A kind of electrolyte sample production line
Technical field
The utility model relates to a kind of electrolyte production line, is specifically related to a kind of electrolyte sample production line.
Background technology
At present, preparation electrolyte is by the preparation of electrolyte production line, or by artificial preparation.Existing electrolyte production line once can be produced at least 500 kilograms of electrolyte, but some client's quantity ordered is less than 500 kilograms.If produce with existing electrolyte production line, will cause part electrolyte to overstock.Yet the amount that human configuration generally is fit to electrolyte is 1 to 5 kilogram, if adopt artificial preparation greater than 5 kilograms and less than 500 kilograms electrolyte, workman's labour intensity is larger.Therefore, how adopting machine preparation a small amount of electrolyte is that people expect one of problem that solves.
The utility model content
For solving the problems of the technologies described above, the utility model provides a kind of electrolyte sample production line, and not only cost is low for it, flexible operation and high productivity, and can be used in production small lot electrolyte.
For achieving the above object, the technical solution of the utility model is as follows:
A kind of electrolyte sample production line comprises several confession solvent devices, preparation still, vacuum tube system, nitrogen tube system, freezing liquid system, and the blow-down pipe system; Several placed side by side for solvent device, comprise purification column and storage tank for solvent device; The top of purification column links to each other with the top of storage tank by pipeline one, and pipeline one in parallel supplies solvent pipe, and is provided with valve one for solvent pipe; The bottom of purification column links to each other with the bottom of storage tank by pipeline two, and pipeline two is provided with a circulating pump; Pipeline two is a blow-off pipe in parallel also; The top of storage tank also is provided with a feed pipe; The top of storage tank sidewall is provided with visor; The preparation still comprises kettle, and kettle comprises kettle cover, inner casing, and shell; Kettle cover and inner casing form a cavity, form a confined chamber between inner casing and the shell; The inner casing center is provided with rabbling mechanism, and the kettle top is provided with for the motor that drives rabbling mechanism, and the bottom of inner casing is provided with discharge nozzle; The confined chamber bottom row of being provided with cooling liquid tube; The cavity top is provided with solvent input pipe and salt adding pipe; All all link to each other with the solvent input pipe for solvent pipe; The vacuum tube system all links to each other with the top of storage tank and cavity; Nitrogen tube system and purification column, storage tank, and the top of cavity all links to each other; The freezing liquid system links to each other with the top of confined chamber respectively with the blow-down pipe system.
Further, the volume of purification column is 50 liters.
Further, the volume of storage tank is 100 liters.
Further, pipeline one is a probe tube in parallel also, and probe tube is provided with valve two.
Further, the top of cavity is provided with temperature measurer.
Further, the sidewall of shell body is provided with Weighing module.
Further, the top of preparation still is provided with by guide rail hangs title, and the efferent duct that hangs title links to each other with the salt adding pipe.
Further, comprise that also explosion-proof electronic claims.
Further, discharge nozzle links to each other with the electrolyte bucket that explosion-proof electronic deserves to be called by defeated electrolyte pipe.
By technique scheme, a kind of electrolyte sample production line provided by the utility model, it comprises several for solvent device, preparation still, vacuum tube system, nitrogen tube system, freezing liquid system, and the blow-down pipe system; Comprise purification column and storage tank for solvent device; A kind of electrolyte sample production line provided by the utility model has that not only cost is low, flexible operation and high productivity, and can be used in the advantage of production small lot electrolyte.
Description of drawings
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, the below will do to introduce simply to the accompanying drawing of required use in embodiment or the description of the Prior Art.
Fig. 1 is the structural representation of the utility model embodiment 1 disclosed a kind of electrolyte sample production line.
The specific embodiment
Below in conjunction with the accompanying drawing among the utility model embodiment, the technical scheme among the utility model embodiment is clearly and completely described.
With reference to figure 1, a kind of electrolyte sample production line provided by the utility model comprises several confession solvent devices, preparation still, vacuum tube system 63, nitrogen tube system 61, freezing liquid system 64, and blow-down pipe system 62; Several placed side by side for solvent device, comprise purification column 2 and storage tank 1 for solvent device; The volume of purification column 2 is 50 liters, and the volume of storage tank 1 is 100 liters.The top of purification column 2 links to each other with the top of storage tank 1 by pipeline 1, and pipeline one 4 in parallel supplies solvent pipe 71, and is provided with valve 1 for solvent pipe 71; The bottom of purification column 2 links to each other with the bottom of storage tank 1 by pipeline 25, and pipeline 25 is provided with a circulating pump 51; Pipeline 25 is a blow-off pipe 52 in parallel also; The top of storage tank 1 also is provided with a feed pipe 12; The two ends of pipeline 1 and pipeline 25 are equipped with valve 3 42.The top of storage tank 1 sidewall is provided with visor 11; The preparation still comprises kettle, and kettle comprises kettle cover 31, inner casing 32, and shell 33; Kettle cover 31 forms a cavity 35 with inner casing 32, forms a confined chamber 34 between inner casing 32 and the shell 33; Inner casing 32 centers are provided with rabbling mechanism 36, and the kettle top is provided with for the motor 39 that drives rabbling mechanism 36, and the bottom of inner casing 32 is provided with discharge nozzle 72; Confined chamber 34 bottoms are provided with row's cooling liquid tube; Cavity 35 tops are provided with solvent input pipe 73 and salt adding pipe 91; All all link to each other with solvent input pipe 73 for solvent pipe 71; Vacuum tube system 63 all links to each other with the top of storage tank 1 with cavity 35; Nitrogen tube system 61 and purification column 2, storage tank 1, and the top of cavity 35 all links to each other; Freezing liquid system 64 links to each other with the top of confined chamber 34 respectively with blow-down pipe system 62.
In addition, pipeline 1 is a probe tube 41 in parallel also, and probe tube 41 is provided with valve 2 411, and this probe tube 41 is conducive to sampling.
In addition, the top of cavity 35 is provided with temperature measurer 37, can detect in real time temperature in the cavity 35 by temperature measurer 37.
In addition, the sidewall of shell 33 bodies is provided with Weighing module 38, can know the weight of every kind of solvent by Weighing module 38, so not only make things convenient for operation, has also greatly improved the quality of electrolyte.
In addition, the top of preparation still is provided with to hang by guide rail 93 and claims 92, hangs to claim 92 efferent duct to link to each other with salt adding pipe 91, claims the 92 online weight that claim salt by hanging, and not only makes things convenient for operation, has also greatly improved the quality of electrolyte.
In addition, this electrolyte sample production line comprises that also explosion-proof electronic claims 8; Discharge nozzle 72 claims the electrolyte bucket 81 on 8 to link to each other by defeated electrolyte pipe with explosion-proof electronic, claims 8 can claim the weight of electrolyte by explosion-proof electronic.
Existing electrolyte is made by four kinds of solvents usually, so need quadruplet for solvent device.For simplicity, only show a cover among Fig. 1 for solvent device.A kind of electrolyte sample production line provided by the utility model production by the production process of the electrolyte that four kinds of solvents are made is: (1) piles qualified molecular sieve in purification column 2; (2) the first solvent is entered storage tank 1 from feed pipe 12, observes level condition by visor 11, wait storage tank 1 full after, then stop to add raw material; (3) start circulating pump 51, carry out dehydration cycle; (4) whether detection the first solvent is qualified behind the circulation certain hour; (5) after the first solvent is qualified, the valve 3 42 of blinding off a line and following near storage tank 1 on one 4; (6) according to the requirement of prescription, prepare still by for solvent pipe 71 the first solvent being injected, and weigh by Weighing module 38, reach requirement to guarantee the first weight of solvent, then manually close the valve 1 on the corresponding confession solvent pipe 71; (7) repeat above-mentioned 1 to 6 step, process satisfactory other three kinds of solvents at other three covers in the solvent device, and successively three kinds of solvents are injected the preparation still by formulation weight; (8) open freezing liquid system 64, provide cooling source to give the preparation still; When (9) adding freezing liquid, mix solvent with rabbling mechanism 36 simultaneously; (10) near below 0 degree centigrade the time when the temperature of mixed solvent, add suitable weight electrolytic salt by prescription requirements, the stirring of limit edged; (11) add electrolytic salt and finish after, add again the additive of regulation by salt adding pipe 91; (12) continue to stir, until mixed solvent is stirred; (13) stir end, get final product by discharge nozzle 72 output electrolyte.This shows that a kind of electrolyte sample production line provided by the utility model has that not only cost is low, flexible operation and high productivity, and can be used in the advantage of production small lot electrolyte.
Need to prove: the quantity for solvent device should be decided according to the quantity of the needed solvent species of preparation electrolyte.To the above-mentioned explanation of the disclosed embodiments, make this area professional and technical personnel can realize or use the utility model.Multiple modification to these embodiment will be apparent concerning those skilled in the art, and General Principle as defined herein can in the situation that does not break away from spirit or scope of the present utility model, realize in other embodiments.Therefore, the utility model will can not be restricted to these embodiment shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.