CN206697444U - multifunctional sample table of scanning electron microscope - Google Patents

multifunctional sample table of scanning electron microscope Download PDF

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Publication number
CN206697444U
CN206697444U CN201720389693.7U CN201720389693U CN206697444U CN 206697444 U CN206697444 U CN 206697444U CN 201720389693 U CN201720389693 U CN 201720389693U CN 206697444 U CN206697444 U CN 206697444U
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China
Prior art keywords
sample
placement table
pressing plate
base
conductive
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CN201720389693.7U
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Chinese (zh)
Inventor
黄成刚
马新民
吴丽荣
杨森
惠媛媛
李志明
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Petrochina Co Ltd
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Petrochina Co Ltd
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Abstract

The utility model relates to a multifunctional sample stage of a scanning electron microscope, which comprises a base, a sample placing table and a conductive pressing plate. The base can be installed on the tray of scanning electron microscope to be connected with the tray electrically conductive. The sample placing table is fixed on the base, is in conductive connection with the base and is used for placing a sample to be tested. One end of the conductive pressure plate is pressed on one side of the sample to be measured, which is provided with the metal coating, and the other end of the conductive pressure plate is connected on the sample placing table and is in conductive connection with the sample placing table. The sample placing table is bent into an L shape by a plate, a first side surface of the sample placing table is horizontally fixed on the base, and a second side surface is vertically upward; the sample to be measured is placed on the first side surface of the sample placing table, and the side with the metal coating faces upwards; the conductive pressure plate is slidably connected to the second side of the sample rest. The utility model discloses can play electrically conductive effect when fixed sample that awaits measuring, can not destroy the metallic coating on sample surface that awaits measuring.

