CN205164701U - A reation kettle for producing silane have a separator - Google Patents
A reation kettle for producing silane have a separator Download PDFInfo
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- CN205164701U CN205164701U CN201520983728.0U CN201520983728U CN205164701U CN 205164701 U CN205164701 U CN 205164701U CN 201520983728 U CN201520983728 U CN 201520983728U CN 205164701 U CN205164701 U CN 205164701U
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- tower
- separator
- reactor
- kettle
- overhead condenser
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Abstract
The utility model relates to a reation kettle for producing silane have a separator. Include: the cauldron body, a cauldron body top and a separator's bottom links to each other, separator's bottom is provided with the tower section, separator's upper portion is provided with the overhead condenser, separator's top is provided with the top of the tower evacuation, be in the tower between overhead condenser and the tower section, the tower is middle and upper to be provided with circulating inlet in feed inlet in the tower, material receiving port and the tower, it is continuous with the bottom of the cauldron body that circulating inlet passes through the circulating pump. Therefore, the utility model has the advantages of as follows: (1 )This reation kettle can make the gas -liquid intensive mixing, and the reaction rate is fast, is favorable to temperature control, (2 )This reation kettle gas -liquid dispersion is better, the circulating pump equilibrium that operates steadily, the extension of equipment life, (3 )Can realize that the reation kettle and the reaction that combines of splitter separate integrated device, have reduced the equipment investment.
Description
Technical field
The utility model relates to a kind of reactor with separator for the production of silane, belongs to chemical materials production equipment field.
Background technology
In the production of silane, reactor is absolutely necessary instrument.Namely the broad understanding of reactor has the container of physics or chemical reaction, by the structural design of container and parameter configuration, realizes the mixing of technological requirement, heating, response function.Reaction liquid mixes in reactor fully with gas reactant, reaction
In usual reactor, gas liquid reaction adopts bubbling method to carry out, and gas-liquid contact is insufficient, and reaction rate is not high, and utilization rate of equipment and installations is very low.And the factors such as in Conventional process, powder feeding mode also can produce powder wall built-up, liquid backflow, cleaning difficulty is large, powder pollution operating environment is severe cause in production process, and powder consumption is large, production efficiency is low and produce respirable dust pollution to problems such as health damage.
In addition, after material in reactor has reacted under normal circumstances, terminate as a reaction member, reaction mass need be squeezed into other separation equipments and be separated, and equipment is more, and utilization rate of equipment and installations is very low.
Utility model content
The utility model mainly solves the above-mentioned technical problem existing for prior art, provides a kind of reactor with separator for the production of silane.This reactor can make gas-liquid fully mix, and reaction speed is fast, and be conducive to temperature and control, and equipment leak point is few, is conducive to environmental protection, Gas-Liquid Dispersion is better, and pump operating cycle is steadily balanced, and service life of equipment extends; In addition, also can reduce the residual material in powdered pipe, be convenient to cleaning; And can effectively reduce dust to fly away, ensure safety of employees.
Above-mentioned technical problem of the present utility model is mainly solved by following technical proposals:
A kind of reactor with separator for the production of silane, comprise kettle, described kettle top is connected with the bottom of a separator, the bottom of described separator is provided with tower joint, the top of described separator is provided with overhead condenser, it is emptying that the top of described separator is provided with tower top, be in tower between described overhead condenser and Ta Jie, be provided with loop head in charging aperture in tower, material receiving port and tower in described tower, described loop head is connected with the bottom of kettle by circulating pump.
Optimize, above-mentioned a kind of reactor with separator for the production of silane, described overhead condenser comprises overhead condenser cooling water inlet and overhead condenser coolant outlet.
Optimize, above-mentioned a kind of reactor with separator for the production of silane, is provided with tower mesoscope in described tower.
Optimize, above-mentioned a kind of reactor with separator for the production of silane, the both sides, top of described kettle are respectively arranged with tower reactor charge door and tower reactor visor, the bottom of described kettle is provided with reacting kettle jacketing, described reacting kettle jacketing is respectively arranged with heat ingress and condensed water discharge outlet.
Optimize, above-mentioned a kind of reactor with separator for the production of silane, the bottom of described kettle is provided with slag-drip opening.
Therefore, the utility model tool has the following advantages: (1) this reactor can make gas-liquid fully mix, and reaction speed is fast, is conducive to temperature and controls; (2) this reactor Gas-Liquid Dispersion is better, and pump operating cycle is steadily balanced, and service life of equipment extends; (3) can the combination integrated reaction and separation device of realization response still and separation equipment, decrease equipment investment, saved energy consumption, effectively improve utilization rate of equipment and installations.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Below by embodiment, and by reference to the accompanying drawings, the technical solution of the utility model is described in further detail.
In figure, loop head 9 in charging aperture 1, tower reactor charge door 2, tower reactor visor 3, heat ingress 4, slag-drip opening 5, condensed water discharge outlet 6, circulating pump 7, tower mesoscope 8, tower in tower, overhead condenser cooling water inlet 10, overhead condenser coolant outlet 11, material receiving port 12, tower top are emptying 13, autoclave body bottom outlet 14, tower joint 15, overhead condenser 16.
