CN212524052U - Novel multifunctional reactor - Google Patents
Novel multifunctional reactor Download PDFInfo
- Publication number
- CN212524052U CN212524052U CN202021029656.3U CN202021029656U CN212524052U CN 212524052 U CN212524052 U CN 212524052U CN 202021029656 U CN202021029656 U CN 202021029656U CN 212524052 U CN212524052 U CN 212524052U
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- reaction
- trap
- reactor
- reaction wells
- magnetic stirring
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- 238000003760 magnetic stirring Methods 0.000 claims abstract description 13
- 238000007789 sealing Methods 0.000 claims abstract description 11
- 229910001873 dinitrogen Inorganic materials 0.000 claims description 7
- 239000002826 coolant Substances 0.000 claims description 6
- 230000007306 turnover Effects 0.000 claims description 3
- 238000003801 milling Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 abstract description 11
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 3
- 238000012216 screening Methods 0.000 abstract description 2
- 238000010907 mechanical stirring Methods 0.000 description 2
- 238000011020 pilot scale process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000003321 amplification Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
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Abstract
The utility model discloses a novel multifunctional reactor, which comprises a reactor main body, a reaction bottle, a ground conduit and a sealing ring, wherein the reactor main body comprises four reaction wells, a nitrogen conduit and a central control screen, the reaction wells are of a round bottom cylinder structure, the four reaction wells are all connected to the central control screen, a magnetic stirring system is arranged at the bottom of the reaction wells, a heating ring is arranged above the magnetic stirring system, a temperature detector is also arranged at the bottom of the reaction wells, heat-conducting cooling oil is filled in the reaction wells, an inlet pipe for circulating the heat-conducting cooling oil is arranged on the side wall, the reaction bottle is arranged in the reaction wells, the upper parts of the reaction bottles are connected through the ground conduit and are fixed through the sealing ring, the utility model can simultaneously carry out multi-, the reaction can be carried out simultaneously according to different conditions such as reaction temperature, material amount and the like, so that condition screening is facilitated, and manpower, material resources and cost are saved.
Description
The technical field is as follows:
the utility model belongs to the technical field of test instrument, especially, relate to a novel multifunctional reactor.
Background art:
the reactor is common equipment in chemical industry and pharmaceutical industry, and a reaction kettle is generally used as the reactor in pilot scale amplification and production stages and is provided with accessories such as mechanical stirring, interlayer heating and cooling and the like. The bench test stage generally comprises a heat-collecting type constant-temperature stirrer, a low-temperature reaction bath and the like, and is generally carried out by magnetic stirring or mechanical stirring.
In the test stage of a medicine and chemical laboratory, multiple conditions are usually required to be screened, only one reaction can be carried out by common reaction equipment, a large number of experimental conditions are required, and too many pieces of equipment are required by the screening conditions, so that the time is delayed, and the manpower and material resources are consumed.
The utility model has the following contents:
to the above problem, the to-be-solved technical problem of the utility model is to provide a novel multifunctional reactor, including reactor main part, reaction flask, mill mouthful pipe and sealing washer, the reactor main part includes four reaction traps, nitrogen gas pipe and well accuse screen, the reaction trap is round bottom cylinder structure, four the reaction trap all is connected to well accuse screen, magnetic stirring system is installed to the reaction trap bottom, the magnetic stirring system top is equipped with the heating coil, the reaction trap bottom still is equipped with temperature detector, is equipped with the heat conduction coolant oil in the reaction trap, is equipped with the business turn over pipe that is used for the circulation of heat conduction coolant oil on the lateral wall, the reaction flask is placed in the reaction trap, the top of reaction flask is fixed through milling mouthful pipe connection and through the sealing washer, it sets up nitrogen gas pipe connection with the reactor main part to mill mouthful pipe.
Preferably, the reaction bottle is a single-mouth eggplant-shaped bottle.
The utility model discloses beneficial effect: the utility model discloses a novel multifunctional reactor can heat simultaneously, the reaction of multiple experimental conditions such as cooling, save time and human cost improve test efficiency.
Description of the drawings:
for ease of illustration, the invention is described in detail by the following detailed description and accompanying drawings.
FIG. 1 is a schematic view of the overall structure of the present invention;
fig. 2 is a schematic diagram of the overall structure of the reaction trap.
In the figure: 1-a reactor body; 2-a central control screen; 3-nitrogen gas conduit; 4-reaction trap; 5-a magnetic stirring system; 6-heating a ring; 7-temperature detector; 8-heat conducting cooling oil; 9-sealing ring; 10-a ground conduit; 11-inlet and outlet pipes for heat-conducting cooling oil circulation; 12-reaction flask.
The specific implementation mode is as follows:
in order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described below with reference to specific embodiments shown in the accompanying drawings. It should be understood that the description is intended to be illustrative only and is not intended to limit the scope of the present invention. Moreover, in the following description, descriptions of well-known structures and techniques are omitted so as to not unnecessarily obscure the concepts of the present invention.
