CN207076455U - A kind of high molecular weight reactive pot - Google Patents
A kind of high molecular weight reactive pot Download PDFInfo
- Publication number
- CN207076455U CN207076455U CN201720955623.3U CN201720955623U CN207076455U CN 207076455 U CN207076455 U CN 207076455U CN 201720955623 U CN201720955623 U CN 201720955623U CN 207076455 U CN207076455 U CN 207076455U
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- China
- Prior art keywords
- agitating shaft
- reactor
- high molecular
- molecular weight
- stirring
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- 238000003756 stirring Methods 0.000 claims abstract description 38
- 238000001514 detection method Methods 0.000 claims abstract description 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 238000001816 cooling Methods 0.000 claims abstract description 19
- 238000009413 insulation Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000005485 electric heating Methods 0.000 claims abstract description 7
- 238000005096 rolling process Methods 0.000 claims abstract description 7
- 125000004122 cyclic group Chemical group 0.000 claims description 8
- 238000005187 foaming Methods 0.000 claims description 7
- 239000000725 suspension Substances 0.000 claims description 7
- 230000005611 electricity Effects 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 7
- 239000007788 liquid Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses a kind of high molecular weight reactive pot,Including reacting furnace-e/or and kettle cover,Reactor is provided with inside reacting furnace-e/or,Heat-insulation layer and interior cooling coil are installed with reacting furnace-e/or inner surface,And electric heating block is provided between interior cooler pan and reactor,Kettle cover both sides are installed with catheter pressure and sample detection conduit respectively,Agitating shaft is provided with by rolling bearing between catheter pressure and sample detection conduit,Agitating shaft both ends are connected to stirring motor and propeller agitator,Internal transporting passage is provided with inside agitating shaft,Propeller agitator is made up of some groups of stirring sheets,Scattered hole of overflowing is equipped between adjacent stirring sheet,Flow guiding disc is also installed with agitating shaft and stirring motor junction,Water conservancy diversion disc side is installed with feed tube respectively,Can be that uniformly mixing can be achieved while added material enters,And the temperature and pressure balance of inside will not be destroyed,Reaction is without dead angle,Form uniform mixing effect comprehensively,Improve the homogeneous degree of W-response.
Description
Technical field
Reaction unit technical field is the utility model is related to, specially a kind of high molecular weight reactive pot.
Background technology
High molecular weight reactive pot refers to that industrially carrying out chemical reaction under high pressure produces high molecular equipment.In production process
In, because high molecular weight reactive needs the reaction condition of HTHP, in the course of reaction of reality, just have to control reaction
Temperature and pressure inside kettle, inside reactor, the increase of temperature can be rapidly achieved heating effect by electrical heating, still
How to cool is to be difficult to accurately control, and in prior art means, this course of reaction is serious hysteresis quality be present,
The reaction response time can not accurately be controlled, in chemical reaction process is carried out, in order to improve the efficiency of reaction, typically all can
It is stirred to improve the extent of reaction, but in this process, only with common agitating mode, it is difficult to reach effective
Stirring, reaction dead angle easily be present, reduce the efficiency and uniformity coefficient of course of reaction.
And need to add various complementary materials according to the demand of reality during the course of the reaction, and at this
During individual, common high molecular weight reactive device all needs directly to uncap to be added, and so carries out auxiliary material and adds a side
Face can destroy internal balance, and the heat of inside and pressure are scattered and disappeared and spread, does not reach the level of demand, on the other hand, directly
The auxiliary material inside reactor is added to want to reach preferable reaction effect, it is necessary to which uniformly stirring is spread, and this is also needs
One process, there is certain hysteresis quality, influence the quality and efficiency of reaction.
Utility model content
In order to overcome the shortcomings of prior art, the utility model provides a kind of high molecular weight reactive pot, can be in addition material
Uniformly mixing can be achieved while material enters, and the temperature and pressure balance of inside will not be destroyed, react no dead angle, formed comprehensively equal
Even mixing effect, the homogeneous degree of W-response is improved, effectively can be solved the problems, such as in background technology.
Technical scheme is used by the utility model solves its technical problem：A kind of high molecular weight reactive pot, including reaction
Body of heater and kettle cover, the reacting furnace-e/or inside are provided with reactor, are provided with chimeric projection in reactor inside top, the kettle cover leads to
Chimeric raised and reactor airtight connection is crossed, heat-insulation layer is installed with reacting furnace-e/or inner surface, in heat-insulation layer and reactor
Between be additionally provided with interior cooling coil, and electric heating block is provided between interior cooler pan and reactor, the kettle cover both sides are fixed respectively
Catheter pressure and sample detection conduit are installed, rolling bearing is additionally provided between catheter pressure and sample detection conduit, it is described
Agitating shaft is provided with inside rolling bearing, the agitating shaft both ends are connected to stirring motor and propeller agitator, described to stir
Mix and form internal transporting passage inside axle for hollow structure, the propeller agitator is made up of some groups of stirring sheets, and is stirred
Piece with agitating shaft oblique, is equipped with scattered hole of overflowing between adjacent stirring sheet, also fixed in agitating shaft and stirring motor junction
Flow guiding disc is installed, the water conservancy diversion disc side is installed with feed tube respectively.
As a kind of preferable technical scheme of the utility model, the interior cooling coil forms closure by twofold mode
Circulation loop, cyclic water tank is respectively connected with interior cooling coil both ends, the cyclic water tank is located at the top of heat-insulation layer, and recirculated water
Adiabatic insulation is additionally provided between case and heat-insulation layer.
As a kind of preferable technical scheme of the utility model, the catheter pressure is connected with pressure detecting by connection ring
Table, and unidirectional relief valve is installed with the inside of pressure detecting table.
As a kind of preferable technical scheme of the utility model, the sample detection conduit is S-type, and sample detection conduit
Reactor bottom is extended to close to reactor inwall.
As a kind of preferable technical scheme of the utility model, also pass through branch between the feed tube and sample detection conduit
Suspension connection is supportted, and Flow-rate adjustment plate is provided with supporting suspension, the Flow-rate adjustment plate is located on feed tube.
As a kind of preferable technical scheme of the utility model, the agitating shaft least significant end is also installed with foaming ring,
The foaming ring is in that interior 8 fonts arrange by symmetry axis of agitating shaft.
Compared with prior art, the beneficial effects of the utility model are：During the utility model is by the way that agitating shaft is arranged to
Hollow structure, and internal transporting passage is internally formed, and connected internal transporting passage and feed tube by the effect of flow guiding disc
Lead to so that the liquid inside feed tube can be entered inside reactor by internal transporting passage, be completed in airtight condition
Under fill process, and entered by the scattered hole of overflowing in stirring in reactor, itself has larger centrifugal action, can
Preferably incorporate in reactor internal liquid, and pressure detecting and sample are realized by catheter pressure and sample detection conduit respectively
Quality is detected, and by just adding interior cooling coil on the outside of electric heating block, control electricity is quickly cooled down by way of water cooling
The heating-up temperature of hot block, there is the advantages of regulation temperature-responsive is fast, and by stirring the propeller agitator of shaft end setting,
Rotating flow is formed during acting on stirring by the oblique of stirring sheet, the region that stirring sheet can be driven not feed through to,
Uniform mixing effect comprehensively is formed, prevents from stirring the generation at dead angle, improves the homogeneous degree of W-response.
Brief description of the drawings
Fig. 1 is the utility model structure diagram；
In figure：1- reacting furnace-e/ors；2- kettle covers；3- reactors；The chimeric projections of 4-；5- heat-insulation layers；Cooling coil in 6-；7- electricity
Hot block；8- catheter pressures；9- sample detection conduits；10- rolling bearings；11- agitating shafts；12- stirring motors；13- push types stir
Mix device；Transporting passage inside 14-；15- stirring sheets；16-, which overflows, dissipates hole；17- flow guiding discs；18- feed tubes；19- cyclic water tanks；20-
Adiabatic insulation；21- connection rings；22- pressure detecting tables；The unidirectional relief valves of 23-；24- supporting suspensions；25- Flow-rate adjustment plates；
26- foaming rings.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Embodiment：
As shown in figure 1, the utility model provides a kind of high molecular weight reactive pot, including reacting furnace-e/or 1 and kettle cover 2, it is described
The inside of reacting furnace-e/or 1 is provided with reactor 3, is provided with chimeric projection 4 in the inside top of reactor 3, the kettle cover 2 passes through chimeric projection
4 with the airtight connection of reactor 3, heat-insulation layer 5 is installed with the inner surface of reacting furnace-e/or 1, between heat-insulation layer 5 and reactor 3
Interior cooling coil 6 is additionally provided with, and electric heating block 7 is provided between interior cooling coil 6 and reactor 3.
