CN207153669U - A kind of organic silicon monomer synthetic reaction device - Google Patents
A kind of organic silicon monomer synthetic reaction device Download PDFInfo
- Publication number
- CN207153669U CN207153669U CN201720984615.1U CN201720984615U CN207153669U CN 207153669 U CN207153669 U CN 207153669U CN 201720984615 U CN201720984615 U CN 201720984615U CN 207153669 U CN207153669 U CN 207153669U
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- CN
- China
- Prior art keywords
- organic silicon
- silicon monomer
- tank
- storage tank
- monochloro methane
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
A kind of organic silicon monomer synthetic reaction device is the utility model is related to, wherein：Retort side is provided with silica flour storage tank, and top is connected by communicating pipe with monochloro methane synthesis tank, monochloro methane synthesis tank side is provided with hydrogen chloride storage tank, top is provided with methanol tank, retort opposite side is provided with copper chloride catalyst storage tank, and bottom is provided with second pressure controlling pump, the opposite side of monochloro methane synthesis tank is provided with zinc chloride catalyst storage tank, and bottom is provided with first pressure controlling pump.The equipment that the utility model design synthesizes dedicated for organic silicon monomer, it is ensured that the specific aim and technicality of organic silicon monomer synthesis, be advantageous to improve the combined coefficient and quality of organic silicon monomer, and device structure is simple, easily operated and maintenance.
Description
Technical field
Organosilicon production equipment technology is the utility model is related to, especially a kind of organic silicon monomer synthetic reaction dress
Put.
Background technology
Organic silicon monomer is the basic material for preparing silicone oil, silicon rubber, silicones and silane coupler, and application is very wide
It is general, and currently for the no special equipment of synthesis of organic silicon monomer, all it is to borrow other equipment to be synthesized, this not only can
The combined coefficient of organic silicon monomer is reduced, and the purity of organic silicon monomer, Shortcomings can be reduced.
The content of the invention
The purpose of this utility model is to provide a kind of organic silicon monomer synthetic reaction device, above-mentioned to overcome the shortcomings of, if
Count the equipment dedicated for organic silicon monomer synthesis, it is ensured that the specific aim and technicality of organic silicon monomer synthesis, be advantageous to carry
The combined coefficient and quality of high organic silicon monomer, and device structure is simple, it is easily operated with repairing.
The technical solution of the utility model：
A kind of organic silicon monomer synthetic reaction device, including retort, monochloro methane synthesis tank；Wherein：Retort side
Silica flour storage tank is provided with, and top is connected by communicating pipe with monochloro methane synthesis tank, monochloro methane synthesis tank side is provided with chlorine
Change hydrogen storage tank, top is provided with methanol tank.
A kind of organic silicon monomer synthetic reaction device, wherein：Retort opposite side is provided with copper chloride catalyst storage tank, and
Bottom is provided with second pressure controlling pump.
A kind of organic silicon monomer synthetic reaction device, wherein：The opposite side of monochloro methane synthesis tank is provided with zinc chloride and urged
Agent storage tank, and bottom is provided with first pressure controlling pump.
The utility model has the advantage of：The equipment that the utility model design synthesizes dedicated for organic silicon monomer, it is ensured that
The specific aim and technicality of organic silicon monomer synthesis, be advantageous to improve the combined coefficient and quality of organic silicon monomer, Er Qieshe
It is standby simple in construction, it is easily operated with repairing.
Brief description of the drawings
Fig. 1 is structure schematic diagram of the present utility model.
Reference：Retort 1, copper chloride catalyst storage tank 2, silica flour storage tank 3, communicating pipe 4, monochloro methane synthesis tank 5,
Hydrogen chloride storage tank 6, methanol tank 7, zinc chloride catalyst storage tank 8, first pressure controlling pump 9, second pressure controlling pump 10.
Embodiment
Embodiment 1, referring to Fig. 1, a kind of organic silicon monomer synthetic reaction device, including retort 1, monochloro methane synthesis
Tank 5；Wherein：The side of retort 1 is provided with silica flour storage tank 3, and top is connected by communicating pipe 4 with monochloro methane synthesis tank 5, and one
The side of chloromethanes synthesis tank 5 is provided with hydrogen chloride storage tank 6, and top is provided with methanol tank 7, designs and is closed dedicated for organic silicon monomer
Into equipment, it is ensured that organic silicon monomer synthesis specific aim and technicality, be advantageous to improve organic silicon monomer combined coefficient
With quality, and device structure is simple, easily operated with maintenance.
Embodiment 2, referring to Fig. 1, a kind of organic silicon monomer synthetic reaction device, wherein：The opposite side of retort 1 is provided with
Copper chloride catalyst storage tank 2, and bottom is provided with second pressure controlling pump 10, is easy to be controlled the pressure in retort 1,
It is easy to the synthesis to organic silicon monomer to be catalyzed simultaneously.Remaining is the same as embodiment 1.
Embodiment 3, referring to Fig. 1, a kind of organic silicon monomer synthetic reaction device, wherein：Monochloro methane synthesis tank 5 it is another
Side is provided with zinc chloride catalyst storage tank 8, and bottom is provided with first pressure controlling pump 9, is easy to monochloro methane synthesis tank 5
Interior pressure is controlled, while is easy to the synthesis to monochloro methane to be catalyzed.Remaining is the same as embodiment 1.
Operation principle：
In reaction, hydrogen chloride is entered in monochloro methane synthesis tank 5 from hydrogen chloride storage tank 6, and methanol enters from methanol tank 7
Entering into monochloro methane synthesis tank 5, zinc chloride catalyst is entered in monochloro methane synthesis tank 5 from zinc chloride catalyst storage tank 8,
Meanwhile it is 0.4MPa that first pressure controlling pump 9, which controls the pressure in monochloro methane synthesis tank 5, and then reaction condition, finally
Generate monochloro methane, the monochloro methane after synthesis entered in retort 1 from communicating pipe 4, at the same time, copper chloride catalyst with
Silica flour is entered in retort 1 from copper chloride catalyst storage tank 2 and silica flour storage tank 3 respectively, meanwhile, second pressure controlling pump 10 is controlled
Pressure in retort 1 processed is 0.2-0.3MPa, reaches reaction condition, ultimately generates organic silicon monomer, finally, to retort 1
Interior organic silicon monomer can obtain organic silicon monomer after carrying out separating-purifying.
Claims (3)
1. a kind of organic silicon monomer synthetic reaction device, including retort (1), monochloro methane synthesis tank (5)；It is characterized in that：
Retort (1) side is provided with silica flour storage tank (3), and top is connected by communicating pipe (4) with monochloro methane synthesis tank (5), and one
Chloromethanes synthesis tank (5) side is provided with hydrogen chloride storage tank (6), and top is provided with methanol tank (7).
A kind of 2. organic silicon monomer synthetic reaction device according to claim 1, it is characterised in that：Retort (1) is another
Side is provided with copper chloride catalyst storage tank (2), and bottom is provided with second pressure controlling pump (10).
A kind of 3. organic silicon monomer synthetic reaction device according to claim 1, it is characterised in that：Monochloro methane synthesis tank
(5) opposite side is provided with zinc chloride catalyst storage tank (8), and bottom is provided with first pressure controlling pump (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720984615.1U CN207153669U (en) | 2017-08-08 | 2017-08-08 | A kind of organic silicon monomer synthetic reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720984615.1U CN207153669U (en) | 2017-08-08 | 2017-08-08 | A kind of organic silicon monomer synthetic reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207153669U true CN207153669U (en) | 2018-03-30 |
Family
ID=61715550
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720984615.1U Expired - Fee Related CN207153669U (en) | 2017-08-08 | 2017-08-08 | A kind of organic silicon monomer synthetic reaction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207153669U (en) |
-
2017
- 2017-08-08 CN CN201720984615.1U patent/CN207153669U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180330 Termination date: 20180808 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |