CN203598801U - Self-circulation chemical synthesis reactor with single-stroke compression function - Google Patents
Self-circulation chemical synthesis reactor with single-stroke compression function Download PDFInfo
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- CN203598801U CN203598801U CN201320827695.1U CN201320827695U CN203598801U CN 203598801 U CN203598801 U CN 203598801U CN 201320827695 U CN201320827695 U CN 201320827695U CN 203598801 U CN203598801 U CN 203598801U
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The utility model discloses a self-circulation chemical synthesis reactor with a single-stroke compression function, and relates to a chemical synthesis reactor. The self-circulation chemical synthesis reactor mainly comprises a reaction chamber, an upper air chamber, a descending channel, a lower air chamber, a cooling water jacket, a cooling rib plate and a housing, wherein the cooling water jacket surrounds the outer side of a housing body on the middle section of the housing, and consists of a space between an outer wall and the outer side of the housing body on the middle section of the housing; the cooling rib plate is closely connected to the inner side of the housing body on the middle section of the housing; the descending channel consists of a space between a housing body on the inner side of the middle section of the housing and a wall body of the reaction chamber; the upper air chamber is above the reaction chamber; the lower air chamber is below the reaction chamber; the upper air chamber consists of an inner space defined by an upper end and a housing body on the upper section of the housing; the lower air chamber consists of an inner space defined by a lower end and a housing body on the lower section of the housing; the reaction chamber is communicated to the upper air chamber; the upper air chamber is communicated to the lower air chamber through the descending channel. According to the self-circulation chemical synthesis reactor, raw material gas can be all synthesized into a target product through single-stroke compression only, so that the electric consumption is greatly reduced, the catalytic efficiency is greatly improved, and the purposes of energy conservation and emission reduction are achieved in a chemical synthesis process.
Description
Technical field
The utility model relates to a kind of chemical industry equipment, specially refers to a kind of chemosynthesis reaction device.
Background technology
Under the condition existing at catalyst, most of chemosynthesis reactions are all reversible reactions, when target product reaches after finite concentration, will be in balance, and reaction will no longer be carried out to the direction of synthetic target product.People are carrying out in the production process of combination reaction, in order to make reaction can continue to carry out to target product direction, must make mix products export from synthesis reactor and fill into new raw material gas in synthesis reactor, target product concentration in synthesis reactor is reduced, after destruction of balance, make combination reaction proceed, after mix products is exported from synthesis reactor, by separation equipment, unreacting gas is separated, again unreacting gas is returned and in synthesis reactor, carries out circular response, because one way catalytic rate is only in 20% left and right, unstripped gas must be by being reacted into target product after the compression that repeatedly circulates in synthesis reactor, and each circulation compression all needs to consume very large compression energy consumption.
In existing synthesis reactor, under the synthetic condition of applications catalyst, the operating pressure of synthetic ammonia is more than 8MPa, the operating pressure of synthesizing methanol is between 3～15MPa, the operating pressure of direct synthesis of dimethyl ether from synthesis gas is between 2～5MPa, obtain above-mentioned operating pressure, must take multi-stage compression to realize, compression energy consumption is very large, therefore, existing synthesis reactor must repeatedly circulate and unstripped gas could be synthesized to the production process of target product with multi-stage compression, has the shortcoming that power consumption is large.
Summary of the invention
The purpose of this utility model is will overcome existing chemical synthesis equipment unstripped gas need be carried out to the large shortcoming of iterative cycles compression power consumption, design a kind of chemosynthesis reaction device that is carried out automatic cycle catalysis by synthesis reactor oneself in inside, make unstripped gas only need compress and just can all synthesize target product by one way, significantly to reduce power consumption and to improve catalytic efficiency, realize energy-saving and emission-reduction in the production of synthetic ammonia, methyl alcohol, dimethyl ether and in other need carry out the production process of chemical synthesis.
The self-loopa chemosynthesis reaction device of a kind of one way compression of the present utility model, it is characterized in that reactor is mainly by reative cell (IV), upper chamber (VII), decline passway (V), lower chamber (III), cooling jacket (VI), cooling floor (25) and shell (9) composition, wherein, reative cell (IV), upper chamber (VII), decline passway (V) and lower chamber (III) are arranged in the interior space of shell (9), cooling jacket (VI) is looped around the hull outside in shell (9) stage casing, cooling jacket (VI) is made up of the space between outer wall (11) and shell (9) middle housing outside, cooling floor (25) is closely connected on the housing inner side in shell (9) stage casing, decline passway (V) is made up of the space between interior side body and the reative cell wall body (7) in shell (9) stage casing, upper chamber (VII) is in the top of reative cell (IV), the below of reative cell (IV) is lower chamber (III), the interior space that upper chamber (VII) is surrounded by upper end (3) and shell (9) upper casing forms, the interior space that lower chamber (III) is surrounded by lower end (16) and the lower piece housing of shell (9) forms, reative cell (IV) is communicated to upper chamber (VII), and upper chamber (VII) is communicated to lower chamber (III) by decline passway (V), reative cell wall body (7) is made up of cylinder sidewall and circular arc bottom, reative cell wall body (7) is connected on the housing of shell (9) by upper supporting piece (4) and lower support element (23), has circulating air input port (24) access and catalyst discharging outlet (12) to pick out in lower sidewall or the circular arc bottom of reative cell wall body (7), the heat-absorbent surface of cooling floor (25) is arranged in decline passway (V), lower chamber (III) has raw material tonifying Qi interface (21) access, lower chamber (III) is communicated to the bottom of reative cell (IV) by circulating air input port (24), the bottom of lower chamber (III) is liquid collecting zone (I), and the bottom of liquid collecting zone (I) has product outlet (17) to pick out.
In the utility model, cooling floor (25) is multi-disc setting, and the heat-absorbent surface of the cooling floor of multi-disc (25) is to be arranged on around mode in decline passway (V); Half partition-type structures that circulating air input port (24) is multi-through hole; Heat insulation layer (8) is installed on the lateral wall of reative cell wall body (7); At the bottom having heaters (10) of reative cell (IV), heater (10) is electric heater and heat exchanger one wherein; On the circulating air input port (24) of reative cell, there is circulating air communicating pipe (14), gas skirt (20) is set in lower chamber (III), the top of gas skirt (20) is connected on the input port of circulating air communicating pipe (14), the interior space of gas skirt (20) forms collection chamber (II), and collection chamber (II) is communicated to reative cell (IV) by circulating air communicating pipe (14); In lower chamber (III), have gas-liquid separator (15), gas-liquid separator (15) comprises louvre type separator, coil pipe cooling separator and surface cooler formula separator; On the top of upper end (3), have catalyst charging hole (VIII), catalyst charging hole (VIII) seals by top cover (1), between top cover (1) and upper end (3) joint face, has sealing ring a(2); Upper end (3) is disk structure, and upper end (3) is arranged on the upper port of shell (9), between upper end (3) and the joint face of shell (9) upper port, has sealing ring b(26); Lower end (16) is circular arc bottom structure, and lower end (16) is arranged on the lower port of shell (9), between the lower port of shell (9) and the joint face of lower end (16), has sealing ring c(19).
In above-mentioned utility model, because reative cell (IV), upper chamber (VII), decline passway (V) and lower chamber (III) coexist in the space of shell (9), and reative cell (IV) is directly communicated to, and upper chamber (VII), upper chamber (VII) are directly communicated to decline passway (V), decline passway (V) is directly communicated to lower chamber (III), therefore, chemosynthesis reaction device is under equal pressure condition, to carry out self-loopa catalytic synthesis, make the wall body (7) of reative cell (IV) not bear pressure, can greatly reduce the material usage of wall body (7).
