CN101744115A - Feed additive and preparation method thereof - Google Patents
Feed additive and preparation method thereof Download PDFInfo
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- CN101744115A CN101744115A CN200810237790A CN200810237790A CN101744115A CN 101744115 A CN101744115 A CN 101744115A CN 200810237790 A CN200810237790 A CN 200810237790A CN 200810237790 A CN200810237790 A CN 200810237790A CN 101744115 A CN101744115 A CN 101744115A
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- feed addictive
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- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000003674 animal food additive Substances 0.000 title claims abstract description 9
- 241001465754 Metazoa Species 0.000 claims abstract description 18
- 235000021120 animal protein Nutrition 0.000 claims abstract description 15
- 239000002734 clay mineral Substances 0.000 claims abstract description 14
- 229920001661 Chitosan Polymers 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 4
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 claims description 13
- 229920001287 Chondroitin sulfate Polymers 0.000 claims description 13
- 229940059329 chondroitin sulfate Drugs 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- 239000002351 wastewater Substances 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 229910000278 bentonite Inorganic materials 0.000 claims description 7
- 229940092782 bentonite Drugs 0.000 claims description 7
- 239000000440 bentonite Substances 0.000 claims description 7
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- 238000013019 agitation Methods 0.000 claims description 6
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 6
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 6
- 239000013049 sediment Substances 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- 239000004411 aluminium Substances 0.000 claims description 4
- 210000000988 bone and bone Anatomy 0.000 claims description 4
- 229940036811 bone meal Drugs 0.000 claims description 4
- 239000002374 bone meal Substances 0.000 claims description 4
- 102000004196 processed proteins & peptides Human genes 0.000 claims description 4
- 108090000765 processed proteins & peptides Proteins 0.000 claims description 4
- -1 compound amino acid Chemical class 0.000 claims description 3
- ONCZQWJXONKSMM-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4].[Si+4].[Si+4].[Si+4] ONCZQWJXONKSMM-UHFFFAOYSA-N 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 229940080314 sodium bentonite Drugs 0.000 claims description 3
- 229910000280 sodium bentonite Inorganic materials 0.000 claims description 3
- 239000006228 supernatant Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 2
- 229920001184 polypeptide Polymers 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims description 2
- 239000000126 substance Substances 0.000 abstract description 5
- 231100000957 no side effect Toxicity 0.000 abstract description 2
- 239000010865 sewage Substances 0.000 abstract description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 235000021049 nutrient content Nutrition 0.000 abstract 1
- 150000004684 trihydrates Chemical class 0.000 abstract 1
- 239000000047 product Substances 0.000 description 10
- 235000019733 Fish meal Nutrition 0.000 description 7
- 239000004467 fishmeal Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 5
- 210000001519 tissue Anatomy 0.000 description 5
- 241000287828 Gallus gallus Species 0.000 description 4
- 238000007599 discharging Methods 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 3
- 210000000845 cartilage Anatomy 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 235000018102 proteins Nutrition 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 210000002435 tendon Anatomy 0.000 description 3
- 230000002792 vascular Effects 0.000 description 3
- 238000011109 contamination Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 210000003746 feather Anatomy 0.000 description 2
- 239000004459 forage Substances 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000004083 survival effect Effects 0.000 description 2
- 241000251730 Chondrichthyes Species 0.000 description 1
- 208000021017 Weight Gain Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 230000003031 feeding effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000002207 metabolite Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000021590 normal diet Nutrition 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 230000004584 weight gain Effects 0.000 description 1
- 235000019786 weight gain Nutrition 0.000 description 1
Landscapes
- Fodder In General (AREA)
- Feed For Specific Animals (AREA)
Abstract
The invention discloses a feed additive and a preparation method thereof. The feed additive is prepared by the following components in percentage by weight: 40 to 70 percent of animal protein, 10 to 20 percent of clay minerals, 0.5 to 1 percent of chitosan, 0.1 to 1 percent of trihydrate alumina and the balance accessory materials. The invention provides the feed additive and the preparation method thereof, wherein the feed additive is rich of animal protein, has no side effect on eating animal bodies and has no residual. The invention solves the problems of chemical composition residual and single nutrient content of the existing feed, is favorable for improving the environment, and can reduce the sewage discharge.
Description
Technical field
The present invention relates to the feed addictive industrial circle, specifically a kind of feed addictive that is rich in animal protein and preparation method thereof.
Background technology
In recent years, along with China's animal husbandry develop rapidly and to the increase day by day of feed protein requirement, the development of feed industry and production also progressively present highly intensification, a large amount of chemical substances are widely used with disease preventing and treating, promote growth of animal and improve the animal product quality as feed addictive, its result often brings the problem of two aspects: the one, and the residue problem of exogenous chemical in animal foodstuff is more and more heavier, thereby human health and public health have been constituted very big threat, reached " egg incident " etc. as " milk powder case " of recent outburst; Be after chemical substance enters in the animal body on the other hand, most of form with original shape or metabolite enters environment with ight soil and urine, severe contamination ecological environment.The feed addictive of research and development high-efficiency environment friendly is the inexorable trend of modern feed advance, also is the powerful guarantee that promotes feed industry, animal husbandry benign development.
For a long time, China's protein resource is the animal protein wretched insufficiency particularly, mainly substitutes by imported fish meal.Yet, because the imported product cost is higher and can't guarantee timely supply, add reasons such as nutritional labeling is single, imported fish meal is at feedstuff industry and fall from favor, and the substitute is cheap feather meal.Yet, although the feather meal protein content up to more than 80%, wherein the overwhelming majority is a keratoprotein, often is difficult for behind the animal edible being absorbed and digesting, and makes feeding effect obviously descend.Exploitation be rich in several amino acids and the feed addictive that easily absorbed by animal imperative.
Chondroitin sulfate is distributed widely in the tissue of humans and animals, is the part that constitutes tissues such as animal cartilage, tendon, vascular wall, skin, has high medical value.At " application of chitosan flocculant in the chondroitin sulfate wastewater treatment " (Ding Xinghua, Zhao Xirong.2007, Guangxi light industry, 9 (106), introduced 89-90) about from become tissues such as animal cartilage, tendon, vascular wall, skin, extracting the production method of chondroitin sulfate, generally to discharge the waste water that contains grease, meat mincing and solubility small-molecular peptides, amino acid type organic in a large number in the process of this method generation chondroitin sulfate, if this direct discharging of waste water not only can cause the huge wasting of resources, but also pollutes the environment.
Summary of the invention
The purpose of this invention is to provide a kind of be rich in animal protein and to the edible animal body have no side effect, the feed addictive of noresidue and preparation method thereof, to overcome the problem that chemical composition is residual and nutritional labeling is single in the existing feed, and help improving environment, reduce sewage discharge.
In order to address the above problem, the present invention has taked following technical scheme:
A kind of feed addictive, by weight percentage, its composition is: animal protein 40%～70%, clay mineral 10%～20%, shitosan 0.5%～1%, aluminium hydroxide 0.1%～1%, all the other are auxiliary material.
Animal protein is compound amino acid and the polypeptide in the chondroitin sulfate factory effluent;
The activated clay mineral are bentonite or diatomite, and bentonite is calcium-base bentonite or sodium bentonite;
Auxiliary material is an animal bones bone meal;
The preparation method of described feed addictive, its step is as follows:
1) umber meter by volume, the chondroitin sulfate factory effluent (protein content is about 10%) of getting 10 parts is transferred in the container, and the pH that regulates waste water with watery hydrochloric acid is 4～10, makes solution I;
2) 1～5 part clay mineral solution is joined the above-mentioned solution I that modulates, continue to stir 10 minutes, make solution II;
3) solution II that obtains under agitation being added mass percent is 0.5～1.5% chitosan solution, continues to stir 3～5 minutes, and making the concentration of shitosan in solution is 500～1000mg/L, makes solution III;
4) solution III that obtains is under agitation added the flocculant of mass percent 1～10%, continue to stir 1～3 minute, make solution IV, wherein the concentration of flocculant in solution is 300～800mg/L;
5) solution IV that obtains was left standstill 1～3 hour, abandoning supernatant, filter sediment;
6) oven dry of gained sediment, pulverizing, packing can be obtained the animal protein feed additive.
The pH that watery hydrochloric acid is regulated waste water is 4.5～8.5, makes the isoelectric point of solution acid alkalinity near the compound amino acid precipitation;
Described chitosan solution is that 1～2 gram shitosan powder is added the 100ml mass concentration is that 2% acetic acid solution fully dissolves and makes;
Flocculant is aluminium polychloride, PAFC or PAFS, is hydrolyzed to aluminium hydroxide in solution;
Described clay mineral solution is that to join volume be that 10～50ml, temperature are that stirring makes in 30～60 ℃ the water to 3～5 gram clay minerals.
Compared with prior art, the present invention has following advantage:
Chondroitin sulfate is distributed widely in the tissue of humans and animals, is the part that constitutes tissues such as animal cartilage, tendon, vascular wall, skin, has high medical value.The present invention is exactly a large amount of waste water that utilize the discharging of the production process of chondroitin sulfate, and it wherein contains grease, meat mincing and organic matters such as solubility small-molecular peptides, amino acids, is good animal protein source; And if this direct discharging of waste water not only can cause the huge wasting of resources, but also can cause environmental pollution.
Not only raw material sources are extensive so the present invention utilizes chondroitin sulfate waste water to make the animals ' protein forage additive, and are cheap, and also solved the severe contamination that the discharging of high concentrated organic wastewater causes environment simultaneously.
The invention solves the environmental pollution that chondroitin sulfate waste water is caused, developed living resources simultaneously, promoted the development of feed industry and aquaculture, realize the green feed additive of safety, noresidue, pollution-free, easy absorption.
The specific embodiment
Embodiment 1: feed addictive
Animal protein 70%, calcium-base bentonite 8%, shitosan 1.5%, aluminium hydroxide 0.5%, all the other are chicken frame bone bone meal.
Embodiment 2: feed addictive
Animal protein 40%, sodium bentonite 15%, shitosan 0.5%, aluminium hydroxide 1.0%, all the other are shark bone bone meal.
Embodiment 3: the preparation method of feed addictive
1) get 100L chondroitin sulfate factory effluent and be transferred in the reactor, the pH that regulates waste water with watery hydrochloric acid is 6.5, makes solution I;
2) 4.5 kilograms of clay minerals being joined volume is that 30L, temperature are in 50 ℃ the water, stirs the clay mineral solution of furnishing pasty state, then the clay mineral solution that obtains is joined the above-mentioned solution I that modulates, and continues to stir 10 minutes, makes solution II;
3) solution II that obtains under agitation being added mass percent is 1% chitosan solution, continues to stir 3 minutes, and making the concentration of shitosan in solution is 1000mg/L, makes solution III;
4) solution III that obtains is under agitation added the flocculant of mass percent 8%, continue to stir 3 minutes, make solution IV, wherein the concentration of aluminium polychloride in solution is 500mg/L, and aluminium polychloride is hydrolyzed to aluminium hydroxide in solution;
5) solution IV that obtains was left standstill 2 hours, abandoning supernatant, filter sediment;
6) oven dry of gained sediment, pulverizing, packing can be obtained the animal protein feed additive.
Embodiment 4: feeding dorking
This product with 3% (mass percent in the feed total amount) in feed replaces the imported fish meal of equivalent to feed fryer, in chick stage, add every day and feed part this product, the per kilogram feed product can make 0.65 kilogram of chick weight gains, can rise in value about 2 yuan 2.15 kilograms/of average weightening finishes in 60 days, 1.52 kilograms/of normal diet group average weightening finishes in 60 days, 0.038 kilogram/of the per day weightening finish of this feed addictive group of feeding, survival rate improves 8-13%, and the material anharmonic ratio reduces by 0.4.Add up to 2.8 yuan of about additional incomes/only.
Embodiment 5: the laying hen of feeding
This product that adds 8% (mass percent in the feed total amount) in feed replaces the imported fish meal of equivalent to feed laying hen, and the difference on effect that the quality of its laying rate, egg and the price of deed and whole fish meal are fed laying hen is not remarkable.Under the identical situation of other conditionally complete, this product with 10% is fed laying hen and is compared with the fish meal nursing laying hen with 10%, the laying rate of feeding this product group improves 18.3% than feeding fish meal group group, and price of deed rate improves 14.9%, every chicken additional income 70.8%.Under the identical condition of basal feed, every chicken adds hello 10 these products of gram, after feeding 110 days, egg production increases by 319 pieces, increases weight 22.3 kilograms, laying rate improves 9.3%, per kilogram egg feed consumption reduces 0.39 kilogram, saves 56.13 kilograms in feed, and average per 1.3 kilograms of these products just can increase production 1 kilogram of egg, and chicken is few sick, and survival rate is than cooperating the high by 18% of forage feed.
Claims (10)
1. feed addictive, it is characterized in that: by weight percentage, its composition is: animal protein 40%～70%, clay mineral 10%～20%, shitosan 0.5%～1%, aluminium hydroxide 0.1%～1%, all the other are auxiliary material.
2. feed addictive according to claim 1 is characterized in that: animal protein is compound amino acid and the polypeptide in the chondroitin sulfate factory effluent.
3. feed addictive according to claim 1 is characterized in that: the activated clay mineral are bentonite or diatomite.
4. feed addictive according to claim 3 is characterized in that: bentonite is calcium-base bentonite or sodium bentonite.
5. feed addictive according to claim 1 is characterized in that: auxiliary material is an animal bones bone meal.
6. the preparation method of a feed addictive as claimed in claim 1, its step is as follows:
1) umber meter by volume, the chondroitin sulfate factory effluent of getting 10 parts is transferred in the container, and the pH that regulates waste water with watery hydrochloric acid is 4～10, makes solution I;
2) 1～5 part clay mineral solution is joined the above-mentioned solution I that modulates, continue to stir 10 minutes, make solution II;
3) solution II that obtains under agitation being added mass percent is 0.5～1.5% chitosan solution, continues to stir 3～5 minutes, and making the concentration of shitosan in solution is 500～1000mg/L, makes solution III;
4) solution III that obtains is under agitation added the flocculant of mass percent 1～10%, continue to stir 1～3 minute, make solution IV, wherein the concentration of flocculant in solution is 300～800mg/L;
5) solution IV that obtains was left standstill 1～3 hour, abandoning supernatant, filter sediment;
6) oven dry of gained sediment, pulverizing, packing can be obtained the animal protein feed additive.
7. the preparation method of feed addictive according to claim 6 is characterized in that: the pH that watery hydrochloric acid is regulated waste water is 4.5～8.5.
8. the preparation method of feed addictive according to claim 6 is characterized in that: described chitosan solution is that 1～2 gram shitosan powder is added the 100ml mass concentration is that 2% acetic acid solution fully dissolves and makes.
9. the preparation method of feed addictive according to claim 6, it is characterized in that: flocculant is aluminium polychloride, PAFC or PAFS.
10. the preparation method of feed addictive according to claim 6 is characterized in that: described clay mineral solution is that to join volume be that 10～50ml, temperature are that stirring makes in 30～60 ℃ the water to 3～5 gram clay minerals.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810237790 CN101744115B (en) | 2008-12-05 | 2008-12-05 | Feed additive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810237790 CN101744115B (en) | 2008-12-05 | 2008-12-05 | Feed additive and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101744115A true CN101744115A (en) | 2010-06-23 |
| CN101744115B CN101744115B (en) | 2013-09-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200810237790 Active CN101744115B (en) | 2008-12-05 | 2008-12-05 | Feed additive and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN101744115B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101979634A (en) * | 2010-09-26 | 2011-02-23 | 许累峰 | Method for preparing fermentation nitrogen source from chondroitin sulfate production waste water |
| CN102687817A (en) * | 2012-06-15 | 2012-09-26 | 徐州金利饲料厂 | Meat duck feed |
| CN104276687A (en) * | 2013-09-10 | 2015-01-14 | 徐磊 | System and method for recycling animal protein feed from casing processing waste liquid |
-
2008
- 2008-12-05 CN CN 200810237790 patent/CN101744115B/en active Active
Non-Patent Citations (1)
| Title |
|---|
| 丁兴华 等: "壳聚糖絮凝剂在硫酸软骨素废水处理中的应用", 《广西轻工业》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101979634A (en) * | 2010-09-26 | 2011-02-23 | 许累峰 | Method for preparing fermentation nitrogen source from chondroitin sulfate production waste water |
| CN101979634B (en) * | 2010-09-26 | 2012-10-03 | 许累峰 | Method for preparing fermentation nitrogen source from chondroitin sulfate production waste water |
| CN102687817A (en) * | 2012-06-15 | 2012-09-26 | 徐州金利饲料厂 | Meat duck feed |
| CN102687817B (en) * | 2012-06-15 | 2013-09-25 | 徐州金利饲料厂 | Meat duck feed |
| CN104276687A (en) * | 2013-09-10 | 2015-01-14 | 徐磊 | System and method for recycling animal protein feed from casing processing waste liquid |
| CN104276687B (en) * | 2013-09-10 | 2016-08-17 | 徐磊 | A kind of method of animal protein feed in recycling casing processing-waste |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101744115B (en) | 2013-09-18 |
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Effective date of registration: 20210601 Address after: 265141 resident Industrial Park, Xujiadian Town, Haiyang City, Yantai City, Shandong Province Patentee after: Yantai jinrunda animal nutrition Co.,Ltd. Address before: No.17 Chunhui Road, Yantai City, Shandong Province 264003 Patentee before: YANTAI INSTITUTE OF COASTAL ZONE RESEARCH, CHINESE ACADEMY OF SCIENCES |
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Denomination of invention: A feed additive and its preparation method Effective date of registration: 20221230 Granted publication date: 20130918 Pledgee: Postal Savings Bank of China Limited Haiyang sub branch Pledgor: Yantai jinrunda animal nutrition Co.,Ltd. Registration number: Y2022980029775 |