the hot plate peak, the flabellum bottom is not less than the hot plate minimum.
As the utility model discloses preferred, the air current return part is including the fan of locating cauldron internal wall upside, locate the vent of cauldron external wall downside and the air-circulating pipe of connecting fan and vent, vent and heated warehouses intercommunication, the fan just is located directly over the vent with heated warehouses intercommunication, the fan is not less than the hot plate peak.
As the utility model discloses preferred, ejection of compact part is including locating the screen cloth at heated warehouses bottom center, locating the ejection of compact valve below the screen cloth and locating the discharge gate of ejection of compact valve below, the screen cloth is parallel to each other with ejection of compact valve.
As the utility model discloses preferred, the feed component is including locating the feedstock channel of cauldron body top upside and locating the feed inlet of feedstock channel top, feedstock channel and heated warehouses intercommunication.
As the utility model discloses it is preferred, cauldron body below is equipped with the mount, the mount lower extreme is higher than the discharge gate lower extreme.
As the utility model discloses preferred, discharge valve is including locating the striker plate of locating the screen cloth below and locating the rotation axis of striker plate one side, the striker plate is parallel to each other with the screen cloth.
Compared with the prior art, the beneficial effects of the utility model are as follows:
1. the utility model discloses a set up hot plate, feeding part, motor, ejection of compact part, stirring part and heated warehouses, in the heating process, the feeding gets into heated warehouses through feeding part, through the hot plate heating feeding, through stirring part stirring feeding messenger its be heated evenly, the feeding that the final heating crystallization was accomplished passes through ejection of compact part heating, has solved the cobalt hydroxide thick liquids and has generally easily reunited in drying process, easy caking, the problem of difficult stoving.
2. The utility model discloses a set up motor, (mixing) shaft and flabellum, flabellum and hot plate mutually perpendicular, through the power of motor, make the (mixing) shaft rotate, it is rotatory around the (mixing) shaft to drive the flabellum, makes the feeding that gets into the heated warehouses be heated evenly, reduces the caking.
3. The utility model discloses a set up fan, air circulating pipe and vent, the fan passes through the air circulating pipe with the vent and is connected, and the fan rotates the air that makes the heated warehouses top and arranges the heated warehouses below by the vent through the air circulating pipe, makes the inside air thermal cycle of heated warehouses for the dry crystallization process of feeding.
4. The utility model discloses a set up screen cloth, discharge valve and discharge gate, the screen cloth is located discharge valve top, and the feeding that the heating was accomplished passes through the screen cloth and filters the entering discharge gate, through the discharge valve discharge cauldron body, can make the feeding discharge that the heating was accomplished controllable, can make the unable discharge of the complete bold granule of unheated.
5. The utility model discloses a set up feed inlet and feedstock channel, the feed inlet is located the feedstock channel top, and the feeding passes through feedstock channel by the feed inlet and gets into the heated warehouses, can make the feeding steadily get into the cauldron body.
6. The utility model discloses a set up the mount, mount and cauldron body fixed connection can make the cauldron body ann steadily fixed, and make the ejection of compact collect the convenience.
7. The utility model discloses a set up striker plate and rotation axis, striker plate and rotation axis handing-over, the striker plate is located the discharge gate below, and the ejection of compact can be controlled through the closure of controlling the striker plate to the feeding that the heating was accomplished, makes ejection of compact safe controllable.
Drawings
Fig. 1 is a schematic structural diagram provided in an embodiment of the present invention;
fig. 2 is a front view provided by an embodiment of the present invention;
fig. 3 isbase:Sub>A cross-sectional front viewbase:Sub>A-base:Sub>A of an embodiment of the present invention;
fig. 4 is a right side view provided by an embodiment of the present invention;
fig. 5 is a B-B right side sectional view provided by the embodiment of the present invention.
In the figure: 1. a kettle body; 2. a motor; 3. a heating chamber; 4. a stirring shaft; 5. a fan blade; 6. a fan; 7. a vent; 8. an air circulation pipe; 9. heating plates; 10. screening a screen; 11. a discharge valve; 12. a discharge port; 13. a feed channel; 14. a feed inlet; 15. a fixed mount; 16. a striker plate; 17. a rotating shaft.
Detailed Description
In order to further understand the contents, features and effects of the present invention, the following embodiments are illustrated and described in detail with reference to the accompanying drawings.
The structure of the present invention will be described in detail with reference to the accompanying drawings.
As shown in fig. 1 to 5, the embodiment of the utility model provides a pair of cobaltous hydroxide production is with heating crystallization device, including the cauldron body 1 with be used for heating the heating device of crystalline cobaltous hydroxide, heating device is including locating the hot plate 9 of the 1 inner wall of the cauldron body, locating the feeding part of the 1 top one side of the cauldron body, locating the motor 22 of the 1 top outer wall of the cauldron body, locating the ejection of compact part of the 1 bottom of the cauldron body, locating the heated warehouses 3 in the cauldron body 1, locating the (mixing) shaft 4 at heated warehouses 3 center, locating the stirring part on the (mixing) shaft 4 and locating the air reflux part of the 1 inner wall one side of the cauldron body, hot plate 9 is located between heated warehouses 3 and the 1 inner wall of the cauldron body, the slope sets up in the 1 bottom of the cauldron body, and 1 bottom height orientation of the cauldron body is kept away from ascending of 4, motor 22 and (mixing) shaft 4 fixed connection, heated warehouses 3 is located between hot plate 9 and (mixing) shaft 4, hot plate 9 topmost is no longer than (mixing) shaft 4.
Referring to fig. 3, the stirring component includes three fan blades 5, the fan blades 5 are connected with the stirring shaft 4, an angle between adjacent fan blades 5 is 120 degrees, the top ends of the fan blades 5 are not higher than the highest point of the heating plate 9, and the bottom ends of the fan blades 5 are not lower than the lowest point of the heating plate 9.
Adopt above-mentioned scheme: through setting up flabellum 5, flabellum 5 and hot plate 9 mutually perpendicular make (mixing) shaft 4 rotate through the power of motor 2, drive flabellum 5 around (mixing) shaft 4 is rotatory, make the feeding that gets into the heated warehouses be heated evenly, reduce the reunion, reduce the caking, be heated fully.
Referring to fig. 5, the air backflow component includes a fan 6 disposed on the upper side of the inner wall of the kettle body 1, a vent 7 disposed on the lower side of the outer wall of the kettle body 1, and an air circulation pipe 8 connecting the fan 6 and the vent 7, the vent 7 is communicated with the heating chamber 3, the fan 6 is communicated with the heating chamber 3 and is located right above the vent 7, and the fan 6 is not lower than the highest point of the heating plate 9.
Adopt above-mentioned scheme: the fan 6 is connected with the vent 7 through an air circulating pipe 8, and the fan 6 rotates to enable air above the heating bin 9 to be discharged below the heating bin 9 through the air circulating pipe 8 from the vent 7, so that air inside the heating bin 9 is thermally circulated, and the feeding, drying and crystallizing process is accelerated.
Referring to fig. 5, the discharging part includes a screen 10 disposed at the center of the bottom of the heating chamber 3, a discharging valve 11 disposed below the screen 10, and a discharging hole 12 disposed below the discharging valve 11, wherein the screen 10 and the discharging valve 11 are parallel to each other.
Adopt above-mentioned scheme: the screen cloth 10 is located 11 tops of ejection of compact valve, and the feeding that the heating was accomplished is filtered through screen cloth 10 and is got into discharge gate 12, discharges the cauldron body 1 through ejection of compact valve 11, and the feeding that can make the heating accomplish is discharged controllable, can make the unable discharge of the complete bold granule of unheated.
Referring to fig. 5, the feeding component includes a feeding channel 13 disposed on the upper side of the top of the kettle 1 and a feeding port 14 disposed above the feeding channel 13, and the feeding channel 13 is communicated with the heating chamber 3.
Adopt above-mentioned scheme: the feed inlet 14 is located the feedstock channel 13 top, and the feeding is passed through feedstock channel 13 by feed inlet 14 and is got into heating chamber 3, can make the feeding steadily get into cauldron body 1.
Referring to fig. 1, a fixing frame 15 is arranged below the kettle body 1, and the lowest end of the fixing frame 15 is higher than the lowest end of the discharge hole 12.
Adopt above-mentioned scheme: the fixed mount 15 is fixedly connected with the kettle body 1, so that the kettle body 1 can be stably fixed, and the discharged materials can be conveniently collected.
Referring to fig. 2, the discharge valve 11 includes a striker plate 16 disposed below the screen mesh 10 and a rotating shaft 17 disposed on one side of the striker plate 16, and the striker plate 16 is parallel to the screen mesh 10.
Adopting the scheme; the striker plate 16 and the handing-over of rotation axis 17, the striker plate 16 are located discharge gate 12 below, and the feeding that the heating was accomplished can be through the closed ejection of compact of controlling striker plate 16, makes ejection of compact safe controllable.