Embodiment:
As shown in Figure 1, a kind of reactor with separator for the production of silane, comprise kettle, kettle top is connected with the bottom of a separator, the bottom of separator is provided with tower joint 15, the top of separator is provided with overhead condenser 16, the top of separator is provided with tower top emptying 13, be in tower between overhead condenser 16 and Ta Jie 15, be provided with loop head 9 in charging aperture 1 in tower, material receiving port 12 and tower in tower, loop head 9 is connected with the bottom of kettle by circulating pump 7.Overhead condenser 16 comprises overhead condenser cooling water inlet 10 and overhead condenser coolant outlet 11.Tower mesoscope 8 is provided with in tower.
In the present embodiment, the both sides, top of kettle are respectively arranged with tower reactor charge door 2 and tower reactor visor 3, and the bottom of kettle is provided with reacting kettle jacketing, reacting kettle jacketing are respectively arranged with heat ingress 4 and condensed water discharge outlet 6, and the bottom of kettle is provided with slag-drip opening 5.
After adopting said structure, material is through circulating pump, and enter reactor Ta Jienei, gas-liquid fully contacts, and material is fast reaction in tower.
In the present embodiment, direct-connected reaction tower joint 15 on reactor, tower joint diameter 300mm-1000mm.∮ 25--∮ 50 Pall ring is filled in tower.In the present embodiment, condenser can select pipe bundle condenser, enamel chip type condenser.
Known from the above description, the present embodiment has following advantage:
(1) this reactor can make gas-liquid fully mix, and reaction speed is fast, is conducive to temperature and controls; (2) this reactor Gas-Liquid Dispersion is better, and pump operating cycle is steadily balanced, and service life of equipment extends; (3) can the combination integrated reaction and separation device of realization response still and separation equipment, decrease equipment investment, saved energy consumption, effectively improve utilization rate of equipment and installations.
Specific embodiment described herein is only to the explanation for example of the utility model spirit.The utility model person of ordinary skill in the field can make various amendment or supplements or adopt similar mode to substitute to described specific embodiment, but can't depart from spirit of the present utility model or surmount the scope that appended claims defines.
Although more employ the terms such as loop head 9 in kettle, tower reactor charge door 2, tower reactor visor 3, heat ingress 4, slag-drip opening 5, condensed water discharge outlet 6, circulating pump 7, tower mesoscope 8, tower, overhead condenser cooling water inlet 10, overhead condenser coolant outlet 11, material receiving port 12, tower top are emptying 13, autoclave body bottom outlet 14, tower joint 15, overhead condenser 16 herein, do not get rid of the possibility using other term.These terms are used to be only used to describe and explain essence of the present utility model more easily; The restriction that they are construed to any one additional is all contrary with the utility model spirit.
Claims (5)
1. the reactor with separator for the production of silane, comprise kettle, it is characterized in that, described kettle top is connected with the bottom of a separator, the bottom of described separator is provided with tower joint (15), the top of described separator is provided with overhead condenser (16), the top of described separator is provided with tower top emptying (13), be in tower between described overhead condenser (16) and tower joint (15), charging aperture in tower (1) is provided with in described tower, loop head (9) in material receiving port (12) and tower, described loop head (9) is connected with the bottom of kettle by circulating pump (7).
2. a kind of reactor with separator for the production of silane according to claim 1, it is characterized in that, described overhead condenser (16) comprises overhead condenser cooling water inlet (10) and overhead condenser coolant outlet (11).
3. a kind of reactor with separator for the production of silane according to claim 1, is characterized in that, be provided with tower mesoscope (8) in described tower.
4. a kind of reactor with separator for the production of silane according to claim 1, it is characterized in that, the both sides, top of described kettle are respectively arranged with tower reactor charge door (2) and tower reactor visor (3), the bottom of described kettle is provided with reacting kettle jacketing, described reacting kettle jacketing is respectively arranged with heat ingress (4) and condensed water discharge outlet (6).
5. a kind of reactor with separator for the production of silane according to claim 1, is characterized in that, the bottom of described kettle is provided with slag-drip opening (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520983728.0U CN205164701U (en) | 2015-12-01 | 2015-12-01 | A reation kettle for producing silane have a separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520983728.0U CN205164701U (en) | 2015-12-01 | 2015-12-01 | A reation kettle for producing silane have a separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205164701U true CN205164701U (en) | 2016-04-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520983728.0U Expired - Fee Related CN205164701U (en) | 2015-12-01 | 2015-12-01 | A reation kettle for producing silane have a separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205164701U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110252212A (en) * | 2019-07-29 | 2019-09-20 | 河南久圣化工有限公司 | A kind of continuous esterification process units of mixed dibasic acid dimethyl ester |
-
2015
- 2015-12-01 CN CN201520983728.0U patent/CN205164701U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110252212A (en) * | 2019-07-29 | 2019-09-20 | 河南久圣化工有限公司 | A kind of continuous esterification process units of mixed dibasic acid dimethyl ester |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160420 Termination date: 20181201 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |