CN205024127U - Draw novel device of tyrosine in follow cystine and tyrosine mixture - Google Patents
Draw novel device of tyrosine in follow cystine and tyrosine mixture Download PDFInfo
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- CN205024127U CN205024127U CN201520694540.4U CN201520694540U CN205024127U CN 205024127 U CN205024127 U CN 205024127U CN 201520694540 U CN201520694540 U CN 201520694540U CN 205024127 U CN205024127 U CN 205024127U
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- tyrosine
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- filter
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Abstract
The utility model discloses a draw novel device of tyrosine in follow cystine and tyrosine mixture, the device belong to amino acid production machinery, include: a reation kettle, filter, the 2nd reation kettle, plate filtration machine, neutralizing tank, centrifuge, drying -machine, its characterized in that: be equipped with first shurry pump and pipeline between a reation kettle and filter, be equipped with first conveyer between filter and the 2nd reation kettle, the 2nd reation kettle and plate filtration machine are equipped with second shurry pump and pipeline, be equipped with third shurry pump and pipeline between a plate filtration machine and a reation kettle, be equipped with fourth shurry pump and pipeline between the 2nd reation kettle and neutralizing tank, neutralizing tank and centrifuge are equipped with the 5th shurry pump and pipeline, be equipped with the second conveyer between centrifuge and drying -machine, be equipped with the product outlet on the drying -machine.
Description
Technical field:
The utility model belongs to amino acids production field, particularly relates to a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture.
Background technology:
Tyrosine is amino acid whose one, and finished product is white crystals body or crystalline powder, belongs to human body non-essential amino acid.Tyrosine is the considerable composition of the health constitutive protein matter of people, many milk-product, meat, fish, wheat, oat and comprise tyrosine protein food in containing tyrosine.Tyrosine is of many uses: can be used for medicine, biochemical reagents, foodstuff additive.Produce tyrosine many uses poultry feather acid hydrolyzation, Yi Mushui, Er Mushui, San Mushui is obtained after acidolysis, the technique of traditional production method is as follows: with three female water for raw material, by three female water-neutralization-filtration-alkali molten-filter--neutralization-acid dissolve-decolouring-refine-oven dry-product.Along with the development of science and technology, it is found that traditional technology exists many defects, be mainly manifested in: 1. severe reaction conditions, quality product and yield instability; 2. production environment has ammonia peculiar smell; 3. supplementary material consumption is high, also will use liquid caustic soda.For above-mentioned defect, the utility model is reformed above-mentioned technique, and the novel process of employing is: San Mushui-neutralization-filtration-acid dissolve-neutralization-once decolouring-secondary decolourization--refining-oven dry-product, and the advantage of this technique is: technique is simple, and production cost is low; Do not need to add new installation, and reaction conditions is gentle; Quality product and stable yield, production environment is without ammonia peculiar smell; Supplementary material consumption is low.
Summary of the invention:
Severe reaction conditions is there is in order to overcome traditional technology production tyrosine, quality product and yield instability, production environment has ammonia peculiar smell, the defect that supplementary material consumption is high, the utility model provides a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture, this device is with the first reactor, filter, second reactor, flame filter press, neutralization tank, separating centrifuge, dryer is equipment, with San Mushui, liquefied ammonia, concentration is the hydrochloric acid of 30%, concentration is the hydrochloric acid of 5%, concentration is the ammoniacal liquor of 10%, gac is that raw material is to produce tyrosine.
The technical solution adopted in the utility model is:
From Gelucystine and tyrosine mixture, extract a new device for tyrosine, comprising: the first reactor 1, filter 2, second reactor 3, flame filter press 4, neutralization tank 5, separating centrifuge 6, dryer 7, it is characterized in that: the first reactor 1 is provided with the first material inlet 8, the first shurry pump and pipeline 9 is provided with between the first reactor 1 and filter 2, filter 2 is provided with liquid exit 10, the first transfer roller 11 is provided with between filter 2 and the second reactor 3, second reactor 3 is provided with the second material inlet 12, second reactor 3 and flame filter press 4 are provided with the second shurry pump and pipeline 13, flame filter press 4 is provided with solid outlet 14, the 3rd shurry pump and pipeline 15 is provided with between flame filter press 4 and the first reactor 1, the 4th shurry pump and pipeline 16 is provided with between the second reactor 3 and neutralization tank 5, neutralization tank 5 is provided with the 3rd material inlet 17, neutralization tank 5 and separating centrifuge 6 are provided with the 5th shurry pump and pipeline 18, separating centrifuge 6 is provided with liquid exit 19, second conveyor 20 is provided with between separating centrifuge 6 and dryer 7, dryer 7 is provided with product outlet 21.
Further technical scheme of the present utility model is:
Described first, second, third, fourth, the 5th shurry pump is stainless steel shurry pump, and corresponding pipeline is polyethylene pipe, and the second shurry pump is two-way conveying.
First, second described transfer roller is scraper conveyor.
First, second described reactor is 3 tonnes, ceramic liner.
Described dryer is Vacuumdrier.
The beneficial effects of the utility model are: provide a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture, the advantage of this device is: use general-purpose equipment combination, rational in infrastructure, technique simple and reaction conditions is gentle, quality product and stable yield, production environment is without ammonia peculiar smell, supplementary material consumption is low, can be mass out tyrosine product.
Accompanying drawing illustrates:
If Fig. 1 is Structure and energy FB(flow block) of the present utility model.
Embodiment
The particular content using this new device to extract tyrosine most preferred embodiment from Gelucystine and tyrosine mixture is further illustrated below in conjunction with accompanying drawing:
1. three female water are sent into the first chemical reaction kettle 1 by the first material inlet 8 be arranged on the first chemical reaction kettle 1, adding liquefied ammonia by same import while stirring adjusts the pH value of three female water to be stop after 4.8-5.0 adding liquefied ammonia and stirring, leave standstill and carry out precipitated crystal in 48 hours, then it is sent into filter 2 filter by being arranged at the first shurry pump between the first reactor 1 and filter 2 and pipeline 9, filtrate portion is discharged by the liquid exit 10 be arranged on filter 2 and is reclaimed, filter cake part sends into the second chemical reaction kettle 3 by the first transfer roller 11 be arranged between filter 2 and the second reactor 3.
2. in the second chemical reaction kettle 3, add the hydrochloric acid that concentration is 30% by the second material inlet 12 be arranged on the second chemical reaction kettle 3, quantity is 4 times of filter cake weight, be heated to 60 DEG C while stirring, gac is added by same import after filter cake all dissolves, quantity is 0.3 times of filter cake weight, stir decolouring to stop after 1 hour stirring, stirring liquid is sent into flame filter press 4 by the second shurry pump and pipeline 13 being arranged at the second reactor 3 and flame filter press 4 filter, the filter cake obtained is discharged by the solid outlet 14 be arranged on flame filter press 4 and is reclaimed, the filtrate obtained is by being arranged at the 3rd shurry pump between flame filter press 4 and the first reactor 1 and the first chemical reaction kettle 1 sent back to by pipeline 15.
3. added when the pH value of filtrate is adjusted to 2.0 by liquefied ammonia in the first chemical reaction kettle 1 by the first material inlet 8 be arranged on the first chemical reaction kettle 1 and obtain solidliquid mixture, solidliquid mixture is sent into filter 2 filter by being arranged at the first shurry pump between the first reactor 1 and filter 2 and pipeline 9, filtrate is discharged by the liquid exit 10 be arranged on filter 2 and is reclaimed, filter cake sends into the second reactor 3 by the first transfer roller 11 be arranged between filter 2 and the second reactor 3, by the second material inlet 12 be arranged on the second reactor 3 to add quantity be the concentration of filter cake weight 4.5 times be 5% hydrochloric acid be stirred to filter cake and dissolve, the gac stirring decolouring of filter cake weight 0.15 times is added after 2 hours again by same import, mixture in still is sent into flame filter press 4 filter by being arranged at the second shurry pump between the second reactor 3 and flame filter press 4 and pipeline 13, filter cake is discharged by the solid outlet 14 be arranged on flame filter press 4 and is reclaimed, filtrate is by being arranged at the second reactor 3 and flame filter press 4 is provided with the second shurry pump and the second chemical reaction kettle 3 sent back to by pipeline 13.
