CN205020084U - Electroplate intelligent production system of additive - Google Patents
Electroplate intelligent production system of additive Download PDFInfo
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- CN205020084U CN205020084U CN201520769420.6U CN201520769420U CN205020084U CN 205020084 U CN205020084 U CN 205020084U CN 201520769420 U CN201520769420 U CN 201520769420U CN 205020084 U CN205020084 U CN 205020084U
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- reactor
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- circulation line
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Abstract
The utility model relates to an electroplate intelligent production system of additive mainly includes reation kettle, charge -in system, ejection of compact system, heating system, distillation condensing equipment and controller, charge -in system, ejection of compact system, heating system, distillation condensing equipment are connected with the controller respectively, reation kettle includes feed inlet, discharge gate, the cauldron body, kettle cover, agitator, drive mechanism and sealing device, charge -in system includes storage bucket, feeding pipe, flowmeter and solenoid valve, charge -in system connects the reation kettle feed inlet, ejection of compact headtotail reation kettle discharge gate, heating system is conduction oil heating system, the heat conduction oil circulation pipeline sets up two, and one sets up in reactor inner wall, and one sets up in reation kettle and to be close to (mixing) shaft department, distillation condensing equipment connects reation kettle upper portion. The utility model has the advantages of can the accurate control material flow of business turn over, can solve the inhomogeneous problem of temperature in the reation kettle simultaneously.
Description
Technical field
The present invention relates to electroplating additive production equipment field, particularly relate to a kind of intellectualized production system of electroplating additive.
Background technology
The electroplating additive that general company produces is various in style, the raw material of often kind of additive more than at least 5 kinds, there are solid, semisolid and liquid, raw material may react disposable all adding, also likely gradation progressively adds in batches, and material addition, reaction temperature etc. all can have an impact to the properties of product of electroplating additive.Electroplating additive performance is assessed by its physical and chemical indexes.And the product physical and chemical indexes of often kind of additive differs, product can through flow processs such as production → initial survey → reinspection → examination → warehouse-ins, the outward appearance, pH, index of refraction, proportion etc. of Quality Control portion to product carry out detection qualified after, could check and accepting storing.If production process can be monitored the index such as temperature, pH, then products obtained therefrom performance is more stable, and quality is better.Usually need heating during additive synthesis, make temperature keep carrying out reaction for a long time within the specific limits to obtain additive product of good performance.
Traditional electroplating additive produces the mode adopting Artificial Control material addition, by technical staff subjective judgement whether charging complete and manual unlocking or close charging basket valve, this is unfavorable for the precision that material adds very much, be easy to produce harmful effect to the properties of product of electroplating additive, and need to detect in real time PH index, not only need to increase PH checkout gear in addition, also need to carry out follow-up adjustment according to detected value, waste time and energy.Also conduction oil reactor is used to heat in traditional method, but a circulation line is only set usually, the unbalanced situation of reaction temperature will be caused like this, local temperature near conduction oil circulation line is high, and heart position in a kettle., especially lower near shaft place temperature, easily harmful effect is caused to electroplating additive performance.These problems are especially outstanding in the preparation process to material addition and the very responsive electroplating additive of reaction temperature.
