CN203373421U - MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment - Google Patents

MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment Download PDF

Info

Publication number
CN203373421U
CN203373421U CN201320389770.0U CN201320389770U CN203373421U CN 203373421 U CN203373421 U CN 203373421U CN 201320389770 U CN201320389770 U CN 201320389770U CN 203373421 U CN203373421 U CN 203373421U
Authority
CN
China
Prior art keywords
mocvd
heat insulation
reaction chamber
gas
insulation cylinder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN201320389770.0U
Other languages
Chinese (zh)
Inventor
贺有志
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHENZHEN S C NEW ENERGY EQUIPMENT CO Ltd
Original Assignee
SHENZHEN S C NEW ENERGY EQUIPMENT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHENZHEN S C NEW ENERGY EQUIPMENT CO Ltd filed Critical SHENZHEN S C NEW ENERGY EQUIPMENT CO Ltd
Priority to CN201320389770.0U priority Critical patent/CN203373421U/en
Application granted granted Critical
Publication of CN203373421U publication Critical patent/CN203373421U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Landscapes

  • Chemical Vapour Deposition (AREA)

Abstract

The utility model discloses MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment. The MOCVD reaction equipment comprises a reaction chamber, primary vapor inlets, vapor exhaust ports, a sheet carrying tray, a heating assembly, a secondary vapor inlet, a manipulator passage, magnetic fluid, a motor, a vacuum pump, a tail gas treatment tank and the like, wherein a first heat insulating tube is arranged in the reaction chamber, and the inside diameter of the first heat insulating tube is smaller than or equal to the diameter of the sheet carrying tray, so that a first chamber, of which the upper circumferential direction is provided with a gap, is formed by the first heat insulating tube and the sheet carrying tray. According to the MOCVD reaction equipment, after protecting gas or cooling gas enters the first chamber, the protecting gas or cooling gas can only pass through the gap and horizontally and outwardly flows along the lower surface of the sheet carrying tray, so that disturbance to a gas field in the reaction chamber caused by the fact that the protecting gas or cooling gas reversely flows relative to main gas flow is prevented.

