CN201268596Y - Industrialized circulating photoreaction apparatus - Google Patents
Industrialized circulating photoreaction apparatus Download PDFInfo
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- CN201268596Y CN201268596Y CNU2008201600385U CN200820160038U CN201268596Y CN 201268596 Y CN201268596 Y CN 201268596Y CN U2008201600385 U CNU2008201600385 U CN U2008201600385U CN 200820160038 U CN200820160038 U CN 200820160038U CN 201268596 Y CN201268596 Y CN 201268596Y
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Abstract
The utility model relates to circulating light reaction equipment which can be industrially applied and comprises a reaction device, a reaction liquid circulating lighting device, and an air heating device. A reaction tank of the reaction device is provided with a feeding hole and a discharging hole, a reaction circulating liquid outlet and a reaction circulating liquid inlet, the reaction tank is connected with a serpentine coil by a circulating pump to form a loop of reaction liquid circularly receiving the lighting; an insulation sleeve of the reaction liquid circulating lighting device is arranged at the periphery of the serpentine coil, and the upper part and the lower part of the insulation sleeve are provided with connecting outlets which are connected with the air heating device to form a hot air circulating system. The utility model realizes the continuous batching feeding of materials participating in the light reaction, thereby solving the problem of the industrialization application of a light reactor, and being suitable for the industrial production like the precious-metal recovery, the chemosynthesis, and the like, and the treatment of noxious gases and other pollutants in the energy and environmental protection field.
Description
Technical field
The utility model relates to the light-catalyzed reaction technology, but particularly a kind of circulation light conversion unit of industrial applications.
Background technology:
Along with science and technology development, professional researchist finds that photoresponse not only can only be used to some extent in the organic chemistry organism is synthetic, and it can also be widely used in other chemical industry, the energy and environmental area.In today that global environmental pollution is extremely paid attention to, photoresponse can be degraded to the agricultural chemicals in the sewage, dyestuff the like waste, can also handle multiple obnoxious flavour, or is used for aspects such as precious metal recovery, health care.Present existing apparatus for photoreaction all is to adopt illumination to finish outside the glassware of placing response liquid basically, and reaction solution is that immobilized, rayed contact reacts liquid are uneven, also only is applicable to the reaction of trace or half middleweight.For this reason, the applicant proposed the patent application of a kind of " organic synthesis photoresponse laboratory apparatus " on September 5th, 2008.Technical scheme that this application proposes is the reaction solution in the reactor to be pumped into carry out rayed in the snake bend.Its major advantage is that the organic liquor that participates in reaction is accepted light-struck area increasing, and it is better to obtain light-struck uniformity coefficient, has improved speed of response, so that photoresponse efficient height.But because its reactor can only disposablely feed intake, thereby the industrial treatment that is applied to large batch of materials such as environmental pollution still is weak.
Summary of the invention
The utility model provides a kind of industrialization circulation light conversion unit, purpose be to realize to participate in photoresponse material continuously, fed batch, thereby solve the problem of the industrial applications of photoreactor.
Technical solution of the present utility model
The utility model mainly is made up of reaction unit, reaction solution circulation illumination apparatus, air heating apparatus.Wherein, the retort of reaction unit setting includes opening for feed and discharge port, the outlet of reaction cycle liquid and import, the outlet of retort circulation fluid is connected by the reaction solution import of recycle pump with the sinuous coil of reaction solution circulation illumination apparatus, and the outlet of the reaction solution of sinuous coil is connected with the circulation fluid import of retort, thereby constitutes the loop that illumination is accepted in the reaction solution circulation.
The beneficial effects of the utility model
(1) the utility model is applicable to that precious metal reclaims and the suitability for industrialized production of chemosynthesis etc., and in the energy and environmental protection field to the processing of pollutents such as poisonous, obnoxious flavour;
(2) the utility model is carried out measure control, temperature of reaction is detected in real time and fully improved the reactant illuminating area reaction mass, thereby has guaranteed reaction conditions, helps material light and urges carrying out smoothly of photoresponse;
(3) the utility model structure is comparatively simple, and equipment cost is lower.
Description of drawings
Accompanying drawing is a structural representation of the present utility model
Embodiment
As shown in the figure, the utility model is mainly by reaction unit, reaction solution circulation illumination apparatus, and air heating apparatus is formed, and described reaction unit 1 mainly comprises retort 11 and support 12 thereof.The retort top is provided with bottom and the top that opening for feed 13, bottom be provided with discharge port 14, side and is provided with reaction solution outlet 15 and import 16.Reaction solution circulation illumination apparatus 2 mainly comprises recycle pump 21, sinuous coil 22, light source 23, insulation sleeve 24 and anchor 25.The insulation sleeve is arranged on the periphery of sinuous coil, and light source uprightly is arranged on the central authorities of sinuous coil, and sinuous coil, light source, insulation sleeve all are fixed on the anchor with web member.Described light source 23 configurable multi-wavelengths' illumination lamp, or be luminescent lamp, or be high voltage mercury lamp or for tungsten lamp or be ultraviolet ray.Described insulation sleeve is arranged on the periphery of sinuous coil, and its upper and lower position is provided with the exit and is connected with included airheater 31, the air pump 33 of air heating apparatus 3 respectively, constitutes the recycle system of warm air.And be provided with draught damper 32 between airheater, the air pump.
In addition, the utility model is provided with liquid meter 26 between the reaction solution outlet of retort and recycle pump; The import and export of retort reaction solution and insulation telescopic interface up and down are equipped with temperatuer detector, and insulation sleeve lining coated has reflector layer, outer wall to be provided with asbestos thermal insulation layer (all not expressions among the figure).