Description

The multifunctional sample platform of ESEM
Technical field
The utility model is on a kind of parts of ESEM, more particularly to a kind of multifunctional sample of ESEM Platform.
Background technology
Exist it is well known that the operation principle of ESEM discharges a large amount of electronics for filament (Flied emission filament or tungsten filament) Accelerate in the presence of magnetic field and electric field, bombardment testing sample surface, be allowed to produce secondary electron or backscattered electron, from into Picture.When substantial amounts of electronics bombards nonconducting testing sample surface under upper state, easily produce charge accumulation and electric discharge is existing As so that High brightness characteristics are presented in image local area.Therefore researcher is in sample non-conductive with sem test Obtaining clearly image can be before testing with plated film instrument in testing sample surface plating last layer conductive metal elements (such as Au, Cr Deng), other faces of testing sample are still non-conductive, then by testing sample bundled fixed and connect surface to be measured with conducting adhesive cloth With metal-like sample platform, it is allowed to export unnecessary electric charge and avoids electric discharge phenomena, is dissipated so as to obtain clearly secondary electron image or the back of the body Radio subgraph (China State Bureau of Quality and Technical Supervision, GB/T 18295-2001 oil and gas reservoir sample of sandstone SEM point Analysis method, p.1-8,2001).This method that binding testing sample is pasted using conducting adhesive cloth is easily destroyed the gold-plated of tested surface Layer, it is unfavorable for secondary supplement test in future.
Researcher consider how sample stages clamping testing sample and solve when designing and manufacturing sample platform of scanning electronic microscope more Certainly rotatable function problem, such as Li Yan fine jades etc., sample platform of scanning electronic microscope, the patent No.:CN201520290865.6.Also there is portion Point sample stage is designed for solving the problems, such as how more setting-out product numbers are so as to improving testing efficiency, such as Cheng Jin etc., one kind Awkward silence at a meeting ESEM multifunctional sample platform, the patent No.:CN201620194696.0;And osmanthus dawn dew etc., scanning electron microscope electron Back scattering multifunctional sample platform, the patent No.:CN201520820847.4.Current yet there are no setting for sample stage in the prior art Meter manufacture is specific to electric discharge and conductivity issues.
Thus, the present inventor relies on experience and the practice for being engaged in relevant industries for many years, proposes a kind of more work(of ESEM Can sample stage, the defects of to overcome prior art.
Utility model content
The purpose of this utility model is the multifunctional sample platform for providing a kind of ESEM, in the same of fixed testing sample When can play electric action, the coat of metal on testing sample surface will not be destroyed.
The purpose of this utility model is achieved in that a kind of multifunctional sample platform of ESEM, the one of testing sample There is the coat of metal side, and the multifunctional sample platform of the ESEM includes:
It base, can be installed on the pallet of the ESEM, and be conductively connected with the pallet;
Sample placement table, it is fixed on the base, and is conductively connected with the base, for places testing sample;With And
Conductive pressing plate, one end of the conductive pressing plate are pressed on the side on the testing sample with the coat of metal, separately One end is connected on the sample placement table and is conductively connected with the sample placement table.
The coat of metal on testing sample surface and sample placement table are conductively connected by conductive pressing plate, so as to electric with scanning The pallet of mirror is conductively connected;Also testing sample is fixed for conductive pressing plate simultaneously, will not destroy the metal on testing sample surface Coating.
In a better embodiment of the present utility model, the conductive pressing plate sample placement table can slide relatively It is connected on the sample placement table.Conductive plate may move, and adapt to the testing sample of different height or width.
In a better embodiment of the present utility model, the sample placement table is bent L-shaped, the sample by sheet material The first side of placement table is horizontally fixed on the base, and second side is straight up;The testing sample is placed on described The first side of sample placement table, there is the side of the coat of metal upward;The conductive pressing plate is slidably connected at the sample and put Put the second side of platform.There is baffle plate vertically upward on one side of sample placement table, and other three sides are open space, so unlimited System puts testing sample specification and size.
In a better embodiment of the present utility model, the conductive pressing plate is L-shaped, the first side of the conductive pressing plate Elongated slot is opened up on wall;Trip bolt is threadedly coupled in the second side of the sample placement table, the trip bolt is positioned at described In elongated slot, the conductive pressing plate can be slided in vertical direction and fixed by the trip bolt;Second side of the conductive pressing plate Wall protrudes horizontally up, for being pressed on the coat of metal of the testing sample.Conductive plate moving up and down is set using " L " shape Meter, testing sample can be not only fixed, and for the conduction on surface to be measured.
In a better embodiment of the present utility model, the nut of the trip bolt is pinched provided with outwardly hand Hold portion.The outwardly setting of nut of trip bolt, it is easy to hand to twist and fixes, it is simple and convenient.
In a better embodiment of the present utility model, the base, the sample placement table and the conductive pressing plate Made using conductive material.
From the above mentioned, multifunctional sample platform of the present utility model has advantages below:1st, test sample will be treated by conductive pressing plate The coat of metal on product surface is conductively connected with sample placement table, so as to which the pallet with ESEM is conductively connected;Conductive pressure simultaneously Also testing sample is fixed for plate, will not destroy the coat of metal on testing sample surface.2nd, one side of sample placement table has vertical Straight upward baffle plate, other three sides are open space, do not limit put testing sample specification and size so.3rd, can on move down Dynamic conductive plate is designed using " L " shape, can not only fix testing sample, and for the conduction on surface to be measured.4th, conductive plate It can move up and down, adapt to the testing sample of different height.5th, the outwardly setting of the nut of trip bolt, it is easy to hand to twist solid It is fixed, it is simple and convenient.
Brief description of the drawings
The following drawings is only intended to, in doing the utility model schematic illustration and explanation, not limit model of the present utility model Enclose.Wherein:
Fig. 1:For the structural representation of the utility model multifunctional sample platform.
Embodiment
In order to which the technical characteristics of the utility model, purpose and effect are more clearly understood, now control illustrates Specific embodiment of the present utility model.In the utility model described " connection ", both including being joined directly together between two parts, Also include by least one intermediate member being connected between two parts.The noun of locality employed in the utility model is (as above, Under, it is forward and backward etc.) be intended merely to reference to the clearer statement technology contents of accompanying drawing, not to the tool of technical solutions of the utility model Body limits.
As shown in figure 1, the utility model provides a kind of multifunctional sample platform 10 of ESEM, the side of testing sample There is the coat of metal, other sides are non-conductive, and beam bombardment is the side with the coat of metal, i.e., surface to be measured.It is described The multifunctional sample platform 10 of ESEM includes base 1, sample placement table 2 and conductive pressing plate 3.Base 1 can be installed to described sweep Retouch in the pallet (not shown) of Electronic Speculum, and be conductively connected with the pallet.The tool of base 1 is not limited in the utility model Body form, illustrated with one of which specific embodiment, the main body of base 1 is round pie, its underpart circle centre position have one to The thin cylindrical rod 11 of lower stretching is attached thereto, and its top is streamlined to be stretched out upwards, and the top of base 1 is fixed with sample placement table 2 It is connected.The main part of base 1 is thick 3mm, diameter 20mm cake, and the thin cylindrical rod 11 of its underpart circle centre position is about 8mm, directly Footpath about 3mm.The thin cylindrical rod 11 is mainly used in the circular hole for the sample tray that interleave scan Electronic Speculum carries.
Sample placement table 2 is fixed on the base 1, and is conductively connected with the base 1, for placing testing sample. The concrete form of unlimited random sample product placement table 2 in the utility model, in a preferable specific embodiment, the sample is shelved Platform 2 is bent L-shaped by sheet material, or is dustpan shape.The first side 21 of the sample placement table 2 is horizontally fixed on the base On 1, first side 21 is length of side 20mm square;Square center is connected as a single entity with base 1.Second side 22 is straight up Stretch out, the width of second side 22 is identical with the length of side of first side 21, and the height stretched out upwards is 10mm.That is sample placement table 2 While with baffle plate vertically upward, other three sides are not blocked, and are formed open space, can be placed different size and the sample of size Product.The lower section center of sample placement table 2 is fixed with base 1 and is connected as a single entity, non-dismountable.The testing sample is placed on the sample The first side 21 of product placement table 2, in the present embodiment, side of the testing sample with the coat of metal upward, electron beam on to Lower bombardment surface to be measured, other sides of testing sample are non-conductive.
One end of conductive pressing plate 3 is pressed on the side on the testing sample with the coat of metal, so as to by testing sample It is fixed on sample placement table 2.The other end of conductive pressing plate 3 be connected on the sample placement table 2 and with the sample Placement table 2 is conductively connected.The coat of metal and sample placement table 2 can be conductively connected by conductive pressing plate 3, so as to pass through base 1 Electrically connected with the pallet of ESEM, it is simultaneous to play a part of fixed testing sample.Conductive pressing plate 3 is not limited in the utility model yet Concrete form, as long as above-mentioned effect can be realized.
In a preferred embodiment, the conductive pressing plate 3 is slidably connected at the second side 22 of the sample placement table 2 On.Specifically, the conductive pressing plate 3 is the L-shaped that flat part is bent into, the first side wall 31 is 30mm × 10mm rectangle;The Two side walls 32 are length of side 10mm square.Elongated slot 33 is opened up on the first side wall 31 of the conductive pressing plate 3.The sample is shelved There are screwed hole, screwed hole internal thread connection trip bolt 4 in the second side 22 of platform 2, the trip bolt 4 is located at the elongated slot In 33, the groove width and the diameter of trip bolt 4 of elongated slot 33 are essentially identical, are allowed to move freely in elongated slot 33.Conduction pressure The first side wall 31 of plate 3 is vertically arranged, and elongated slot 33 is enclosed on trip bolt 4, is slided in vertical direction and by the trip bolt 4 It is fixed.The second sidewall 32 of the conductive pressing plate 3 protrudes horizontally up, and for being pressed on the coat of metal of the testing sample, rises To fixed and electric action.Conductive pressing plate 3 moves up and down the testing sample for adapting to different height.
Further, the trip bolt 4 includes screw rod and nut, and screw rod uses the horizontal tail self-tapping screw pattern of standard, Nut is provided with outwardly hand grips, is easy to hand to twist and fixes.
In above-mentioned various embodiments, base 1, sample placement table 2 and conductive pressing plate 3 are made using conductive material, example As used metal material, the multifunctional sample platform 10 of monolithic conductive is formed.
The schematical embodiment of the utility model is the foregoing is only, is not limited to model of the present utility model Enclose.All combinations of illustrated feature are not necessarily the solution that the utility model is limited in embodiment, can be with Understand that these additional construction features and operations improvement can be used alone or be combined with each other.It will therefore be appreciated that The utility model is not limited to the combination of any specific feature or element, and any desired combinations of features described here is all It can be carried out without departing from the scope of protection of the utility model, any those skilled in the art, not depart from the utility model Design and principle on the premise of made equivalent variations and modification, the scope of the utility model protection all should be belonged to.

