CN205710264U - 一种线路板蚀刻废液处理系统 - Google Patents
一种线路板蚀刻废液处理系统 Download PDFInfo
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- CN205710264U CN205710264U CN201620585910.5U CN201620585910U CN205710264U CN 205710264 U CN205710264 U CN 205710264U CN 201620585910 U CN201620585910 U CN 201620585910U CN 205710264 U CN205710264 U CN 205710264U
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- 238000005530 etching Methods 0.000 title claims abstract description 25
- 239000002699 waste material Substances 0.000 title claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 230000003647 oxidation Effects 0.000 claims abstract description 16
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 16
- 238000000926 separation method Methods 0.000 claims abstract description 15
- 238000003828 vacuum filtration Methods 0.000 claims abstract description 15
- 239000012153 distilled water Substances 0.000 claims abstract description 14
- 239000010413 mother solution Substances 0.000 claims abstract description 5
- 238000004064 recycling Methods 0.000 claims abstract description 4
- 238000001704 evaporation Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 4
- 238000010025 steaming Methods 0.000 claims description 2
- 239000010865 sewage Substances 0.000 abstract description 4
- 239000000243 solution Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 10
- 239000002351 wastewater Substances 0.000 description 10
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound 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- CVTZKFWZDBJAHE-UHFFFAOYSA-N [N].N Chemical compound 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[N].N CVTZKFWZDBJAHE-UHFFFAOYSA-N 0.000 description 6
- 229910052802 copper Inorganic materials 0.000 description 6
- 239000010949 copper Substances 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 230000002378 acidificating Effects 0.000 description 5
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- VQSXKKXMSXGLBZ-UHFFFAOYSA-L copper;chloride;hydroxide Chemical compound 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[OH-].[Cl-].[Cu+2] VQSXKKXMSXGLBZ-UHFFFAOYSA-L 0.000 description 4
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[Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N ammonia chloride Chemical compound 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[NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 3
- 235000019516 cod Nutrition 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- 230000001590 oxidative Effects 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- ORTQZVOHEJQUHG-UHFFFAOYSA-L Copper(II) chloride Chemical compound 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Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 230000003750 conditioning Effects 0.000 description 1
- -1 copper Nitrogen Chemical compound 0.000 description 1
- 230000005712 crystallization Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000003628 erosive Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000010808 liquid waste Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N phosphorus Chemical compound 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Abstract