The utility model discloses a theory of operation:
when the device is used, firstly feeding materials enter the heating bin 3 through the feeding channel 13, then the feeding materials are heated through the heating plate 9, then the feeding materials are stirred through the fan blades 5 to be heated uniformly, the caking is reduced, meanwhile, air sucked into the heating bin 3 by the fan 6 is discharged to the bottom of the heating bin 3 from the air vent 7 through the air circulating pipe 8, the temperature of the air in the heating bin 3 is kept consistent, finally, the feeding materials after being heated and crystallized enter the discharging valve 11 through the screen 10, and the feeding materials after being heated can be collected through controlling the material baffle 16.
In summary, the following steps: this heating crystallization device is used in cobalt hydrate production through setting up hot plate 9, feeding part, motor 22, ejection of compact part, stirring part and heated warehouses 3, has solved the problem that the cobalt hydrate finished product can't heat the crystallization of current equipment preparation.
It should be noted that, in this document, relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides a cobalt hydroxide production is with heating crystallization device, includes cauldron body (1) and the heating device who is used for heating crystallization cobalt hydroxide, its characterized in that: heating device is including locating hot plate (9) of cauldron body (1) inner wall, locating the feeding part of cauldron body (1) top one side, locating motor (2) of cauldron body (1) top outer wall, locating the ejection of compact part of cauldron body (1) bottom, locating heated warehouses (3) in the cauldron body (1), locating (mixing) shaft (4) at heated warehouses (3) center, locating the stirring part on (mixing) shaft (4) and locating the air reflux part of cauldron body (1) inner wall one side, hot plate (9) are located between heated warehouses (3) and cauldron body (1) inner wall, the slope sets up cauldron body (1) bottom, and stirring shaft (4) rise is highly kept away from to highly orientation in cauldron body (1) bottom, motor (2) and (mixing) shaft (4) fixed connection, heated warehouses (3) are located between hot plate (9) and (mixing) shaft (4), hot plate (9) topmost is no longer than (mixing) top (mixing) 4).
2. The heating crystallization device for producing cobalt hydroxide as claimed in claim 1, wherein: stirring part includes three flabellum (5), flabellum (5) are connected with (mixing) shaft (4), angle 120 degrees between adjacent flabellum (5), flabellum (5) top is not higher than hot plate (9) peak, flabellum (5) bottom is not less than hot plate (9) minimum.
3. The heating crystallization device for producing cobalt hydroxide as claimed in claim 1, wherein: the air reflux part comprises a fan (6) arranged on the upper side of the inner wall of the kettle body (1), a vent (7) arranged on the lower side of the outer wall of the kettle body (1) and an air circulation pipe (8) connected with the fan (6) and the vent (7), the vent (7) is communicated with the heating bin (3), the fan (6) is communicated with the heating bin (3) and is positioned right above the vent (7), and the fan (6) is not lower than the highest point of the heating plate (9).
4. The heating crystallization device for producing cobalt hydroxide as claimed in claim 1, wherein: the discharging component comprises a screen (10) arranged at the center of the bottom of the heating bin (3), a discharging valve (11) arranged below the screen (10) and a discharging port (12) arranged below the discharging valve (11), and the screen (10) is parallel to the discharging valve (11).
5. The heating crystallization device for producing cobalt hydroxide as claimed in claim 1, wherein: the feeding part comprises a feeding channel (13) arranged on the upper side of the top of the kettle body (1) and a feeding hole (14) arranged above the feeding channel (13), and the feeding channel (13) is communicated with the heating bin (3).
6. The heating crystallization device for producing cobalt hydroxide as claimed in claim 1, wherein: the cauldron body (1) below is equipped with mount (15), mount (15) least significant end is higher than discharge gate (12) least significant end.
7. The heating crystallization device for producing cobalt hydroxide as claimed in claim 4, wherein: discharge valve (11) are including locating striker plate (16) of screen cloth (10) below and locating rotation axis (17) of striker plate (16) one side, striker plate (16) are parallel to each other with screen cloth (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222327130.9U CN218529850U (en) | 2022-09-02 | 2022-09-02 | Heating crystallization device for cobalt hydroxide production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222327130.9U CN218529850U (en) | 2022-09-02 | 2022-09-02 | Heating crystallization device for cobalt hydroxide production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218529850U true CN218529850U (en) | 2023-02-28 |
Family
ID=85270076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222327130.9U Expired - Fee Related CN218529850U (en) | 2022-09-02 | 2022-09-02 | Heating crystallization device for cobalt hydroxide production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218529850U (en) |
-
2022
- 2022-09-02 CN CN202222327130.9U patent/CN218529850U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20230228 |