Claims (6)

1. there is the coat of metal a kind of multifunctional sample platform of ESEM, the side of testing sample, it is characterised in that the scanning The multifunctional sample platform of Electronic Speculum includes:
It base, can be installed on the pallet of the ESEM, and be conductively connected with the pallet;
Sample placement table, it is fixed on the base, and is conductively connected with the base, for places testing sample;And
Conductive pressing plate, one end of the conductive pressing plate are pressed on the side on the testing sample with the coat of metal, the other end It is connected on the sample placement table and is conductively connected with the sample placement table.
2. the multifunctional sample platform of ESEM as claimed in claim 1, it is characterised in that the conductive pressing plate can relative institute State being connected on the sample placement table for sample placement table slip.
3. the multifunctional sample platform of ESEM as claimed in claim 1, it is characterised in that the sample placement table is by sheet material Bend L-shaped, the first side of the sample placement table is horizontally fixed on the base, and second side is straight up;It is described Testing sample is placed on the first side of the sample placement table, has the side of the coat of metal upward;The conductive pressing plate is slided The dynamic second side for being connected to the sample placement table.
4. the multifunctional sample platform of ESEM as claimed in claim 3, it is characterised in that the conductive pressing plate is L-shaped, institute State and elongated slot is opened up on the first side wall of conductive pressing plate;Trip bolt is threadedly coupled in the second side of the sample placement table, institute State trip bolt to be located in the elongated slot, the conductive pressing plate can be slided in vertical direction and fixed by the trip bolt;Institute The second sidewall for stating conductive pressing plate protrudes horizontally up, for being pressed on the coat of metal of the testing sample.
5. the multifunctional sample platform of ESEM as claimed in claim 4, it is characterised in that on the nut of the trip bolt Provided with outwardly hand grips.
6. the multifunctional sample platform of the ESEM as any one of claim 1-5, it is characterised in that the base, The sample placement table and the conductive pressing plate are made using conductive material.
CN201720389693.7U 2017-04-14 2017-04-14 multifunctional sample table of scanning electron microscope Active CN206697444U (en)

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Publications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112397365A (en) * 2019-08-14 2021-02-23 中国科学院上海硅酸盐研究所 Sample table suitable for TIC3X three-ion-beam cutting instrument
CN115394620A (en) * 2022-10-27 2022-11-25 中铝材料应用研究院有限公司 Scanning electron microscope sample stage

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112397365A (en) * 2019-08-14 2021-02-23 中国科学院上海硅酸盐研究所 Sample table suitable for TIC3X three-ion-beam cutting instrument
CN112397365B (en) * 2019-08-14 2022-06-14 中国科学院上海硅酸盐研究所 Sample table suitable for TIC3X three-ion-beam cutting instrument
CN115394620A (en) * 2022-10-27 2022-11-25 中铝材料应用研究院有限公司 Scanning electron microscope sample stage

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