Above-mentioned utility model in the specific implementation, cooling water inlet (22) is connected on the feed pipe of cooling system, coolant outlet (5) is connected on the return pipe of cooling system, in reative cell (IV), catalyst is set simultaneously, the catalyst according to target requirement of product is selected and is activated, then in combination reaction device, input unstripped gas, unstripped gas is entered in reative cell (IV), in reative cell (IV), just carry out chemosynthesis reaction, generate target product, in the time that unstripped gas carries out chemosynthesis reaction, can produce heat, the reaction heat generating can make to heat up in reative cell (IV), thereby unreacting gas and gaseous state target product in reative cell (IV) are heated up, the density of the gaseous mixture of unreacting gas and the mixing of gaseous state target product is diminished, according to gravity circulation theory, gaseous mixture after intensification can carry out ascending motion, enter into upper chamber (VII), simultaneously, decline passway (V) is subject to the cooling effect of shell (9) middle housing and cooling floor (25), make unreacting gas or gaseous mixture in decline passway (V) be subject to cooling, temperature declines, the density of unreacting gas or gaseous mixture is increased, according to gravity circulation theory, unreacting gas after cooling or gaseous mixture can carry out descending motion, enter into lower chamber (III), gaseous mixture in lower chamber (III) after gas-liquid separator (15) separates, be separated into liquid target product and the unreacting gas of gaseous state, liquid target product exports (17) by product and product efferent duct (18) output enters product storage tank, unreacting gas enters reative cell (IV) by circulating air communicating pipe (14) by circulating air input port (24) and carries out circular response, the unstripped gas that synthetic target product consumes supplements by raw material tonifying Qi interface (21), so go round and begin again, by chemosynthesis reaction device oneself, in inside, isobaric condition forms automatic cycle, and isolate in time target product, make target product concentration in combination reaction device all the time lower than equalization point, make combination reaction can continue to carry out.The utility model makes unstripped gas only need be compressed and just can all be synthesized target product by one way, and do not need a mixture output-response device to separate outward, overcome unstripped gas and need carry out the large shortcoming of iterative cycles compression power consumption, improved catalytic efficiency, realized energy-saving and emission-reduction.
In above-mentioned utility model, in the outer space in shell (9) stage casing of chemosynthesis reaction device, cooling jacket (VI) is set and cooling floor (25) is set in decline passway (V), make gaseous mixture fast cooling and carry out descending motion, automatically produce downward gravitation, thereby make space between reative cell wall body (7) and shell (9) be subject to cooling effect and form the decline passway (V) of gaseous mixture, gaseous mixture in upper chamber (VII) is incorporated in lower chamber (III), in lower chamber (III), gaseous mixture is separated again, isolated unreacting gas supplements in reative cell (IV) in time by circulating air input port (24), the gaseous mixture heating up in driving a reaction chamber (IV) accelerates ascending motion, the gaseous mixture that accelerates ascending motion in reative cell (IV) makes the gaseous mixture in decline passway (V) accelerate descending motion by ringing again, thus, constantly produce circulation power in inside by chemosynthesis reaction device oneself.The utility model takes to arrange the measure of cooling floor (25) in decline passway (V), than adopting cooling tube bundle or cooling coil structure more simply, more to save material.
In above-mentioned utility model, the effect that heater (10) is set in the bottom of reative cell (IV) is to carry out auxiliary heating for reative cell (IV), initial generation in equipment investment operation is applicable to the synthetic room temperature of target product, in the time that normally moving, equipment carries out the adjusting of operating temperature, meanwhile, play the effect that makes unstripped gas accelerate circulation catalysis.Described heater (10) is electric heater or heat exchanger, selects existing products in markets.
In above-mentioned utility model, gas skirt (20) is set in lower chamber (III) and on circulating air input port (24), has circulating air communicating pipe (14), the top of gas skirt (20) is connected on the input port of circulating air communicating pipe (14), its effect is that unreacting gas is assembled at gas skirt (20), make the interior space of gas skirt (20) form collection chamber (II), make heavy target product enter the top less than gas skirt (20), thereby prevent that the gaseous state target product in lower chamber (III) from feeding back in reative cell (IV) by circulating air input port (24), be conducive to improve the catalytic efficiency in reative cell (IV).
In above-mentioned utility model, gas-liquid separator (15) is set in lower chamber (III), its objective is that a target product separates in time, reduce the target product concentration in combination reaction device, combination reaction is carried out to favourable direction, make unstripped gas accelerate synthetic target product, improve catalytic efficiency.Described gas-liquid separator (15) comprises louvre type separator, coil pipe cooling separator and surface cooler formula separator, in the time using louvre type separator, carry out gas-liquid separation with collision separate mode, when aerosol particle in mixture runs into louver plate washer in flow process, mutually condense agglomerating and form liquid target product through collision; In the time using coil pipe cooling separator and surface cooler formula separator, carry out gas-liquid separation in condensation separation mode, in the time that the surface temperature of coil pipe or surface cooler drops to below the evaporating temperature of target product, just make the target product of gaseous state condense in the surface of coil pipe or surface cooler and isolate liquid product, or in the time that the room temperature of lower chamber (III) is reduced to below the evaporating temperature of target product, the target product of gaseous state is just condensed into liquid target product, reaches separation object.
In above-mentioned utility model, circulating air input port (24) is designed to half partition-type structures of multi-through hole, catalyst in reative cell (IV) can not leaked by circulating air input port (24), and half partition-type structures of multi-through hole can not hinder unreacting gas and enter in reative cell (IV).
In above-mentioned utility model, the object that heat insulation layer (8) is installed on the lateral wall of the wall body (7) of reative cell is to make reaction heat in reative cell (IV) can not have influence on the cooling effect of decline passway (V), also make the cooling effect of decline passway (V) can not have influence on the thermogenic action in reative cell (IV), thereby guarantee the temperature that keeps chemical reaction to need in reative cell (IV) simultaneously.
The beneficial effects of the utility model are: the self-loopa chemosynthesis reaction device of a kind of one way compression of design, and adopt cooling floor (25) as the cooling device in decline passway, make synthesis reactor inner structure simpler; When production, make unstripped gas only need compress and just can all synthesize target product by one way, significantly to reduce power consumption and to improve catalytic efficiency, in the production process of chemical synthesis, realize energy-saving and emission-reduction.Compared with routine techniques, the utility model has overcome conventional chemical synthesis equipment need carry out the large shortcoming of iterative cycles compression power consumption unstripped gas.The utility model can be applied on the production line of the chemical synthesis products such as methyl alcohol, dimethyl ether, synthetic ammonia.
Accompanying drawing explanation
Fig. 1 is the structure chart of a kind of self-loopa chemosynthesis reaction device of the present utility model.
Fig. 2 is the A-A profile of Fig. 1.
In figure: 1. top cover, 2. sealing ring a, 3. upper end, 4. upper supporting piece, 5. coolant outlet, 6. temperature sensor, 7. reative cell wall body, 8. heat insulation layer, 9. shell, 10. heater, the outer wall of 11. cooling jackets, 12. catalyst discharging outlets, 13. catalyst discharge ducts, 14. circulating air communicating pipes, 15. gas-liquid separators, 16. lower ends, 17. product outlets, 18. product efferent ducts, 19. sealing ring c, 20. gas skirts, 21. raw material tonifying Qi interfaces, 22. cooling water inlets, 23. lower support elements, 24. circulating air input ports, 25. cooling floors, 26. sealing ring b, I. liquid collecting zone, II. collection chamber, III. lower chamber, IV. reative cell, V. decline passway, VI. cooling jacket, VII. upper chamber, VIII. catalyst charging hole.
The specific embodiment
In embodiment shown in Fig. 1, the self-loopa chemosynthesis reaction device of one way compression is mainly by reative cell (IV), upper chamber (VII), decline passway (V), lower chamber (III), cooling jacket (VI), cooling floor (25) and shell (9) composition, wherein, reative cell (IV), upper chamber (VII), decline passway (V) and lower chamber (III) are arranged in the interior space of shell (9), cooling jacket (VI) is looped around the hull outside in shell (9) stage casing, cooling jacket (VI) is made up of the space between outer wall (11) and shell (9) middle housing outside, cooling floor (25) is closely connected on the housing inner side in shell (9) stage casing, decline passway (V) is made up of the space between interior side body and the reative cell wall body (7) in shell (9) stage casing, upper chamber (VII) is in the top of reative cell (IV), the below of reative cell (IV) is lower chamber (III), the interior space that upper chamber (VII) is surrounded by upper end (3) and shell (9) upper casing forms, the interior space that lower chamber (III) is surrounded by lower end (16) and the lower piece housing of shell (9) forms, reative cell (IV) is communicated to upper chamber (VII), and upper chamber (VII) is communicated to lower chamber (III) by decline passway (V), reative cell wall body (7) is made up of cylinder sidewall and circular arc bottom, reative cell wall body (7) is connected on the housing of shell (9) by upper supporting piece (4) and lower support element (23), has circulating air input port (24) access and catalyst discharging outlet (12) to pick out in lower sidewall or the circular arc bottom of reative cell wall body (7), the heat-absorbent surface of cooling floor (25) is arranged in decline passway (V), lower chamber (III) has raw material tonifying Qi interface (21) access, lower chamber (III) is communicated to the bottom of reative cell (IV) by circulating air input port (24), the bottom of lower chamber (III) is liquid collecting zone (I), and the bottom of liquid collecting zone (I) has product outlet (17) to pick out.In the present embodiment, cooling floor (25) is set to 24, and the heat-absorbent surface of 24 cooling floors (25) is to be arranged on around mode in decline passway (V); Half partition-type structures that circulating air input port (24) is multi-through hole; Heat insulation layer (8) is installed on the lateral wall of reative cell wall body (7); At the bottom having heaters (10) of reative cell (IV), heater (10) is electric heater, selects commercially available prod; On the circulating air input port (24) of reative cell, there is circulating air communicating pipe (14), gas skirt (20) is set in lower chamber (III), the top of gas skirt (20) is connected on the input port of circulating air communicating pipe (14), the interior space of gas skirt (20) forms collection chamber (II), and collection chamber (II) is communicated to reative cell (IV) by circulating air communicating pipe (14); In lower chamber (III), have gas-liquid separator (15), gas-liquid separator (15) is surface cooler formula separator, selects commercially available prod; On the top of upper end (3), have catalyst charging hole (VIII), catalyst charging hole (VIII) seals by top cover (1), between top cover (1) and upper end (3) joint face, has sealing ring a(2); Upper end (3) is disk structure, and upper end (3) is arranged on the upper port of shell (9), between upper end (3) and the joint face of shell (9) upper port, has sealing ring b(26); Lower end (16) is circular arc bottom structure, and lower end (16) is arranged on the lower port of shell (9), between the lower port of shell (9) and the joint face of lower end (16), has sealing ring c(19); In upper chamber (VII), there is temperature sensor (6).