The both sides of kettle cover 2 are installed with catheter pressure 8 and sample detection conduit 9 respectively, and the catheter pressure 8 passes through
Connection ring 21 is connected with pressure detecting table 22, and is installed with unidirectional relief valve 23 in the inner side of pressure detecting table 22, on the one hand
The monitoring of pressure is realized, the pressure of setting value is on the other hand exceeded by the release of unidirectional relief valve 23, maintains the balance model of pressure
Enclose, the sample detection conduit 9 is S-type, and sample detection conduit 9 extends to the bottom of reactor 3 close to the inwall of reactor 3, just
In extracting uniform reactive material, the precision of detection is improved, is additionally provided with and turns between catheter pressure 8 and sample detection conduit 9
Dynamic bearing 10, the inside of rolling bearing 10 are provided with agitating shaft 11, and the both ends of agitating shaft 11 are connected to stirring motor 12
With propeller agitator 13, the inside of agitating shaft 11 forms internal transporting passage 14, the pusher stirring for hollow structure
Device 13 is made up of some groups of stirring sheets 15, and stirring sheet 15 is equipped with the oblique of agitating shaft 11 between adjacent stirring sheet 15
Overflow and dissipate hole 16, flow guiding disc 17, the side of flow guiding disc 17 point are also installed with agitating shaft 11 and the junction of stirring motor 12
Feed tube 18 is not installed with, is also connected between the feed tube 18 and sample detection conduit 9 by supporting suspension 24, and
Supporting suspension 24 is provided with Flow-rate adjustment plate 25, and the Flow-rate adjustment plate 25 is located on feed tube 18, adjusts feed tube 18
Enter flow quantity degree.
Preferably, the interior cooling coil 6 forms closed loop by twofold mode, in interior cooling coil 6
Both ends are respectively connected with cyclic water tank 19, and the cyclic water tank 19 is located at the top of heat-insulation layer 5, and cyclic water tank 19 and heat-insulation layer 5 it
Between be additionally provided with adiabatic insulation 20, the response modes of quick temperature control are realized by way of water cooling, and by separating heat-insulation layer 5,
Being exchanged with each other between heat can be prevented, influences the heat-sinking capability of cooling system.
It may further be preferable that the least significant end of agitating shaft 11 is also installed with foaming ring 26, the foaming ring 26 is in
Interior 8 font and with agitating shaft 11 be symmetry axis arrange, by the stirring bubble of bubble ring 26, the bubble of formation can improve
Mixing uniformity inside reaction solution.
Of the present utility model to be mainly characterized by, the utility model by agitating shaft by being arranged to hollow structure, and inside
Portion forms internal transporting passage, and is connected internal transporting passage with feed tube by the effect of flow guiding disc so that enters
Liquid inside liquid pipe can be entered inside reactor by internal transporting passage, complete fill process in confined conditions,
And entered by the scattered hole of overflowing in stirring in reactor, itself has larger centrifugal action, can preferably incorporate anti-
Answer in kettle internal liquid, and realize that pressure detecting and sample quality detect by catheter pressure and sample detection conduit respectively,
And by just adding interior cooling coil on the outside of electric heating block, the heating temperature of control electric heating block is quickly cooled down by way of water cooling
Degree, there is the advantages of regulation temperature-responsive is fast, and by the propeller agitator in stirring shaft end setting, pass through stirring sheet
Oblique forms rotating flow during acting on stirring, the region that stirring sheet can be driven not feed through to, and is formed comprehensively uniform
Mixing effect, prevent from stirring the generation at dead angle, improve the homogeneous degree of W-response.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and
And in the case of without departing substantially from spirit or essential attributes of the present utility model, it can realize that this practicality is new in other specific forms
Type.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and is nonrestrictive, this practicality is new
The scope of type limits by appended claims rather than described above, it is intended that the equivalency fallen in claim is contained
All changes in justice and scope are included in the utility model.Any reference in claim should not be considered as limitation
Involved claim.
