CN205340222U - Chromatographic fractionation device - Google Patents
Chromatographic fractionation device Download PDFInfo
- Publication number
- CN205340222U CN205340222U CN201521071224.8U CN201521071224U CN205340222U CN 205340222 U CN205340222 U CN 205340222U CN 201521071224 U CN201521071224 U CN 201521071224U CN 205340222 U CN205340222 U CN 205340222U
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- chromatographic column
- chromatographic
- lower wall
- plate
- separation device
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Abstract
The utility model discloses a chromatographic fractionation device belongs to separator, and its structure comprises actuating system, transmission system, rotatory distribution valve and chromatographic column and pipe connection, the chromatographic column adopts a stainless steel round section of thick bamboo, and the upper end faces imported one side at first filter screen to be provided with the baffle for import, lower extreme is equipped with first filter screen for the export in the chromatographic column inner chamber of entrance point, is equipped with the second filter screen in the chromatographic column inner chamber of exit end, sets up an export on the upper portion of chromatographic column is close to the lateral wall of first filter screen to fill in the shutoff with the metal, chromatographic column support through the disc between chromatographic column and the macroaxis connects into as an organic wholely. The utility model discloses a chromatographic fractionation device has characteristics such as simple structure, low in production cost, therefore has fine popularization and application value.
Description
Technical field
This utility model relates to a kind of segregation apparatus, especially a kind of chromatographic separation device.
Background technology
Simulated moving bed chromatography partition method is to exchange, at ion, a kind of advanced chromatographic separation technology grown up on moving bed basis, this isolation technics has been widely used for the fields such as petrochemical industry, medicine, food and biochemical engineering at present, and achieves good Social and economic benef@.China's starch sugar industry develops rapidly in recent years, product category is increasing, wherein especially starch yield for maximum with fruit/glucose, but high fructose syrup domestic at present is first generation product, in beverage industry, the sweeting agent as used by " coca cola ", " JIANLIBAO " all adopts the second filial generation high fructose syrup that fructose content is 55% of external import.Therefore, domestic 42% high fructose syrup product is badly in need of the renewal replacement, and makes the 55% optimal technological means of high fructose syrup and adopt chromatographic separation technology exactly.And realizing the technical way of process-scale chromatography isolation technics, optimal lectotype selection adopts moving bed imitation chromatogram separation facility exactly.But present used chromatographic separation device structure is complicated, and cost is high, is unfavorable for domestic application and popularization.
Utility model content
Technical assignment of the present utility model is that this chromatographic separation device has simple in construction, the feature that production cost is low for above-mentioned a kind of chromatographic separation device of not enough offer of the prior art.
This utility model solves its technical problem be the technical scheme is that it is by drive system, drive system, rotary distributor and chromatographic column and pipeline connect and compose, drive system is reductor, reductor is arranged on reducer pedestal, drive system is that reductor shaft is connected with driven gear, driven gear is connected with driving gear, driving gear is connected with big axle, big axle top is provided with Anti-withdrawing bolt, the lower end of big axle is connected to thimble by thrust bearing and rolling bearing, thimble bottom is provided with thimble adjusting bolt, big axle is connected to rotary distributor, rotary distributor, chromatographic column and big axle are arranged in casing, upper plate it is provided with between casing and reducer pedestal, rotary distributor from upper dish contact with lower card dynamic mutually with, upper dish and big between centers are provided with thrust bearing and rolling bearing, described lower wall is provided with the lower wall runner through hole of circumference uniform distribution, described lower wall runner through hole is corresponding with chromatographic column inlet and outlet number, and be connected with chromatographic column inlet and outlet successively, upper dish is provided with the upper dish runner through hole corresponding with lower wall runner through hole, it is characterized in that: described chromatographic column adopts rustless steel cylinder, upper end is import, lower end is outlet, the chromatographic column inner chamber of entrance point is provided with the first drainage screen, the side facing import at the first drainage screen is provided with baffle plate, the chromatographic column inner chamber of the port of export is provided with the second drainage screen, one outlet is set on the sidewall of the first drainage screen on the top of chromatographic column, and block with metal closures；
It is connected in one by discoidal chromatographic column support between described chromatographic column and big axle.
The casing of described big axle bottom is provided with lower middle plate, bottom of shell is provided with lower plate, it is provided with blower fan between lower middle plate and lower plate, blower fan one end connects intake stack, the other end connects wind pipe, electric furnace heating wire it is provided with in wind pipe, intake stack communicates with lower middle plate respectively with the other end of wind pipe, in lower, plate is connected by bolt block with the middle part of lower plate, bolt block is provided with by cap, thimble adjusting bolt is arranged on by the top of cap, and lower plate is provided with directional wheel and universal wheel.
Driving gear is tied by fastening screw and is connected to contact shoe, the bottom of contact shoe is circumferentially evenly distributed with the contact equal with chromatographic column number, the upper plate of contact shoe bottom is provided with proximity switch support, being provided with proximity switch on proximity switch support, described proximity switch is corresponding with contact position.
Between contact shoe bottom and thrust bearing big axle on be provided with butterfly spring, be provided with spring pressure cap between butterfly spring and contact shoe.
It is provided with gasket seal between upper dish and lower wall.
The upper and lower two ends of chromatographic column are respectively arranged with ferrule fitting, and upper dish and lower wall and pipeline junction are provided with pipeline ferrule fitting.
Lower tray bottom is provided with positioning disk, fixes with lower wall by fastening bolt.
Described first, second drainage screen is the unidirectional penetrating film of macromolecule, is set to multilamellar.
Compared to the prior art chromatographic separation device of the present utility model, has beneficial effect highlighted below: simple in construction, and production cost is low, improves production efficiency, it is possible to stably control product quality, easy to use, convenient operation and management etc. feature.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of chromatographic separation device；
Accompanying drawing 2 is the sectional view of chromatographic column；
Accompanying drawing 3 is the full sectional view of upper dish；
Accompanying drawing 4 is layout and the runner schematic diagram of passage in upper dish；
Accompanying drawing 5 is the full sectional view of lower wall；
Accompanying drawing 6 is the schematic layout pattern of passage in lower wall；
Accompanying drawing 7 is the sectional view of gasket seal；
Accompanying drawing 8 is gasket seal top view；
Accompanying drawing 9 is the schematic diagram of chromatographic column support；
Description of reference numerals: 1, reductor, 2, reducer pedestal, 3, driven gear, 4, spring pressure cap, 5, butterfly spring, 6, upper plate, 7, thrust bearing, 8, upper dish, 9, pipeline ferrule fitting, 10, lower wall, 11, positioning disk, 12, fastening bolt, 13, big axle, 14, thimble, 15, thimble adjusting bolt, 16, intake stack, 17, blower fan, 18, lower plate, 19, directional wheel, 20, Anti-withdrawing bolt, 21, driving gear, 22, contact shoe, 23, contact, 24, proximity switch support, 25, rolling bearing, 26, drainage road through hole on upper dish, 27, drainage road through hole under upper dish, 28, drainage road through hole on lower wall, 29, drainage road through hole under lower wall, 30, ferrule fitting, 31, chromatographic column, 32, by cap, 33, plate in lower, 34, bolt block, 35, electric furnace heating wire, 36, wind pipe, 37, universal wheel, 38, proximity switch, 39, gasket seal, 40, casing, 41, pipeline, 46, glucose exports, 47U shape pipe, 48 first drainage screens, 49 second drainage screens, 50 baffle plates, 51 outlets, 52 chromatographic column supports, 521 sleeves, 522 grooves.
Detailed description of the invention
With reference to Figure of description 1, accompanying drawing 2, chromatographic separation device of the present utility model is described in detail below.
Chromatographic separation device of the present utility model, its structure is by drive system, drive system, rotary distributor and 12 root chromatogram columns 31 and pipeline 41 connect and compose, drive system is reductor 1, reductor 1 is arranged on reducer pedestal 2, drive system is that reductor shaft is connected with driven gear 3, driven gear 3 is connected with driving gear 21, driving gear 21 is connected with big axle 13, big axle 13 top is provided with Anti-withdrawing bolt 20, the lower end of big axle 13 is connected to thimble 14 by thrust bearing 7 and rolling bearing 25, thimble 14 bottom is provided with thimble adjusting bolt 15, big axle 13 is connected to rotary distributor, rotary distributor, chromatographic column 31 and big axle 13 are arranged in casing 40, upper plate 6 it is provided with between casing 40 and reducer pedestal 2, rotary distributor from upper dish 8 and lower wall 10 contact dynamic mutually with, it is provided with thrust bearing 7 and rolling bearing 25 between upper dish 8 and big axle 13, described lower wall 10 is provided with 24 lower wall runner through holes of circumference uniform distribution, described lower wall runner through hole is corresponding with chromatographic column 31 inlet and outlet number, and be connected with chromatographic column 31 inlet and outlet successively, upper dish 8 is provided with the upper dish runner through hole corresponding with lower wall runner through hole, described upper dish runner through hole arranges joint.
12 above-mentioned root chromatogram columns are concatenated with one another.
Upper dish and lower wall pairing are arranged, it is respectively arranged with 12 pairs of inlet union and 12 pairs of outlet connections, inlet union on upper dish is connected by U-tube 47 with outlet connection, and inlet union and outlet connection on lower wall are connected to chromatographic column 31 inlet and outlet respectively through arm.
Above-mentioned chromatographic column 31 adopts stainless steel, and upper end is import, and lower end is outlet, is provided with the first drainage screen 48 in the chromatographic column inner chamber of entrance point, and drainage screen adopts the unidirectional penetrating film of macromolecule, is set to multilamellar, and by skeletal support.Being provided with the second drainage screen 49 in the chromatographic column inner chamber of the port of export, drainage screen adopts the unidirectional penetrating film of macromolecule, is set to multilamellar, and by skeletal support.
For avoiding drainage screen is impacted, the side facing import at the first drainage screen is provided with baffle plate 50, for disperses impact forces.
One outlet 51 is set on the top of chromatographic column on the sidewall of the first drainage screen, and at exit metal closures, opens and unload connection.
Lower wall runner through hole is divided on 12 lower walls drainage road through hole 28 and drainage road through hole 29 under 12 lower walls, on lower wall, drainage road through hole 28 is connected respectively through the import of pipeline 41 with chromatographic column 31, under lower wall, drainage road through hole 29 is connected respectively through the outlet of pipeline 41 with chromatographic column 31, upper dish runner through hole is divided on 12 upper dishes drainage road through hole 26 and drainage road through hole 27 under 12 upper dishes, on described upper dish, drainage road through hole 26 communicates with drainage road through hole 29 under lower wall, and under upper dish, drainage road through hole 27 communicates with drainage road through hole 28 on lower wall.
The casing 40 of described big axle 13 bottom is provided with lower middle plate 33, lower plate 18 it is provided with bottom casing 40, it is provided with blower fan 17 between lower middle plate 33 and lower plate 18, blower fan 17 one end connects intake stack 16, the other end connects wind pipe 36, electric furnace heating wire 35 it is provided with in wind pipe 36, intake stack 16 communicates with lower middle plate 33 respectively with the other end of wind pipe 36, in lower, plate 33 is connected by bolt block 34 with the middle part of lower plate 18, bolt block 34 is provided with by cap 32, thimble adjusting bolt 15 is arranged on by the top of cap 32, lower plate 18 is provided with directional wheel 19 and universal wheel 37.
Driving gear 21 is connected to contact shoe 22 by fastening bolt 12, the bottom of contact shoe 22 is circumferentially evenly distributed with 12 contacts 23 equal with chromatographic column 31 number, the upper plate 6 of contact shoe 22 bottom is provided with proximity switch support 24, being provided with proximity switch 38 on proximity switch support 24, described proximity switch 38 is corresponding with position, contact 23.
Between contact shoe 22 bottom and thrust bearing 7 big axle 13 on be provided with butterfly spring 5, be provided with spring pressure cap 4 between butterfly spring 5 and contact shoe 22, regulate the function of spring pressure size.
Between upper dish 8 and lower wall 10, it is provided with gasket seal 39, gasket seal 39 is provided with the hole communicated with upper dish runner through hole, had both kept material negotiability, possess again sealing effectiveness, maintain device long-term operation.
Chromatographic column about 31 two ends are respectively arranged with ferrule fitting 30, upper dish 8 and lower wall 10 and are provided with pipeline ferrule fitting 9 with pipeline 41 junction.
It is fixed by a discoidal chromatographic column support 52 between 12 above-mentioned root chromatogram columns and big axle 13, chromatographic column support has the sleeve 521 fixing with big axle, and be positioned at the groove 522 of the stationary chromatographic post of periphery, fix with clip.
Bottom lower wall 10, it is provided with positioning disk 11, fixes with lower wall 10 by fastening bolt 12.
Reductor 1 rotates, driven gear 3 is driven to rotate, driven gear 3 is meshed with driving gear 21, thus driving driving gear 21 to rotate, driving gear 21 drives big axle 13 to rotate, and lower wall 10 on big axle 13, chromatographic column 31 and contact shoe 22 1 pieces are along big axle 13 synchronous axial system, and upper dish 8 maintains static, when lower wall 10 often rotates 30 degree, lower wall runner through hole communicates with upper dish runner through hole.
Proximity switch 38 is connected with external controller, when contact 23 touches proximity switch 38, proximity switch 38 passes the signal to controller, controller controls reductor 1 and stops operating, at this moment lower wall runner through hole communicates with upper dish runner through hole, lower wall runner through hole can be entered from material inlet 45 along upper dish runner through hole by needing the material fruit/glucose separated, hence in chromatographic column 31, after reductor 1 stops a period of time, restart, after again rotating 30 degree, namely when next contact 23 touches proximity switch 38, reductor 1 stops operating again, at this moment material can enter in next chromatographic column 31 along upper dish runner through hole, circulate successively, when the glucose in the fruit/glucose separated in chromatographic column is separated, 46 discharges are exported from the glucose of upper dish from column bottom along lower wall runner through hole, owing to fructose is than glucose high adsorption capacity, more late than glucose can export 44 discharges from the fructose of upper dish, reach the purpose separated.
Except the technical characteristic described in description, it is the known technology of those skilled in the art.
Claims (8)
1. chromatographic separation device, it is by drive system, drive system, rotary distributor and chromatographic column and pipeline connect and compose, drive system is reductor, reductor is arranged on reducer pedestal, drive system is that reductor shaft is connected with driven gear, driven gear is connected with driving gear, driving gear is connected with big axle, big axle top is provided with Anti-withdrawing bolt, the lower end of big axle is connected to thimble by thrust bearing and rolling bearing, thimble bottom is provided with thimble adjusting bolt, big axle is connected to rotary distributor, rotary distributor, chromatographic column and big axle are arranged in casing, upper plate it is provided with between casing and reducer pedestal, rotary distributor from upper dish contact with lower card dynamic mutually with, upper dish and big between centers are provided with thrust bearing and rolling bearing, described lower wall is provided with the lower wall runner through hole of circumference uniform distribution, described lower wall runner through hole is corresponding with chromatographic column inlet and outlet number, and be connected with chromatographic column inlet and outlet successively, upper dish is provided with the upper dish runner through hole corresponding with lower wall runner through hole, it is characterized in that: described chromatographic column adopts rustless steel cylinder, upper end is import, lower end is outlet, the chromatographic column inner chamber of entrance point is provided with the first drainage screen, the side facing import at the first drainage screen is provided with baffle plate, the chromatographic column inner chamber of the port of export is provided with the second drainage screen, one outlet is set on the sidewall of the first drainage screen on the top of chromatographic column, and block with metal closures；
It is connected in one by discoidal chromatographic column support between described chromatographic column and big axle.
2. chromatographic separation device according to claim 1, it is characterized in that: the casing of described big axle bottom is provided with lower middle plate, bottom of shell is provided with lower plate, it is provided with blower fan between lower middle plate and lower plate, blower fan one end connects intake stack, the other end connects wind pipe, electric furnace heating wire it is provided with in wind pipe, intake stack communicates with lower middle plate respectively with the other end of wind pipe, in lower, plate is connected by bolt block with the middle part of lower plate, bolt block is provided with by cap, thimble adjusting bolt is arranged on by the top of cap, lower plate is provided with directional wheel and universal wheel.
3. chromatographic separation device according to claim 1, it is characterized in that: tied by fastening screw on driving gear and be connected to contact shoe, the bottom of contact shoe is circumferentially evenly distributed with the contact equal with chromatographic column number, the upper plate of contact shoe bottom is provided with proximity switch support, being provided with proximity switch on proximity switch support, described proximity switch is corresponding with contact position.
4. chromatographic separation device according to claim 3, is characterized in that: is provided with butterfly spring on the big axle between contact shoe bottom and thrust bearing, is provided with spring pressure cap between butterfly spring and contact shoe.
5. chromatographic separation device according to claim 1, is characterized in that: be provided with gasket seal between upper dish and lower wall.
6. chromatographic separation device according to claim 1, is characterized in that: the upper and lower two ends of chromatographic column are respectively arranged with ferrule fitting, and upper dish and lower wall and pipeline junction are provided with pipeline ferrule fitting.
7. chromatographic separation device according to claim 1, is characterized in that: lower tray bottom is provided with positioning disk, fixes with lower wall by fastening bolt.
8. chromatographic separation device according to claim 1, is characterized in that: first, second drainage screen is the unidirectional penetrating film of macromolecule, is set to multilamellar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521071224.8U CN205340222U (en) | 2015-12-19 | 2015-12-19 | Chromatographic fractionation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521071224.8U CN205340222U (en) | 2015-12-19 | 2015-12-19 | Chromatographic fractionation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205340222U true CN205340222U (en) | 2016-06-29 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201521071224.8U Expired - Fee Related CN205340222U (en) | 2015-12-19 | 2015-12-19 | Chromatographic fractionation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205340222U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106267893A (en) * | 2016-08-23 | 2017-01-04 | 兆光生物工程(邹平)有限公司 | A kind of moving bed imitation chromatogram separation facility |
| CN109283271A (en) * | 2018-10-15 | 2019-01-29 | 兰州东立龙信息技术有限公司 | A kind of chromatographic column sampling system |
-
2015
- 2015-12-19 CN CN201521071224.8U patent/CN205340222U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106267893A (en) * | 2016-08-23 | 2017-01-04 | 兆光生物工程(邹平)有限公司 | A kind of moving bed imitation chromatogram separation facility |
| CN106267893B (en) * | 2016-08-23 | 2018-06-29 | 兆光生物工程(邹平)有限公司 | A kind of moving bed imitation chromatogram separation facility |
| CN109283271A (en) * | 2018-10-15 | 2019-01-29 | 兰州东立龙信息技术有限公司 | A kind of chromatographic column sampling system |
| CN109283271B (en) * | 2018-10-15 | 2023-11-03 | 兰州东立龙信息技术有限公司 | Chromatographic column sampling system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160629 Termination date: 20211219 |