Utility model content
In order to solve the problems of the technologies described above, provide that a kind of material adds accurately, reaction temperature evenly and the higher electroplating additive production system of automaticity, the utility model provides following technical scheme:
A kind of intellectualized production system of electroplating additive, mainly comprise reactor, feed system, discharge system, heating system, distillation condensing unit and controller, described feed system, discharge system, heating system, distillation condensing unit are connected with reactor and controller respectively;
Described reactor comprises charging aperture, discharging opening, kettle, kettle cover, agitator, transmission mechanism and sealing device, described charging aperture is arranged at kettle cover top, described discharging opening is arranged at kettle bottom, described agitator comprises the shaft be vertically installed in reactor and the impeller type stirring blade being arranged on shaft bottom, described transmission mechanism comprises motor and speed reducer, described transmission mechanism connects shaft, and described kettle is connected by sealing device with kettle cover;
Described feed system comprises several charging baskets, feeding pipe, flowmeter one and magnetic valve one, described feeding pipe comprises charging branch pipeline and charging main line, described charging branch pipeline is all connected with charging main line, described some charging baskets are connected to independently charging branch pipeline separately, and by charging main line coupled reaction still charging aperture, described flowmeter one is arranged on charging main line, and described magnetic valve one is arranged on charging main line, and is positioned at below flowmeter one; Described flowmeter one and magnetic valve one are all connected to controller, data on flows in pipeline is flowed to controller by described flowmeter one, described controller carries out switch control rule to rear to magnetic valve one according to flow-rate ratio, described feed system is positioned at above reactor, and utilize difference in height to carry out the conveying of material, can control accurately material addition and not need manual intervention;
Described discharge system comprises discharging pipeline, flowmeter two, magnetic valve two, material storing tank, described discharging pipeline coupled reaction still discharging opening, described discharging pipeline is provided with flowmeter two and magnetic valve two, described flowmeter two and magnetic valve two be connection control device respectively, and the data that described controller returns according to flowmeter two carry out switch control rule in conjunction with the capacity of material storage tank to magnetic valve;
Described heating system is heat-conducting oil heating system, mainly comprise electric heater, oil cylinder, circulating pump and circulation line, described electric heater connects oil cylinder, for the heating of conduction oil, described circulating pump connects oil cylinder and circulation line, for conduction oil is pumped in circulation line, described conduction oil circulation line arranges two, circulation line one is arranged at reactor inwall, circulation line two is arranged in reactor near shaft place, a bracing or strutting arrangement is also provided with below described circulation line two, for increasing the stability of circulation line two, described distillation condensing unit coupled reaction still top.The uniformity of reaction temperature can must be ensured to greatest extent by arranging two conduction oil circulation lines.
Further, described circulation line one and two includes oil pipe, oil-in and oil-out, the oil-in of described circulation line one is arranged at reactor top, oil-out is arranged at reactor bottom, the oil-in of described circulation line two is arranged at reactor bottom, and oil-out is arranged at reactor top.Because the temperature at oil-in place is a little more than the temperature at oil-out place, therefore reactor top and the bottom are also easily caused to there is temperature difference, so the oil-in one of two conduction oil circulation lines is on top, one, in bottom, further can ensure that in still, top and the bottom temperature is consistent like this.
Further, outside described reactor kettle, be also enclosed with heat-insulation layer, be conducive to the utilization ratio improving heat energy.
Further, described heat-insulation layer is the lamination layer structure of at least one deck rubber-plastic sponge, felt, aluminium foil, good heat insulating.
Further, also comprise a device for detecting temperature, described device for detecting temperature is arranged between two circulation lines, described device for detecting temperature connection control device, be conducive to Real-Time Monitoring reaction temperature, controller controls heating system according to the temperature of device for detecting temperature.
Further, described reactor kettle cover is also provided with Manual material feeding mouth, when needing to add certain a small amount of material, the mode of Manual material feeding can be adopted, one is the use that can reduce charging basket, flowmeter, magnetic valve, save cost, two is when addition is little, and the precision due to flowmeter can be avoided to cause the inaccurate of material addition.
Further, described bracing or strutting arrangement is a four-point supporting device, and four angle seats of described bracing or strutting arrangement are connected with reactor autoclave body bottom by bolt, gasket seal.For increasing the stability of circulation line two, and detachably.
The beneficial effects of the utility model are:
(1), material addition control accuracy is high, can avoid the subjective error in conventional method;
(2), reactor outside, top and the bottom uniformity of temperature profile inside;
(3), because material addition is accurate, the pH value detecting unit in traditional scheme can be reduced, reduce costs and system complexity;
(4), due to high to material addition, reaction temperature control accuracy, the physical and chemical performance of electroplating additive can be improved, even can reach the performance indications of laboratory-scale.
Accompanying drawing explanation
Fig. 1, primary structure schematic diagram of the present utility model
Fig. 2, system block diagram of the present utility model
The structural representation of Fig. 3, bracing or strutting arrangement of the present utility model
In figure: 1, reactor, 11, charging aperture, 12, discharging opening, 13, kettle, 14, kettle cover, 15, agitator, 151, shaft, 152, paddle, 161, motor, 162, decelerator, 2, feed system, 21, charging basket, 22, feeding pipe, 221, charging branch pipeline, 222, charging main line, 23, flowmeter one, 24, magnetic valve one, 3, discharge system, 31, discharging pipeline, 32, flowmeter two, 33, magnetic valve two, 34, material storing tank, 4, heating system, 41, electric heater, 42, oil cylinder, 43, circulating pump, 441, circulation line one, 442, circulation line two, A, oil-in, B, oil-out, 5, distillation condensing unit, 6, controller, 7, heat-insulation layer, 8, device for detecting temperature, 9, Manual material feeding mouth, 100, bracing or strutting arrangement, 101, angle seat
Detailed description of the invention
The technical solution of the utility model is further illustrated for nickel plating brightener.
The intellectualized production system of nickel plating brightener, mainly comprise reactor 1, feed system 2, discharge system 3, heating system 4, distillation condensing unit 5 and controller 6, described feed system 2, discharge system 3, heating system 4, distillation condensing unit 5 are connected with reactor 1 and controller 6 respectively;
Described reactor 1 comprises charging aperture 11, discharging opening 12, kettle 13, kettle cover 14, agitator 15, transmission mechanism and sealing device 17, described charging aperture 11 is arranged at kettle cover 13 top, described discharging opening 12 is arranged at kettle 13 bottom, described agitator 15 comprises the shaft 151 be vertically installed in reactor 1 and the impeller type stirring blade 152 being arranged on shaft bottom, described transmission mechanism comprises motor 161 and reductor 162, described transmission mechanism connects shaft 151, and described kettle 13 is connected by sealing device 17 with kettle cover 14;
Described feed system 2 comprises 5 charging baskets 21, article 5, charging branch pipeline 221, flowmeter 1 and magnetic valve 1, described 5 charging baskets 21 are equipped with DL-METHIONINE respectively, glycine, alanine, cystine, phytic acid, described charging basket 21 is connected to independently charging branch pipeline 221 separately, described charging branch pipeline 221 connects charging main line 222, and by charging main line 222 coupled reaction still charging aperture 11, described flowmeter 1 is arranged on charging main line 222, described magnetic valve 1 is arranged on charging main line 222, and be positioned at below flowmeter 1, described flowmeter 1 and magnetic valve 1 are all connected to controller 6, data on flows in pipeline is flowed to controller 6 by described flowmeter 1, described controller 6 carries out switch control rule to rear to magnetic valve 1 according to flow-rate ratio, described feed system 2 is positioned at above reactor 1, and utilize difference in height to carry out the conveying of material, can control accurately material addition and not need manual intervention, described reactor kettle cover 14 is also provided with Manual material feeding mouth 9, when needing to add certain a small amount of material, the mode of Manual material feeding can be adopted, one is the use that can reduce charging basket, flowmeter, magnetic valve, save cost, two is when addition is little, and the precision due to flowmeter can be avoided to cause the inaccurate of material addition, and the agent that walks of nicotinic acid in the present embodiment, low unit is added by Manual material feeding mouth 9 after weighing.Also need in the present embodiment to add a large amount of water, can be extracted by suction pump.
Described discharge system 3 comprises discharging pipeline 31, flowmeter 2 32, magnetic valve 2 33, material storing tank 34, described discharging pipeline 31 coupled reaction still discharging opening 12, described discharging pipeline 31 is provided with flowmeter 2 32 and magnetic valve 2 33, described flowmeter 2 32 and magnetic valve 2 33 be connection control device 6 respectively, and the data that described controller 6 returns according to flowmeter 2 32 carry out switch control rule in conjunction with the capacity of material storage tank 34 to magnetic valve 2 33;
Described heating system 4 is heat-conducting oil heating system, mainly comprise electric heater 41, oil cylinder 42, circulating pump 43 and circulation line, described electric heater 41 connects oil cylinder 42, for the heating of conduction oil, described circulating pump 43 connects oil cylinder 42 and circulation line, for conduction oil is pumped in circulation line, described conduction oil circulation line arranges two, circulation line 1 is arranged at reactor 1 inwall, circulation line 2 442 is arranged in reactor 1 near shaft 151 place, a bracing or strutting arrangement 100 is also provided with below described circulation line 2 442, described bracing or strutting arrangement 100 is a four-point supporting device, four angle seats 101 of described bracing or strutting arrangement 100 pass through bolt, gasket seal is connected with reactor autoclave body bottom, described distillation condensing unit 5 coupled reaction still 1 top.The uniformity of reaction temperature can must be ensured to greatest extent by arranging two conduction oil circulation lines.
Described circulation line one 441 and 2 442 includes oil pipe, oil-in A and oil-out B, the oil-in A of described circulation line 1 is arranged at reactor 1 top, oil-out B is arranged at reactor 1 bottom, the oil-in A of described circulation line 2 442 is arranged at reactor 1 bottom, and oil-out B is arranged at reactor 1 top.Because the temperature at oil-in A place is a little more than the temperature at oil-out B place, therefore reactor top and the bottom are also easily caused to there is temperature difference, so the oil-in one of two conduction oil circulation lines is on top, one, in bottom, further can ensure that in still, top and the bottom temperature is consistent like this.Also be enclosed with rubber-plastic sponge outside described reactor kettle, heat-insulation layer 7 that felt, aluminium foil are composited, be conducive to the utilization ratio improving heat energy.
Also comprise a device for detecting temperature 8, described device for detecting temperature 8 is arranged between two circulation lines, described device for detecting temperature 8 connection control device 6, be conducive to Real-Time Monitoring reaction temperature, controller 6 controls heating system according to the temperature of device for detecting temperature 8.
Adopt the nickel plating brightener that production system of the present utility model is produced, bright performance is high and lasting, the heat endurance of brightener own and chemical stability good.
With above-mentioned foundation the utility model desirable embodiment for enlightenment, by above-mentioned description, relevant staff in the scope not departing from this utility model technological thought, can carry out various change and amendment completely.This uses novel technical scope to be not limited to content on description, must determine its technical scope according to right.
Claims (7)
1. the intellectualized production system of an electroplating additive, it is characterized in that: mainly comprise reactor, feed system, discharge system, heating system, distillation condensing unit and controller, described feed system, discharge system, heating system, distillation condensing unit are connected with reactor and controller respectively;
Described reactor comprises charging aperture, discharging opening, kettle, kettle cover, agitator, transmission mechanism and sealing device, described charging aperture is arranged at kettle cover top, described discharging opening is arranged at kettle bottom, described agitator comprises the shaft be vertically installed in reactor and the impeller type stirring blade being arranged on shaft bottom, described transmission mechanism comprises motor and speed reducer, described transmission mechanism connects shaft, and described kettle is connected by sealing device with kettle cover;
Described feed system comprises several charging baskets, feeding pipe, flowmeter one and magnetic valve one, described feeding pipe comprises branch pipeline and main line, described branch pipeline is all connected with main line, described some charging baskets are connected to independently charging branch pipeline separately, and by charging main line coupled reaction still charging aperture, described flowmeter one is arranged on charging main line, and described magnetic valve one is arranged on charging main line, and is positioned at below flowmeter one; Described flowmeter one and magnetic valve one are all connected to controller, data on flows in pipeline is flowed to controller by described flowmeter one, described controller carries out switch control rule to rear to magnetic valve one according to flow-rate ratio, described feed system is positioned at above reactor, and utilizes difference in height to carry out the conveying of material;
Described discharge system comprises discharging pipeline, flowmeter two, magnetic valve two, material storing tank, described discharging pipeline coupled reaction still discharging opening, described discharging pipeline is provided with flowmeter two and magnetic valve two, described flowmeter two and magnetic valve two be connection control device respectively, and the data that described controller returns according to flowmeter two carry out switch control rule in conjunction with the capacity of material storage tank to magnetic valve;
Described heating system is heat-conducting oil heating system, mainly comprise electric heater, oil cylinder, circulating pump and circulation line, described electric heater connects oil cylinder, for the heating of conduction oil, described circulating pump connects oil cylinder and circulation line, for conduction oil is pumped in circulation line, described conduction oil circulation line arranges two, circulation line one is arranged at reactor inwall, circulation line two is arranged in reactor near shaft place, a bracing or strutting arrangement is also provided with, described distillation condensing unit coupled reaction still top below described circulation line two.
2. the intellectualized production system of a kind of electroplating additive as claimed in claim 1, it is characterized in that: described circulation line one and two includes oil pipe, oil-in and oil-out, the oil-in of described circulation line one is arranged at reactor top, oil-out is arranged at reactor bottom, the oil-in of described circulation line two is arranged at reactor bottom, and oil-out is arranged at reactor top.
3. the intellectualized production system of a kind of electroplating additive as claimed in claim 1, is characterized in that: be also enclosed with heat-insulation layer outside described reactor kettle.
4. the intellectualized production system of a kind of electroplating additive as claimed in claim 3, is characterized in that: described heat-insulation layer is the lamination layer structure of at least one deck rubber-plastic sponge, felt, aluminium foil.
5. the intellectualized production system of a kind of electroplating additive as claimed in claim 1, is characterized in that: also comprise a device for detecting temperature, and described device for detecting temperature is arranged between two circulation lines, described device for detecting temperature connection control device.
6. the intellectualized production system of a kind of electroplating additive as claimed in claim 1, is characterized in that: described reactor kettle cover is also provided with Manual material feeding mouth.
7. the intellectualized production system of a kind of electroplating additive as claimed in claim 1, is characterized in that: described bracing or strutting arrangement is a four-point supporting device, and four angle seats of described bracing or strutting arrangement are connected with reactor autoclave body bottom by bolt, gasket seal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520769420.6U CN205020084U (en) | 2015-09-30 | 2015-09-30 | Electroplate intelligent production system of additive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520769420.6U CN205020084U (en) | 2015-09-30 | 2015-09-30 | Electroplate intelligent production system of additive |
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| Publication Number | Publication Date |
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| CN205020084U true CN205020084U (en) | 2016-02-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201520769420.6U Expired - Fee Related CN205020084U (en) | 2015-09-30 | 2015-09-30 | Electroplate intelligent production system of additive |
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| CN (1) | CN205020084U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107858735A (en) * | 2017-12-26 | 2018-03-30 | 西北工业大学 | A kind of electrolytic cell for composite electrodeposition |
| CN108914199A (en) * | 2018-08-21 | 2018-11-30 | 陕西汉和新材料科技有限公司 | A kind of additive tank water bath heating system |
-
2015
- 2015-09-30 CN CN201520769420.6U patent/CN205020084U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107858735A (en) * | 2017-12-26 | 2018-03-30 | 西北工业大学 | A kind of electrolytic cell for composite electrodeposition |
| CN108914199A (en) * | 2018-08-21 | 2018-11-30 | 陕西汉和新材料科技有限公司 | A kind of additive tank water bath heating system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 212300 Zhenjiang city of Jiangsu province Danyang Yanling Town South Patentee after: JIANGSU MENGDE NEW MATERIALS TECHNOLOGY CO., LTD. Address before: 212300 Zhenjiang city of Jiangsu province Danyang Yanling Town South Patentee before: JIANGSU MENGDE PLATING CHEMICALS CO., LTD. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160210 Termination date: 20200930 |