Below in conjunction with accompanying drawing, sketch working process of the present utility model:
The utility model finishes by the above-mentioned requirements assembling, can come into operation.Open the opening for feed 13 of reaction tank deck, to desire reaction mass by working specification adds in the retort, add-on accounts for jar interior space about 1/2nd, open recycle pump 21, then reaction solution carries out circular flow to sinuous coil 22, the edge joint that flows on the sinuous coil limit is located at the irradiation of the illuminator 23 of sinuous coil central authorities, reaction solution obtains evenly and big area illumination: meanwhile, air pump 33 work of air heating apparatus, empty hot heater 31 is sent into warm air in the insulation sleeve, and hot air circulate is incubated the reaction solution in the sinuous coil.Can adopt the draught damper 32 of liquid meter 26 and air heating apparatus to control the flow of reaction solution and warm air respectively in the utility model working process; With the needed temperature condition of temperatuer detector monitoring reaction, to guarantee carrying out smoothly of material photoresponse.In addition can also be from discharge port 14 sample examinations of retort, whether assaying reaction is complete.When meeting the requirements, can material be emitted from discharge port.The utility model can constantly feed intake to retort with batch mode and carry out successive reaction, to satisfy the demand of industrial treatment material as required.
Claims (7)
1, industrialization circulation light conversion unit, comprise reaction unit (1), reaction solution circulation illumination apparatus (2), air heating apparatus (3), it is characterized in that: the retort (11) that described reaction unit is provided with includes opening for feed (13) and discharge port (14), reaction cycle liquid outlet (15) and import (16), the outlet of retort circulation fluid is connected by the reaction solution import of recycle pump (21) with reaction solution circulation illumination apparatus sinuous coil (22), and the outlet of the reaction solution of sinuous coil is connected with the circulation fluid import of retort, constitutes the loop that illumination is accepted in the reaction solution circulation.
2, industrialization circulation light conversion unit according to claim 1, it is characterized in that: described reaction unit 1 also comprises retort support (12).
3, industrialization circulation light conversion unit according to claim 1, it is characterized in that: described reaction solution circulation illumination apparatus (2) mainly comprises recycle pump (21), sinuous coil (22), light source (23), insulation sleeve (24) and anchor (25), the insulation sleeve is arranged on the periphery of sinuous coil, light source uprightly is arranged on the central authorities of sinuous coil, and sinuous coil, light source, insulation sleeve all are fixed on the anchor with web member.
4, industrialization circulation light conversion unit according to claim 3 is characterized in that: described light source 23 or for luminescent lamp, or be high voltage mercury lamp or for tungsten lamp or be UV-lamp.
5, industrialization circulation light conversion unit according to claim 3, it is characterized in that: the upper and lower position of described described insulation telescopic is provided with the exit and is connected with included airheater (31), the air pump (33) of air heating apparatus (3) respectively, be provided with draught damper 32 between airheater, the air pump, constitute the recycle system of warm air.
6, industrialization circulation light conversion unit according to claim 1 is characterized in that: be provided with liquid meter (26) between the reaction solution outlet of described retort and the recycle pump; The import and export place of retort reaction solution is equipped with temperatuer detector.
7, industrialization circulation light conversion unit according to claim 5 is characterized in that: described insulation telescopic inwall coated has reflector layer, outer wall to be provided with the asbestos thermal insulation layer, and interface is equipped with temperatuer detector up and down.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201600385U CN201268596Y (en) | 2008-09-25 | 2008-09-25 | Industrialized circulating photoreaction apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201600385U CN201268596Y (en) | 2008-09-25 | 2008-09-25 | Industrialized circulating photoreaction apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201268596Y true CN201268596Y (en) | 2009-07-08 |
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ID=40841190
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008201600385U Expired - Fee Related CN201268596Y (en) | 2008-09-25 | 2008-09-25 | Industrialized circulating photoreaction apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201268596Y (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102895932A (en) * | 2012-10-17 | 2013-01-30 | 联化科技股份有限公司 | Device for photo-catalytic bromination reaction |
| TWI644724B (en) * | 2017-12-29 | 2018-12-21 | 國立清華大學 | Light reaction chemical processing system |
| CN110102234A (en) * | 2019-06-21 | 2019-08-09 | 山东方明药业集团股份有限公司 | A kind of light reaction production equipment |
| CN112978846A (en) * | 2019-12-16 | 2021-06-18 | 中国科学院过程工程研究所 | Micro-droplet photoreaction device and method for industrial wastewater |
-
2008
- 2008-09-25 CN CNU2008201600385U patent/CN201268596Y/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102895932A (en) * | 2012-10-17 | 2013-01-30 | 联化科技股份有限公司 | Device for photo-catalytic bromination reaction |
| TWI644724B (en) * | 2017-12-29 | 2018-12-21 | 國立清華大學 | Light reaction chemical processing system |
| CN110102234A (en) * | 2019-06-21 | 2019-08-09 | 山东方明药业集团股份有限公司 | A kind of light reaction production equipment |
| CN112978846A (en) * | 2019-12-16 | 2021-06-18 | 中国科学院过程工程研究所 | Micro-droplet photoreaction device and method for industrial wastewater |
| CN112978846B (en) * | 2019-12-16 | 2023-11-03 | 中国科学院过程工程研究所 | Industrial wastewater micro-droplet photoreaction device and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090708 Termination date: 20100925 |