4. in the second chemical reaction kettle 3, the gac of filtrate weight 0.10 times is added by the second material inlet 12 be arranged on the second chemical reaction kettle, and adjust temperature in the kettle to be 65 DEG C, to stir it after 1 hour by being arranged at the 4th shurry pump between the second reactor 3 and neutralization tank 5 and neutralization tank 5 sent into by pipeline 16, by in neutralization tank 5 during liquid heat to 50 DEG C, the ammoniacal liquor that concentration is 10% is added while stirring by the 3rd material inlet be arranged on neutralization tank 5, the pH adjusting liquid in tank is 2.5, stop heating up, after cooling to normal temperature by solidliquid mixture in tank by being arranged at the 5th shurry pump between neutralization tank 5 and separating centrifuge 6 and separating centrifuge 6 centrifugation sent into by pipeline 18, the liquid portion obtained is discharged by the liquid exit 19 be arranged on separating centrifuge 6 and is reclaimed, solid part sends into dryer 7 by the second conveyor 20 be arranged between separating centrifuge 6 and dryer 7 dries obtain finished product after moisture is less than 0.2% at the temperature of 90 DEG C, finished product is by being arranged at product outlet 21 discharging on dryer 7.
Certainly, the utility model also has other embodiment, not leaving the improvement of any technology, principle and the technique done under spiritual background of the present utility model, all drops within protection domain of the present utility model.
Claims (5)
1. from Gelucystine and tyrosine mixture, extract a new device for tyrosine, comprising: the first reactor (1), filter (2), the second reactor (3), flame filter press (4), neutralization tank (5), separating centrifuge (6), dryer (7), it is characterized in that: the first reactor (1) is provided with the first material inlet (8), the first shurry pump and pipeline (9) is provided with between the first reactor (1) and filter (2), filter (2) is provided with liquid exit (10), the first transfer roller (11) is provided with between filter (2) and the second reactor (3), second reactor (3) is provided with the second material inlet (12), second reactor (3) and flame filter press (4) are provided with the second shurry pump and pipeline (13), flame filter press (4) is provided with solid outlet (14), the 3rd shurry pump and pipeline (15) is provided with between flame filter press (4) and the first reactor (1), the 4th shurry pump and pipeline (16) is provided with between the second reactor (3) and neutralization tank (5), neutralization tank (5) is provided with the 3rd material inlet (17), neutralization tank (5) and separating centrifuge (6) are provided with the 5th shurry pump and pipeline (18), separating centrifuge (6) is provided with liquid exit (19), second conveyor (20) is provided with between separating centrifuge (6) and dryer (7), dryer (7) is provided with product outlet (21).
2. a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture as claimed in claim 1, it is characterized in that: described first, second, third, fourth, the 5th shurry pump is stainless steel shurry pump, corresponding pipeline is polyethylene pipe, and the second shurry pump is two-way conveying.
3. a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture as claimed in claim 1, is characterized in that: first, second described transfer roller is scraper conveyor.
4. a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture as claimed in claim 1, is characterized in that: first, second described reactor is 3 tonnes, ceramic liner.
5. a kind of new device extracting tyrosine from Gelucystine and tyrosine mixture as claimed in claim 1, is characterized in that: described dryer is Vacuumdrier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520694540.4U CN205024127U (en) | 2015-09-10 | 2015-09-10 | Draw novel device of tyrosine in follow cystine and tyrosine mixture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520694540.4U CN205024127U (en) | 2015-09-10 | 2015-09-10 | Draw novel device of tyrosine in follow cystine and tyrosine mixture |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205024127U true CN205024127U (en) | 2016-02-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520694540.4U Expired - Fee Related CN205024127U (en) | 2015-09-10 | 2015-09-10 | Draw novel device of tyrosine in follow cystine and tyrosine mixture |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205024127U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106010940A (en) * | 2016-06-30 | 2016-10-12 | 宜兴市前成生物有限公司 | Production system of aspartic acid |
-
2015
- 2015-09-10 CN CN201520694540.4U patent/CN205024127U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106010940A (en) * | 2016-06-30 | 2016-10-12 | 宜兴市前成生物有限公司 | Production system of aspartic acid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160210 Termination date: 20190910 |