CN206292142U - One seed nucleus level pipe fitting intercrystalline corrosion detection means - Google Patents

One seed nucleus level pipe fitting intercrystalline corrosion detection means Download PDF

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Publication number
CN206292142U
CN206292142U CN201621226562.9U CN201621226562U CN206292142U CN 206292142 U CN206292142 U CN 206292142U CN 201621226562 U CN201621226562 U CN 201621226562U CN 206292142 U CN206292142 U CN 206292142U
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China
Prior art keywords
pipe fitting
detection means
level pipe
sour cylinder
kuppe
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CN201621226562.9U
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Chinese (zh)
Inventor
屈鹰
陈勇
王小军
潘峰
刘志诚
张双庆
庄惠银
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Sichuan Sanzhong Scmp Nuclear Equipment Manufacture Inc (assanem)
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Sichuan Sanzhong Scmp Nuclear Equipment Manufacture Inc (assanem)
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Abstract

One seed nucleus level pipe fitting intercrystalline corrosion detection means, including sour cylinder, protective case, heating mantle, kuppe and condensation reflux unit.Protective case and heating mantle are sheathed on sour cylinder outside successively, and sour cylinder top is fixed in kuppe activity, and condensation reflux unit is movably connected on the top of kuppe.The utility model replaces existing conical flask using the larger sour cylinder of volume, to accommodate the core level pipe fitting sample with large surface area, so as to reduce pipe fitting sample difficulty of processing, it is ensured that sampling is comprehensive, it is ensured that result of the test correctness.

Description

One seed nucleus level pipe fitting intercrystalline corrosion detection means
Technical field
The utility model is related to core level pipe fitting technical field of quality detection, more particularly to seed nucleus level pipe fitting intercrystalline corrosion inspection Survey device.
Background technology
At present, when intercrystalline corrosion detection is carried out, need to be according to GB/T4334-2008《The corrosion stainless steel of metal and alloy Huey test method》Regulation carry out sampling processing.Because the conical flask volume that existing Huey test is used is smaller, Thus the surface area of sample is smaller, only 20mmX30mm.And core level tube wall thickness is generally more than ten centimetres to tens centimetres, and firmly Degree is high, and according to existing sampling size, on the one hand sampling difficulty of processing is very big, on the other hand, samples too small relative to pipe fitting, difficult To represent pipe fitting general token, conclusion (of pressure testing) is caused to there is error.
Utility model content
The utility model provides seed nucleus level pipe fitting intercrystalline corrosion detection means, not enough to solve above-mentioned prior art.Adopt Replace existing conical flask with the larger sour cylinder of volume, to accommodate the core level pipe fitting sample with large surface area, so as to drop Low pipe fitting sample difficulty of processing, it is ensured that sampling is comprehensive, it is ensured that result of the test correctness.
In order to realize the purpose of this utility model, intend using following technology:
One seed nucleus level pipe fitting intercrystalline corrosion detection means, it is characterised in that including sour cylinder, protective case, heating mantle, kuppe And condensation reflux unit, the protective case and the heating mantle be sheathed on the sour cylinder outside successively, and the kuppe activity is solid Due to the sour cylinder top, the condensation reflux unit is movably connected on the top of the kuppe.
Further, the sour cylinder is cylindrical, and cylinder inner bottom part is provided with specimen holder, and top is provided with convex edge.
Further, the kuppe is in frustum, includes bottom plug, oblique top and refluxing opening, the oblique top successively from the bottom to top Bottom is provided with locking edge.
Further, the bottom plug fits in the sour cylinder top inner wall, and the locking is arranged at the convex edge along laminating Top.
Further, the heating mantle top is provided with some lockers, and the locker activity pressure is located at the locking at.
Further, the sour cylinder, the specimen holder and the kuppe use glass material.
Further, the bottom plug outer surface uses frosting technology.
Further, the protective case uses heat-conducting and corrosion-resistant material.
Further, the heating mantle uses adjustable thermostatic heater.
Further, the height of the sour cylinder is more than the protective case and the height of the heating mantle.
The beneficial effects of the utility model are:
1st, the utility model replaces existing conical flask using the larger sour cylinder of volume, to accommodate with large surface area Core level pipe fitting sample, so as to reduce pipe fitting sample difficulty of processing, it is ensured that sampling is comprehensive, it is ensured that result of the test correctness.
2nd, the utility model closes sour cylinder using frustum kuppe and water conservancy diversion boiling is sour, simple to operate, sealing property reliability, And be conducive to the sour film-cooled heat of increase boiling, accelerate acid solution cooling.
3rd, the utility model, compared with traditional heating plate, is conducive to raising heat energy utilization to imitate using the constant temperature electric heating sour cylinder of set heating Rate, saving energy consumption.
Brief description of the drawings
Fig. 1 shows the utility model structural representation.
Specific embodiment
As shown in figure 1, seed nucleus level pipe fitting intercrystalline corrosion detection means, including sour cylinder 1, protective case 2, heating mantle 3, water conservancy diversion Cover 4 and condensation reflux unit 5.The protective case 2 and the heating mantle 3 are sheathed on the outside of the sour cylinder 1, the kuppe successively The top of the sour cylinder 1 is fixed in 4 activities, and the condensation reflux unit 5 is movably connected on the top of the kuppe 4.The acid Cylinder 1 is used to contain sample and testing liquid.The protective case 2 is used to protect sour cylinder 1, and prevents the rupture of sour cylinder 1 post-etching The heating mantle 3.The heating mantle 3 is used to provide constant temperature for the testing liquid in the sour cylinder 1, to keep slight boiling condition to complete Detection process.The kuppe 4 is used to close the sour cylinder 1, and derives the boiling testing liquid in the sour cylinder 1.It is described cold Solidifying reflux 5 is used to cool down the testing liquid of boiling, promotes it to flow back, to keep volume of sample solution in the sour cylinder 1.
The sour cylinder 1 is cylindrical, and cylinder inner bottom part is provided with specimen holder 11, and top is provided with convex edge 12.The specimen holder 11 is used Core level pipe fitting sample to be detected is put in load.It is easy to pick and place the sour cylinder 1 in the convex edge 12.
The kuppe 4 is in frustum, includes bottom plug 41, oblique top 42 and refluxing opening 43, the oblique top successively from the bottom to top 42 bottoms are provided with locking along 44.The bottom plug 41 fits in the top inner wall of sour cylinder 1, and the locking is arranged at institute along 44 laminatings State the top of convex edge 12.The bottom plug 41 is used to close the kuppe 4 and the sour cylinder 1.The oblique top 42 is boiled for water conservancy diversion The testing liquid risen, is conducive to the film-cooled heat of increase boiling liquid, the cooling of accelerated test solution.
The top of the heating mantle 3 is provided with some lockers 6, and the activity of the locker 6 pressure is locked at along 44 located at described.Institute State the sealing property that locker 6 is conducive to improving the kuppe 4 and the sour cylinder 1, it is to avoid testing liquid in specimen Leakage.
The sour cylinder 1, the specimen holder 11 and the kuppe 4 use glass material.It is easy to observation, and it is rotten to intergranular Corrosion test is noiseless.
The outer surface of the bottom plug 41 uses frosting technology.It is close with the sour cylinder 1 further to improve the kuppe 4 Sealing property.
The protective case 2 uses heat-conducting and corrosion-resistant material.Improve the sour cylinder 1 be heated, anticollision performance, and in the acid When cylinder 1 occurs leakage, the heating mantle 3 is protected to exempt from corrosion.
The heating mantle 3 uses adjustable thermostatic heater.It is easy to regulate and control heating-up temperature, to keep long-time testing liquid Slight boiling condition.
The height of the sour cylinder 1 is more than the protective case 2 and the height of the heating mantle 3.It is easy to taking for the sour cylinder 1 Put, and be easy to observe the response situation in the sour cylinder 1.
Illustrate that the utility model specific embodiment is as follows in conjunction with the embodiments:
Using the method B in GB/T4334-2008-stainless steel sulfuric acid-ferric sulfate corrosion tests, nuclear power is responsible for Welding junction carries out intercrystalline corrosion detection.
10cmx15cm is sampled in nuclear power supervisor's welding test block, grinding is the sample sheet 9 of thickness 3mm.
The sour cylinder 1 diameter 30cm, height 20cm.After height is set with the outside of it for the protective case 2 of 10cm, move into In the heating mantle 3 of inside wall height 10cm.
The specimen holder 11 has glass column to be spliced, and external dimensions is 12cmx17cmx4cm, by the sample sheet 9 loads are located at the hollow out upper surface of the specimen holder 11.
3L sulfuric acid-ferric sulfate testing liquid is added in the sour cylinder 1, the sample sheet 9 is fully immersed in experiment Solution middle part.
The kuppe 4 is covered on the top of the sour cylinder 1, the bottom plug 41 is probeed into the top of the sour cylinder 1, and fit In the inwall of sour cylinder 1;The locking is set along 44 loads, fit in the top of the convex edge 12, seal described using liquid paraffin Lock the gap along between 44 and the convex edge 12.
The locker 6 is pressed successively and is locked at along 44 located at described, the kuppe 4 is closed with the sour cylinder 1.
The condensation reflux unit 5 is sealed by attachment structure and is arranged at the refluxing opening 43.Complete this practicality new Type is assembled.
Start the heating mantle 3 to heat up, the testing liquid in the sour cylinder 1 is seethed with excitement.Adjust the temperature of the heating mantle 3 Degree, makes testing liquid keep slight boiling condition, after constant temperature 120h, closes the heating mantle 3.
The locking of the locker 6 is released, the condensation reflux unit 5 is pulled down from the kuppe 4, led described Stream cover 4 is pulled down from the top of the sour cylinder 1.
The sample sheet 9 is taken out in from the sour cylinder 1, it is clean, dry with the soft corrosion product for brushing off surface under flowing water It is dry, weigh, calculate corrosion rate, to evaluate sample intercrystalline corrosion result.

Claims (9)

1. a seed nucleus level pipe fitting intercrystalline corrosion detection means, it is characterised in that including sour cylinder (1), protective case (2), heating mantle (3), kuppe (4) and condensation reflux unit (5), the protective case (2) and the heating mantle (3) are sheathed on the sour cylinder successively (1) sour cylinder (1) top is fixed in outside, the kuppe (4) activity, and the condensation reflux unit (5) is movably connected on The top of the kuppe (4).
2. seed nucleus according to claim 1 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the sour cylinder (1) Cylindrical, cylinder inner bottom part is provided with specimen holder (11), and top is provided with convex edge (12);The kuppe (4) in frustum, by it is lower extremely On successively include bottom plug (41), oblique top (42) and refluxing opening (43), oblique top (42) bottom be provided with locking edge (44).
3. seed nucleus according to claim 2 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the bottom plug (41) Sour cylinder (1) top inner wall is fitted in, the locking is arranged at the top of the convex edge (12) along (44) laminating.
4. seed nucleus according to claim 2 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the heating mantle (3) top is provided with some lockers (6), and locker (6) the activity pressure is located at the locking along (44) place.
5. seed nucleus according to claim 2 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the sour cylinder (1), The specimen holder (11) and the kuppe (4) use glass material.
6. seed nucleus according to claim 2 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the bottom plug (41) Outer surface uses frosting technology.
7. seed nucleus according to claim 1 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the protective case (2) heat-conducting and corrosion-resistant material is used.
8. seed nucleus according to claim 1 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the heating mantle (3) adjustable thermostatic heater is used.
9. seed nucleus according to claim 1 level pipe fitting intercrystalline corrosion detection means, it is characterised in that the sour cylinder (1) Height of the height more than the protective case (2) and the heating mantle (3).
CN201621226562.9U 2016-11-15 2016-11-15 One seed nucleus level pipe fitting intercrystalline corrosion detection means Active CN206292142U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621226562.9U CN206292142U (en) 2016-11-15 2016-11-15 One seed nucleus level pipe fitting intercrystalline corrosion detection means

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621226562.9U CN206292142U (en) 2016-11-15 2016-11-15 One seed nucleus level pipe fitting intercrystalline corrosion detection means

Publications (1)

Publication Number Publication Date
CN206292142U true CN206292142U (en) 2017-06-30

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107462513A (en) * 2017-07-03 2017-12-12 岭东核电有限公司 The decision method and decision-making system of the intergranular stress corrosion of nuclear power station steam generator

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107462513A (en) * 2017-07-03 2017-12-12 岭东核电有限公司 The decision method and decision-making system of the intergranular stress corrosion of nuclear power station steam generator

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