CN205599135U - Metal organic chemistry light reaction unit - Google Patents
Metal organic chemistry light reaction unit Download PDFInfo
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- CN205599135U CN205599135U CN201620432499.8U CN201620432499U CN205599135U CN 205599135 U CN205599135 U CN 205599135U CN 201620432499 U CN201620432499 U CN 201620432499U CN 205599135 U CN205599135 U CN 205599135U
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- reaction chamber
- reaction
- reactant liquor
- photoreaction
- cooling
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Abstract
The utility model provides a metal organic chemistry light reaction unit, including reaction liquid container, reaction chamber, reaction metal, ultraviolet radiation lamp and cooling system, reaction liquid container in be equipped with metal organic chemistry reaction liquid, reaction liquid container passes through the transfer line to be connected with the reaction chamber, the reaction chamber respectively be equipped with a fixing base in both sides about in, be fixed with the reaction metal between the fixing base, the reaction chamber left and right sides be equipped with the ultraviolet radiation lamp that the symmetry set up, the reaction chamber in still be equipped with cooling system, the utility model discloses simple structure, convenient to use is equipped with reaction liquid container, can be with reacting the reagent intensive mixing, both sides respectively are equipped with the ultraviolet lamp for illumination is even, is equipped with condensing equipment, guarantees that the reaction temperature is invariable and suitable, has improved the effect and the efficiency of reaction.
Description
Technical field
This utility model relates to organic synthesis equipment technical field, particularly relates to a kind of Organometallic Chemistry apparatus for photoreaction.
Background technology
In some chemical reaction, particularly in organic reaction, need to carry out under ultraviolet light irradiation, simultaneously need to metallic catalyst participates in reaction.Existing Organometallic Chemistry apparatus for photoreaction directly adds different organic reaction reagent in reaction chamber, cause reacting uneven, ultraviolet light irradiates the effect of uneven impact reaction, owing to reaction can produce heat, and the temperature in reative cell is raised, so that the inadaptable reaction of temperature, further impact effect.
Utility model content
This utility model provides a kind of Organometallic Chemistry apparatus for photoreaction, simple in construction, easy to use, being provided with reactant liquor container, can be sufficiently mixed by reaction reagent, both sides are respectively provided with uviol lamp, make uniform illumination, it is provided with condensing unit, it is ensured that reaction temperature is constant and suitable, improves effect and the efficiency of reaction.
For solving above-mentioned technical problem, the embodiment of the present application provides a kind of Organometallic Chemistry apparatus for photoreaction, including reactant liquor container, reaction chamber, reacting metal, ultra-vioket radiation lamp and cooling system, it is provided with Organometallic Chemistry reactant liquor in described reactant liquor container, reactant liquor container is connected with reaction chamber by tube for transfusion, in described reaction chamber, upper and lower both sides are respectively provided with a fixing seat, it is fixed with reacting metal between fixing seat, the described reaction chamber left and right sides is provided with symmetrically arranged ultra-vioket radiation lamp, is additionally provided with cooling system in described reaction chamber.
As the preferred embodiment of this programme, described reactant liquor upper vessel portion is provided with feed(raw material)inlet, and bottom is provided with heated base, and reactant liquor container bottom is provided with agitating device.
As the preferred embodiment of this programme, described cooling system includes cooling liquid container and cooling tube, and described cooling liquid container is built with coolant, and cooling tube is centered around around reacting metal in the shape of a spiral.
As the preferred embodiment of this programme, it is provided with the reaction pump of conveying reactant liquor in the middle part of described tube for transfusion, in the middle part of described cooling tube, is provided with the cooling pump of circulating cooling liquid.
As the preferred embodiment of this programme, between described ultra-vioket radiation lamp and reaction chamber, set Packed transparent glass layer.
As the preferred embodiment of this programme, being provided with temperature sensor inside described reaction chamber, described temperature sensor is connected and controls its duty with cooling pump, and described reaction chamber bottom is provided with leakage fluid dram.
The one or more technical schemes provided in the embodiment of the present application, at least have the following technical effect that or advantage:
Simple in construction, easy to use, it is provided with reactant liquor container, reaction reagent can be sufficiently mixed, both sides are respectively provided with uviol lamp so that uniform illumination, are provided with condensing unit, it is ensured that reaction temperature is constant and suitable, improve effect and the efficiency of reaction.
Accompanying drawing explanation
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, the accompanying drawing used required in embodiment or description of the prior art will be briefly described below,
It should be evident that the accompanying drawing in describing below is only embodiments more of the present utility model, for those of ordinary skill in the art, on the premise of not paying creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the structural representation of the embodiment of the present application；
In Fig. 1,1, reactant liquor container, 2, reaction chamber, 3, reacting metal, 4, ultra-vioket radiation lamp, 5, fixing seat, 6, feed(raw material)inlet, 7, heated base, 8, agitating device, 9, tube for transfusion, 10, cooling liquid container, 11, cooling tube, 12, reaction pump, 13, cooling pump, 14, leakage fluid dram, 15, transparent glass layer.
Detailed description of the invention
This utility model provides a kind of Organometallic Chemistry apparatus for photoreaction, simple in construction, easy to use, being provided with reactant liquor container, can be sufficiently mixed by reaction reagent, both sides are respectively provided with uviol lamp, make uniform illumination, it is provided with condensing unit, it is ensured that reaction temperature is constant and suitable, improves effect and the efficiency of reaction.
In order to be better understood from technique scheme, below in conjunction with Figure of description and specific embodiment, technique scheme is described in detail.
As shown in Figure 1, a kind of Organometallic Chemistry apparatus for photoreaction described in the present embodiment, including reactant liquor container 1, reaction chamber 2, reacting metal 3, ultra-vioket radiation lamp 4 and cooling system, it is provided with Organometallic Chemistry reactant liquor in described reactant liquor container 1, reactant liquor container 1 is connected with reaction chamber 2 by tube for transfusion 9, in described reaction chamber 2, upper and lower both sides are respectively provided with a fixing seat 5, it is fixed with reacting metal 3 between fixing seat 5, described reaction chamber 2 left and right sides is provided with symmetrically arranged ultra-vioket radiation lamp 4, is additionally provided with cooling system in described reaction chamber 2.
Wherein, in actual applications, described reactant liquor container 1 top is provided with feed(raw material)inlet 6, and bottom is provided with heated base 7, is provided with agitating device 8 bottom reactant liquor container 1.
Wherein, in actual applications, described cooling system includes that cooling liquid container 10 and cooling tube 11, described cooling liquid container 10 are centered around around reacting metal 3 in the shape of a spiral built with coolant, cooling tube 11.
Wherein, in actual applications, it is provided with the reaction pump 12 of conveying reactant liquor in the middle part of described tube for transfusion 9, in the middle part of described cooling tube 11, is provided with the cooling pump 13 of circulating cooling liquid.
Wherein, in actual applications, Packed transparent glass layer 15 is set between described ultra-vioket radiation lamp 4 and reaction chamber 2.
Wherein, in actual applications, described reaction chamber 2 is internal is provided with temperature sensor 16, and described temperature sensor 16 is connected and controls its duty with cooling pump 13, and described reaction chamber 2 bottom is provided with leakage fluid dram 14.
The above, it it is only preferred embodiment of the present utility model, not this utility model is made any pro forma restriction, although this utility model is disclosed above with preferred embodiment, but it is not limited to this utility model, any those skilled in the art, in the range of without departing from technical solutions of the utility model, when the technology contents of available the disclosure above makes a little change or is modified to the Equivalent embodiments of equivalent variations, in every case it is the content without departing from technical solutions of the utility model, any simple modification above example made according to technical spirit of the present utility model, equivalent variations and modification, all still fall within the range of technical solutions of the utility model.
Claims (6)
1. an Organometallic Chemistry apparatus for photoreaction, including reactant liquor container (1), reaction chamber (2), reacting metal (3), ultra-vioket radiation lamp (4) and cooling system, it is characterized in that, it is provided with Organometallic Chemistry reactant liquor in described reactant liquor container (1), reactant liquor container (1) is connected with reaction chamber (2) by tube for transfusion (9), in described reaction chamber (2), upper and lower both sides are respectively provided with a fixing seat (5), it is fixed with reacting metal (3) between fixing seat (5), described reaction chamber (2) left and right sides is symmetrically arranged with ultra-vioket radiation lamp (4), it is additionally provided with cooling system in described reaction chamber (2).
A kind of Organometallic Chemistry apparatus for photoreaction the most according to claim 1, it is characterized in that, described reactant liquor container (1) top is provided with feed(raw material)inlet (6), and bottom is provided with heated base (7), and reactant liquor container (1) bottom is provided with agitating device (8).
A kind of Organometallic Chemistry apparatus for photoreaction the most according to claim 1, it is characterized in that, described cooling system includes cooling liquid container (10) and cooling tube (11), described cooling liquid container (10) is built with coolant, and cooling tube (11) is centered around reacting metal (3) around in the shape of a spiral.
A kind of Organometallic Chemistry apparatus for photoreaction the most according to claim 1, it is characterised in that described tube for transfusion (9) middle part is provided with the reaction pump (12) of conveying reactant liquor, described cooling tube (11) middle part is provided with the cooling pump (13) of circulating cooling liquid.
A kind of Organometallic Chemistry apparatus for photoreaction the most according to claim 1, it is characterised in that set Packed transparent glass layer (15) between described ultra-vioket radiation lamp (4) and reaction chamber (2).
A kind of Organometallic Chemistry apparatus for photoreaction the most according to claim 1, it is characterized in that, described reaction chamber (2) is internal is provided with temperature sensor (16), described temperature sensor (16) is connected with cooling pump (13) and controls its duty, and described reaction chamber (2) bottom is provided with leakage fluid dram (14).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620432499.8U CN205599135U (en) | 2016-05-14 | 2016-05-14 | Metal organic chemistry light reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620432499.8U CN205599135U (en) | 2016-05-14 | 2016-05-14 | Metal organic chemistry light reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205599135U true CN205599135U (en) | 2016-09-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620432499.8U Expired - Fee Related CN205599135U (en) | 2016-05-14 | 2016-05-14 | Metal organic chemistry light reaction unit |
Country Status (1)
| Country | Link |
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| CN (1) | CN205599135U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI644724B (en) * | 2017-12-29 | 2018-12-21 | 國立清華大學 | Light reaction chemical processing system |
-
2016
- 2016-05-14 CN CN201620432499.8U patent/CN205599135U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI644724B (en) * | 2017-12-29 | 2018-12-21 | 國立清華大學 | Light reaction chemical processing system |
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160928 Termination date: 20170514 |
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| CF01 | Termination of patent right due to non-payment of annual fee |