本实用新型属于污水处理技术领域，公开了一种线路板蚀刻废液处理系统。所述系统包括依次连接的氧化池、反应池、真空抽滤系统和蒸发系统；所述氧化池出水口连接至反应池，反应池出水口连接至真空抽滤系统；所述真空抽滤系统设置清液出口和晶体出口，清液出口连接至蒸发系统；所述蒸发系统设置蒸馏水出口和浓液出口，蒸馏水出口连接至回用水池，浓液出口连接至固液分离系统，固液分离系统与蒸发系统之间设置母液循环回路。本实用新型的系统可实现线路板蚀刻废液最大程度的无害化处理并实现一定的经济价值。
Description
技术领域
[0001]本实用新型属于污水处理技术领域，具体涉及一种线路板蚀刻废液处理系统。
背景技术
[0002]印制线路板是电子行业重要的基础产业，由于电子工业快速发展，我国PCB的产量增长速度很快，蚀刻是印制电路板工艺不可缺少的工序，其生产过程中产生的废水统称为蚀刻液，其污染物主要分为三大类:重金属(Cu2+、Sn+、Ni+、Pb2+等)、无机盐(NH4+、C1—等)、有机物(溶解的保护膜等)，通常是采用离子交换、萃取、化学沉淀等方法回收废水里的铜，回收铜后的废水由于其成分复杂，毒性大，氨氮浓度非常高(几万至十几万PPM)，含碳量低，采用传统的生物脱氮技术很难有效处理，本专利采用蒸发结晶法处理，出水氨氮指标在25ppm以下，可满足《GB8978-1996污水排放标准》二级排放标准。
实用新型内容
[0003]为了解决现有技术的缺点和不足之处，本实用新型的目的在于提供一种线路板蚀刻废液处理系统。
[0004]本实用新型目的通过以下技术方案实现:
[0005] —种线路板蚀刻废液处理系统，包括依次连接的氧化池、反应池、真空抽滤系统和蒸发系统;所述氧化池出水口连接至反应池，反应池出水口连接至真空抽滤系统;所述真空抽滤系统设置清液出口和晶体出口，清液出口连接至蒸发系统;所述蒸发系统设置蒸馏水出口和浓液出口，蒸馏水出口连接至回用水池，浓液出口连接至固液分离系统，固液分离系统与蒸发系统之间设置母液循环回路。
[0006]上述处理系统所述的连接是指通过常规管道和栗连接。其中氧化池的主要作用为加入H2O2或NaClO等氧化剂，氧化有机物，降低酸性蚀刻液的COD，反应池的作用为加入碱性蚀刻液混合，再通过氨水或盐酸调节溶液的PH值，并控制反应温度和反应时间，使铜以碱式氯化铜的方式沉淀下来，真空抽滤系统的作用是分离碱式氯化铜固体和溶液，蒸发系统可以是机械式蒸汽再压缩蒸发系统，也可以是多效蒸发系统，其作用为处理回收铜后的高氨氮废水，使废水可以满足二级排放标准，回用水池的作用是回用水存储，固液分离系统的作用是固液分离系统的作用是分离固体和母液。固液分离系统可以是离心机，也可以是压滤机，也可以是真空抽滤设备。
[0007]采用上述系统对线路板废水进行处理的工作原理如下:
[0008] (I)将酸性蚀刻液送入氧化池，通过加入H2O2或NaClO等氧化剂，氧化有机物，降低酸性蚀刻液的C0D。
[0009] (2)氧化后的废水由栗送入反应池，加入碱性蚀刻液混合，然后加入氨水或盐酸调节溶液的PH值至3〜5，并控制反应温度在70〜80°C，这一步的主要目的是使大部分铜变为碱式氯化铜沉淀；
[0010] (3)反应池的固液混合物送入真空抽滤系统，过滤出的固体为碱式氯化铜晶体，可以回收或卖出；
[0011] (4)抽滤后的清液进入蒸发系统，通过蒸发系统的不断蒸发，水等低沸点物吸收热量变为二次蒸汽，二次蒸汽冷凝后变为蒸馏水，蒸馏水可以达到《GB8978-1996污水综合排放标准》的二级排放标准，其氨氮值在25ppm以内。蒸馏水排入回用水池，可以直接排放或回用。无机盐等高沸点物被截留在浓缩液中，浓缩液为固液混合物。
[0012] (6)浓缩液由栗送入固液分离系统，分离后固体主要为氯化铵晶体，可以卖出，母液返回蒸发系统继续蒸发。
[0013]本实用新型具有如下优点及有益效果:
[0014] (I)本实用新型的系统用于处理线路板蚀刻废液，可以回收大部分铜，可以通过蒸发结晶得到可以卖出的氯化铵晶体，实现线路板蚀刻废液最大程度的无害化处理并实现了经济价值；
[0015] (2)现有的系统及方法都难以将蚀刻废液中的氨氮值降低至排放标准，本实用新型系统采用了蒸发技术做为核心，处理后氨氮的含量在25ppm以下，满足《GB8978-1996污水综合排放标准》的二级排放标准，可以直接排放；
[0016] (3)本系统采用了低能耗及低运行费用的机械式蒸汽再压缩蒸发技术或多效蒸发技术，大大降低了蒸发的运行能耗。
附图说明
[0017]图1为本实用新型所述线路板蚀刻废液处理系统的连接关系构造图。
具体实施方式
[0018]下面结合实施例及附图对本实用新型作进一步详细的描述，但本实用新型的实施方式不限于此。
[0019] 实施例1
[0020]本实施例的一种线路板蚀刻废液处理系统，其连接关系构造图如图1所示。所述系统包括依次连接的氧化池、反应池、真空抽滤系统和蒸发系统;所述氧化池出水口连接至反应池，反应池出水口连接至真空抽滤系统;所述真空抽滤系统设置清液出口和固体出口，清液出口连接至蒸发系统;所述蒸发系统设置蒸馏水出口和浓液出口，蒸馏水出口连接至回用水池，浓液出口连接至固液分离系统，固液分离系统与蒸发系统之间设置母液循环回路。[0021 ]采用本实施例的系统对线路板蚀刻废液进行处理的过程如下:
[0022] (I)将酸性蚀刻液送入氧化池，通过加入H2O2或NaClO等氧化剂，氧化有机物，降低酸性蚀刻液的C0D。
[0023] (2)氧化后的废水由栗送入反应池，加入碱性蚀刻液混合，然后加入氨水或盐酸调节溶液的PH值至4，并控制反应温度在75°C，这一步的主要目的是使大部分铜变为碱式氯化铜沉淀；
[0024] (3)反应池的固液混合物送入真空抽滤系统，过滤出的固体为碱式氯化铜晶体，可以回收或卖出；
[0025] (4)抽滤后的清液进入蒸发系统，通过蒸发系统的不断蒸发，水等低沸点物吸收热量变为二次蒸汽，二次蒸汽冷凝后变为蒸馏水，蒸馏水可以达到《GB8978-1996污水综合排放标准》的二级排放标准，其氨氮值在20ppm左右。蒸馏水排入回用水池，可以直接排放或回用。无机盐等高沸点物被截留在浓缩液中，浓缩液为固液混合物。
[0026] (6)浓缩液由栗送入固液分离系统，分离后固体主要为氯化铵晶体，可以卖出，母液返回蒸发系统继续蒸发。
[0027]上述实施例为本实用新型较佳的实施方式，但本实用新型的实施方式并不受上述实施例的限制，其它的任何未背离本实用新型的精神实质与原理下所作的改变、修饰、替代、组合、简化，均应为等效的置换方式，都包含在本实用新型的保护范围之内。
Claims (3)
1.一种线路板蚀刻废液处理系统，其特征在于:所述系统包括依次连接的氧化池、反应池、真空抽滤系统和蒸发系统;所述氧化池出水口连接至反应池，反应池出水口连接至真空抽滤系统;所述真空抽滤系统设置清液出口和晶体出口，清液出口连接至蒸发系统;所述蒸发系统设置蒸馏水出口和浓液出口，蒸馏水出口连接至回用水池，浓液出口连接至固液分离系统，固液分离系统与蒸发系统之间设置母液循环回路。
2.根据权利要求1所述的一种线路板蚀刻废液处理系统，其特征在于:所述的蒸发系统是指机械式蒸汽再压缩蒸发系统或多效蒸发系统。
3.根据权利要求1所述的一种线路板蚀刻废液处理系统，其特征在于:所述的固液分离系统是指离心机、压滤机或真空抽滤设备。
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