As shown in figures 1-2, the utility model relates to a novel multifunctional reactor, which comprises a reactor main body 1, a reaction bottle 12, a ground conduit 10 and a sealing ring 9, the reactor body 1 comprises four reaction wells 4, a nitrogen guide pipe 3 and a central control screen 2, the reaction wells 4 are of a round-bottom cylindrical structure, the four reaction wells 4 are all connected to the central control screen 2, a magnetic stirring system 5 is arranged at the bottom of the reaction well 4, a heating ring 6 is arranged above the magnetic stirring system 5, the bottom of the reaction trap 4 is also provided with a temperature detector 7, the reaction trap 4 is internally provided with heat conduction cooling oil 8, the side wall is provided with an inlet and outlet pipe 11 for heat conduction cooling oil circulation, the reaction bottle 12 is placed in the reaction trap 4, the upper part of the reaction bottle 12 is connected through a ground conduit 10 and fixed through a sealing ring 9, and the ground conduit 10 is connected with a nitrogen conduit 3 arranged on the reactor main body 1.
Specifically, the reactor body comprises four reaction wells 4, a nitrogen guide pipe 3 for experiments requiring nitrogen protection, and additionally comprises a central control screen 2, wherein the four reaction wells 4 are connected to the central control screen 2. The reaction trap 4 is a round-bottom cylinder, and the bottom of the reaction trap is provided with a magnetic stirring system 5 which is used for providing magnetic stirring for the reactor main body 1; a heating ring 6 is arranged above the magnetic stirring system 5 and used for heating; the bottom of the reaction trap 4 is also provided with a temperature detector 7 for detecting the temperature of the system; the reaction trap 4 is filled with special heat-conducting cooling oil which can be heated and cooled; the side wall is provided with an inlet and outlet pipe 11 for heat conduction cooling oil circulation, which is used for reducing the temperature of the system; a sealing ring 9 is arranged above the reaction trap 4 and used for fixing a reaction bottle 12; the reaction vessel 12 used in the reaction well 4 is generally a single-mouth eggplant-shaped vessel.
The working principle is as follows: open reactor main part 1 switch, reaction trap 4 regulates and control the temperature according to the temperature that experimental needs, low temperature reaction then closes heating ring 6 heating effect, open the business turn over pipe 11 of heat conduction coolant oil circulation, cool down reaction trap 4 inside heat conduction coolant oil 8, reaction trap 4 is placed into to required reaction bottle 12 of experimental scale, add magnetic stirrers, required reaction mass, reaction bottle 12 top is connected with ground mouthful pipe 10, with the fixed reaction bottle of sealing washer 9, the pilot scale generally requires the reaction system to be the nitrogen gas system, through grinding mouthful pipe 10 and reactor main part 1 set up nitrogen gas pipe 3 and being connected. If the reaction is carried out under the heating condition, the inlet and outlet pipe 11 for circulating the heat-conducting cooling oil is closed, the heating ring 6 is started for heating, the temperature is adjusted according to the temperature of the system detected by the temperature detector 7, and the temperature regulation and control are completed in the central control screen 2.
The basic principles and the main features of the invention and the advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (2)
1. The utility model provides a novel multifunctional reactor, a serial communication port, includes reactor main part, reaction flask, mill mouthful pipe and sealing washer, the reactor main part includes four reaction traps, nitrogen gas pipe and well accuse screen, the reaction trap is round bottom cylinder structure, four the reaction trap all is connected to well accuse screen, magnetic stirring system is installed to the reaction trap bottom, the magnetic stirring system top is equipped with the heating collar, the reaction trap bottom still is equipped with temperature detector, is equipped with the heat conduction coolant oil in the reaction trap, is equipped with the business turn over pipe that is used for the circulation of heat conduction coolant oil on the lateral wall, the reaction flask is placed in the reaction trap, the top of reaction flask is fixed through milling mouthful pipe connection and through the sealing washer, it sets up nitrogen gas pipe connection with the reactor main part to grind mouthful pipe.
2. The novel multifunctional reactor according to claim 1, characterized in that: the reaction bottle is a single-mouth eggplant-shaped bottle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021029656.3U CN212524052U (en) | 2020-06-08 | 2020-06-08 | Novel multifunctional reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202021029656.3U CN212524052U (en) | 2020-06-08 | 2020-06-08 | Novel multifunctional reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212524052U true CN212524052U (en) | 2021-02-12 |
Family
ID=74640144
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202021029656.3U Active CN212524052U (en) | 2020-06-08 | 2020-06-08 | Novel multifunctional reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212524052U (en) |
-
2020
- 2020-06-08 CN CN202021029656.3U patent/CN212524052U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A new multifunctional reactor Effective date of registration: 20220420 Granted publication date: 20210212 Pledgee: Fujian Straits bank Limited by Share Ltd. Fuqing branch Pledgor: FUJIAN KANGHONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2022350000042 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230413 Granted publication date: 20210212 Pledgee: Fujian Straits bank Limited by Share Ltd. Fuqing branch Pledgor: FUJIAN KANGHONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2022350000042 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A New Type of Multifunctional Reactor Effective date of registration: 20230418 Granted publication date: 20210212 Pledgee: Fujian Straits bank Limited by Share Ltd. Fuqing branch Pledgor: FUJIAN KANGHONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2023350000121 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20210212 Pledgee: Fujian Straits bank Limited by Share Ltd. Fuqing branch Pledgor: FUJIAN KANGHONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2023350000121 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right |