When the present embodiment is applied on producing, cooling water inlet (22) is connected on the feed pipe of cooling system, coolant outlet (5) is connected on the return pipe of cooling system, in reative cell (IV), catalyst is set simultaneously, the catalyst according to target requirement of product is selected and is activated, then in combination reaction device, input unstripped gas, unstripped gas is entered in reative cell (IV), in reative cell (IV), just carry out chemosynthesis reaction, generate target product, in the time that unstripped gas carries out chemosynthesis reaction, can produce heat, the reaction heat generating can make to heat up in reative cell (IV), thereby unreacting gas and gaseous state target product in reative cell (IV) are heated up, the density of the gaseous mixture of unreacting gas and the mixing of gaseous state target product is diminished, according to gravity circulation theory, gaseous mixture after intensification can carry out ascending motion, enter into upper chamber (VII), simultaneously, decline passway (V) is subject to the cooling effect of shell (9) middle housing and cooling floor (25), make unreacting gas or gaseous mixture in decline passway (V) be subject to cooling, temperature declines, the density of unreacting gas or gaseous mixture is increased, according to gravity circulation theory, unreacting gas after cooling or gaseous mixture can carry out descending motion, enter into lower chamber (III), gaseous mixture in lower chamber (III) after gas-liquid separator (15) separates, be separated into liquid target product and the unreacting gas of gaseous state, liquid target product exports (17) by product and product efferent duct (18) output enters product storage tank, unreacting gas enters reative cell (IV) by circulating air communicating pipe (14) by circulating air input port (24) and carries out circular response, the unstripped gas that synthetic target product consumes supplements by raw material tonifying Qi interface (21), so go round and begin again, by chemosynthesis reaction device oneself, in inside, isobaric condition forms automatic cycle, and isolate in time target product, make target product concentration in combination reaction device all the time lower than equalization point, make combination reaction can continue to carry out.The utility model makes unstripped gas only need be compressed and just can all be synthesized target product by one way, and do not need a mixture output-response device to separate outward, overcome unstripped gas and need carry out the large shortcoming of iterative cycles compression power consumption, improved catalytic efficiency, realized energy-saving and emission-reduction.In process of production, obtain the temperature in reative cell (IV) by temperature sensor (6), then move by operate heater (10) or stop controlling the temperature in reative cell (IV), make it to meet the temperature requirement of chemical synthesis.
On the production line of the above embodiments as methyl alcohol, dimethyl ether, synthetic ammonia or other chemical synthesis product, apply.In the time applying as synthesizing methanol equipment, arrange with 48% CuO, 46% ZnO and 5% Al at reative cell (IV)
2o
3for the pellet type catalyst of component, then the H of the CO of a volume and two volumes
2after mixing, be input in combination reaction device as unstripped gas, carry out synthesizing methanol production, the reaction equation that unstripped gas synthesizes methyl alcohol is CO+2H
2→ CH
3oH+102.5kj; In the time applying as one-step method dimethyl ether synthesis equipment, arrange with 48% CuO, 46% ZnO and 5% Al at reative cell (IV)
2o
3for the pellet type catalyst of component, then add and fill out ZSM-5 molecular sieve, then the H of the CO of a volume and two volumes
2after mixing, be input in combination reaction device as unstripped gas, carry out dimethyl ether synthesis production, the reaction equation that unstripped gas synthesizes dimethyl ether is 2CO+4H
2→ (CH
3)
2o+H
2o+200.2kj; In the time applying as ammonia synthesis unit, arrange with catalyst component take Fe as main, with Al at reative cell (IV)
2o
3, K
2o, CaO, SiO
2, BaO is promoter, then the N of a volume
2h with three volumes
2after mixing, be input in combination reaction device as unstripped gas, carry out Ammonia Production, the reaction equation that unstripped gas synthesizes ammonia is N
2+ 3H
2→ 2NH
3+ 92.1kj.
Claims (10)
1. the self-loopa chemosynthesis reaction device of an one way compression, it is characterized in that reactor is mainly by reative cell (IV), upper chamber (VII), decline passway (V), lower chamber (III), cooling jacket (VI), cooling floor (25) and shell (9) composition, wherein, reative cell (IV), upper chamber (VII), decline passway (V) and lower chamber (III) are arranged in the interior space of shell (9), cooling jacket (VI) is looped around the hull outside in shell (9) stage casing, cooling jacket (VI) is made up of the space between outer wall (11) and shell (9) middle housing outside, cooling floor (25) is closely connected on the housing inner side in shell (9) stage casing, decline passway (V) is made up of the space between interior side body and the reative cell wall body (7) in shell (9) stage casing, upper chamber (VII) is in the top of reative cell (IV), the below of reative cell (IV) is lower chamber (III), the interior space that upper chamber (VII) is surrounded by upper end (3) and shell (9) upper casing forms, the interior space that lower chamber (III) is surrounded by lower end (16) and the lower piece housing of shell (9) forms, reative cell (IV) is communicated to upper chamber (VII), and upper chamber (VII) is communicated to lower chamber (III) by decline passway (V),
Reative cell wall body (7) is made up of cylinder sidewall and circular arc bottom, reative cell wall body (7) is connected on the housing of shell (9) by upper supporting piece (4) and lower support element (23), has circulating air input port (24) access and catalyst discharging outlet (12) to pick out in lower sidewall or the circular arc bottom of reative cell wall body (7); The heat-absorbent surface of cooling floor (25) is arranged in decline passway (V); Lower chamber (III) has raw material tonifying Qi interface (21) access, lower chamber (III) is communicated to the bottom of reative cell (IV) by circulating air input port (24), the bottom of lower chamber (III) is liquid collecting zone (I), and the bottom of liquid collecting zone (I) has product outlet (17) to pick out.
2. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, is characterized in that cooling floor (25) is for multi-disc setting, and the heat-absorbent surface of the cooling floor of multi-disc (25) is to be arranged on around mode in decline passway (V).
3. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, is characterized in that half partition-type structures of circulating air input port (24) for multi-through hole.
4. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, is characterized in that installing heat insulation layer (8) on the lateral wall of reative cell wall body (7).
5. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, is characterized in that the bottom having heaters (10) at reative cell (IV), and heater (10) is electric heater and heat exchanger one wherein.
6. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, it is characterized in that there is circulating air communicating pipe (14) on the circulating air input port (24) of reative cell, gas skirt (20) is set in lower chamber (III), the top of gas skirt (20) is connected on the input port of circulating air communicating pipe (14), the interior space of gas skirt (20) forms collection chamber (II), and collection chamber (II) is communicated to reative cell (IV) by circulating air communicating pipe (14).
7. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, it is characterized in that in lower chamber (III), there is gas-liquid separator (15), gas-liquid separator (15) comprises louvre type separator, coil pipe cooling separator and surface cooler formula separator.
8. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, it is characterized in that on the top of upper end (3), there is catalyst charging hole (VIII), catalyst charging hole (VIII) seals by top cover (1), between top cover (1) and upper end (3) joint face, has sealing ring a(2).
9. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, it is characterized in that upper end (3) is disk structure, upper end (3) is arranged on the upper port of shell (9), between upper end (3) and the joint face of shell (9) upper port, has sealing ring b(26).
10. the self-loopa chemosynthesis reaction device of a kind of one way compression according to claim 1, it is characterized in that lower end (16) is for circular arc bottom structure, lower end (16) is arranged on the lower port of shell (9), between the lower port of shell (9) and the joint face of lower end (16), has sealing ring c(19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320827695.1U CN203598801U (en) | 2013-12-17 | 2013-12-17 | Self-circulation chemical synthesis reactor with single-stroke compression function |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320827695.1U CN203598801U (en) | 2013-12-17 | 2013-12-17 | Self-circulation chemical synthesis reactor with single-stroke compression function |
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| Publication Number | Publication Date |
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| CN203598801U true CN203598801U (en) | 2014-05-21 |
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| CN201320827695.1U Withdrawn - After Issue CN203598801U (en) | 2013-12-17 | 2013-12-17 | Self-circulation chemical synthesis reactor with single-stroke compression function |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103691368A (en) * | 2013-12-17 | 2014-04-02 | 衢州昀睿工业设计有限公司 | One-way compression type self-circulation chemical synthesis reactor |
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2013
- 2013-12-17 CN CN201320827695.1U patent/CN203598801U/en not_active Withdrawn - After Issue
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103691368A (en) * | 2013-12-17 | 2014-04-02 | 衢州昀睿工业设计有限公司 | One-way compression type self-circulation chemical synthesis reactor |
| CN103691368B (en) * | 2013-12-17 | 2015-06-10 | 衢州昀睿工业设计有限公司 | One-way compression type self-circulation chemical synthesis reactor |
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