Claims (6)
1. a kind of high molecular weight reactive pot, including reacting furnace-e/or（1）And kettle cover（2）, the reacting furnace-e/or（1）Inside is provided with reactor
（3）, in reactor（3）Inside top is provided with chimeric projection（4）, the kettle cover（2）Pass through chimeric projection（4）With reactor（3）
Airtight connection, in reacting furnace-e/or（1）Inner surface is installed with heat-insulation layer（5）, it is characterised in that：In heat-insulation layer（5）And reaction
Kettle（3）Between be additionally provided with interior cooling coil（6）, and in interior cooling coil（6）And reactor（3）Between be provided with electric heating block（7）, institute
State kettle cover（2）Both sides are installed with catheter pressure respectively（8）With sample detection conduit（9）, in catheter pressure（8）Examined with sample
Survey conduit（9）Between be additionally provided with rolling bearing（10）, the rolling bearing（10）Inside is provided with agitating shaft（11）, the agitating shaft
（11）Both ends are connected to stirring motor（12）And propeller agitator（13）, the agitating shaft（11）Inside is hollow structure
Form internal transporting passage（14）, the propeller agitator（13）By some groups of stirring sheets（15）Composition, and stirring sheet（15）
And agitating shaft（11）Oblique, in adjacent stirring sheet（15）Between be equipped with scattered hole of overflowing（16）, in agitating shaft（11）With stirring electricity
Machine（12）Junction is also installed with flow guiding disc（17）, the flow guiding disc（17）Side is installed with feed tube respectively
（18）.
A kind of 2. high molecular weight reactive pot according to claim 1, it is characterised in that：The interior cooling coil（6）By double
Folding mode forms closed loop, in interior cooling coil（6）Both ends are respectively connected with cyclic water tank（19）, the cyclic water tank
（19）It is located at heat-insulation layer（5）Top, and cyclic water tank（19）And heat-insulation layer（5）Between be additionally provided with adiabatic insulation（20）.
A kind of 3. high molecular weight reactive pot according to claim 1, it is characterised in that：The catheter pressure（8）Pass through connection
Ring（21）It is connected with pressure detecting table（22）, and in pressure detecting table（22）Inner side is installed with unidirectional relief valve（23）.
A kind of 4. high molecular weight reactive pot according to claim 1, it is characterised in that：The sample detection conduit（9）In S
Type, and sample detection conduit（9）Close to reactor（3）Inwall extends to reactor（3）Bottom.
A kind of 5. high molecular weight reactive pot according to claim 1, it is characterised in that：The feed tube（18）And sample detection
Conduit（9）Between also pass through supporting suspension（24）Connection, and in supporting suspension（24）It is provided with Flow-rate adjustment plate（25）, it is described
Flow-rate adjustment plate（25）It is located at feed tube（18）On.
A kind of 6. high molecular weight reactive pot according to claim 1, it is characterised in that：The agitating shaft（11）Least significant end is also solid
Dingan County is equipped with foaming ring（26）, the foaming ring（26）In interior 8 font and with agitating shaft（11）Arranged for symmetry axis.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720955623.3U CN207076455U (en) | 2017-08-02 | 2017-08-02 | A kind of high molecular weight reactive pot |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720955623.3U CN207076455U (en) | 2017-08-02 | 2017-08-02 | A kind of high molecular weight reactive pot |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207076455U true CN207076455U (en) | 2018-03-09 |
Family
ID=61425083
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720955623.3U Expired - Fee Related CN207076455U (en) | 2017-08-02 | 2017-08-02 | A kind of high molecular weight reactive pot |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207076455U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111545155A (en) * | 2020-05-25 | 2020-08-18 | 南京诺知信息科技有限公司 | Reaction device for laboratory for preparing terephthalic acid |
| CN112936634A (en) * | 2021-02-02 | 2021-06-11 | 新沂市星辰新材料科技有限公司 | Dispersion and homogenization equipment for preparing PVC (polyvinyl chloride) terminator and working method thereof |
-
2017
- 2017-08-02 CN CN201720955623.3U patent/CN207076455U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111545155A (en) * | 2020-05-25 | 2020-08-18 | 南京诺知信息科技有限公司 | Reaction device for laboratory for preparing terephthalic acid |
| CN112936634A (en) * | 2021-02-02 | 2021-06-11 | 新沂市星辰新材料科技有限公司 | Dispersion and homogenization equipment for preparing PVC (polyvinyl chloride) terminator and working method thereof |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180309 |
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| CF01 | Termination of patent right due to non-payment of annual fee |