Description

A kind of MOCVD conversion unit
Technical field
The utility model relates to a kind of chemical vapor depsotition equipment, relates in particular to a kind of MOCVD conversion unit.
Background technology
In the photoelectricity industry, the MOCVD conversion unit is the nucleus equipment of being not only the epitaxial wafer growth, is also the key equipment for preparing compound semiconductor film.The MOCVD reaction chamber, as the core component of equipment, generally comprises reaction chamber, diffuser, heating unit, the equal device of air of exhaust vacuum.
Produce the uniform film of thickness and component, guarantee around substrate uniformly outside temperature, also need to provide a uniform gas field, the air-flow that forms the gas field evenly enters from inlet mouth, from venting port, discharge, before this air-flow does not arrive substrate surface after entering reaction chamber, whether its air-flow velocity, concentration evenly equate, and the alkyls, the hydride that enter reaction chamber whether pre-reaction etc. is arranged is all vital.
Along with the development of technology, basically can guarantee a uniform inlet air flow at present.Current exhaust mode is mainly that reaction chamber is vacuumized, vacuum extractor comprises and is arranged on a reaction chamber bottom vacuum pipe venting hole (hole is greater than φ 63), and the vacuum pump be connected with this venting hole by corrugated tube and ball valve, pressure controller etc.Adopt this device to carry out exhaust and have some defects: the first, main air stream enters from reaction chamber top, because flange in the bottom vacuumizing and exhausting mouth is very large, and be arranged on a side of slide glass dish, main air stream is subject to the valve tube draft of a bias, cause main air stream to arrive air-flow concentration and the speed of each position of substrate surface on the slide glass dish inconsistent, thereby it is even to affect thickness and the component of substrate growing film; Second, shielding gas or cooling gas that reaction chamber flange in the bottom center enters, to enter from lower to upper, and main air stream is to enter from top to bottom in reaction chamber inside, the air-flow of both direction is relative in body of wall, add the exhaust draft of vaccum exhaust outlet of flange in the bottom single side face to the attraction of two air-flows, cause the air-flow confusion in reaction chamber, the even gas field of substrate growth demand has been produced to great destructiveness; The 3rd, the bore of vaccum exhaust outlet is larger, also just larger to the disposable free air delivery of air-flow in cavity, when reaction chamber pressure is down to 20Torr from atmospheric pressure state, open former seconds of vacuum pump, because disposable free air delivery is large, and without any buffering, impact to vacuum pump is very large, has seriously reduced the work-ing life of vacuum pump.
Therefore, how providing the more uniform MOCVD conversion unit in a kind of gas field is industry technical problem urgently to be resolved hurrily.
The utility model content
The utility model, in order to solve reaction chamber reaction gases and shielding gas/cooling gas relative movement in prior art, causes the problem of air-flow confusion, proposes a kind of MOCVD conversion unit.
The MOCVD conversion unit that the utility model proposes comprise sealing reaction chamber, be located at the reaction chamber top primary air inlet, be located at reaction chamber bottom venting port, be located at slide glass dish and heating component on the reaction chamber axle center, be located at the inferior inlet mouth of slide glass dish below, reaction chamber bottom, also comprise the first heat insulation cylinder that is arranged on the heating component outside, slide glass dish below, this first heat insulation cylinder and slide glass dish form a top circumferential direction and establish gapped the first cavity.
In the technical program, can also be at the second heat insulation cylinder of the arranged outside concentric of the first heat insulation cylinder, venting port is between first, second heat insulation cylinder, and be horizontally disposed with all gas dash plates of vacuum between first, second heat insulation cylinder, described vacuum all gas dash plate is provided with the first through hole, and on described the first heat insulation cylinder, vacuum all evenly is provided with the second through hole in the below of gas dash plate.Air-flow velocity in the diameter of the first through hole and quantity and the second heat insulation cylinder is proportional, and the air-flow velocity between the diameter of the second through hole and quantity and the second heat insulation cylinder and reaction chamber inwall is proportional.
Further, venting port can also at least evenly arrange 2.
Further again, the end that inferior inlet mouth is positioned at the reaction chamber bottom also is provided with the magnetic fluid shrouding.
The utility model can not be subject to the impact of other air-flows after having adopted the first heat insulation cylinder to make main air stream enter reaction chamber, has avoided gaseous exchange that the gas field in reaction chamber is caused confusion, for the substrate growth provides a uniform gas field.And a plurality of venting ports evenly are set, air-flow can be disperseed, alleviated the impact of exhaust to vacuum pump, in the work-ing life of having improved vacuum pump, also reduced the noise in the working process simultaneously.The utility model can solve the impact vacuumized whole gas field effectively, has improved greatly the quality of substrate growth.
The accompanying drawing explanation
Below in conjunction with embodiment and accompanying drawing, the utility model is elaborated, wherein:
Fig. 1 is structural representation of the present utility model.
Embodiment
As shown in Figure 1, the MOCVD conversion unit that the utility model one embodiment proposes, mainly comprise sealing reaction chamber 1, be located at the reaction chamber top primary air inlet 2, be located at reaction chamber bottom venting port 3, be located at slide glass dish 4 and heating component 5 on the reaction chamber inner axes, be located at slide glass dish below, reaction chamber bottom inferior inlet mouth 6, be arranged on reaction chamber one side the mechanical manipulator path 10, be located at magnetic fluid and motor 12 below reaction chamber, vacuum pump and vent gas treatment case 13 etc.
In reaction chamber, in the heating component outside, slide glass dish below also is provided with the first heat insulation cylinder 7, the internal diameter of this first heat insulation cylinder is less than or equal to the diameter of slide glass dish, it and slide glass dish form a top circumferential direction and establish gapped the first cavity 14, in the present embodiment, slide glass tray bottom external diameter is more smaller than top external diameter, its cross-sectional shape is a T font, the first heat insulation cylinder just is arranged on the top lower position of slide glass tray bottom one side, just leave like this gap of horizontal direction between the below of slide glass dish and the first heat insulation cylinder, because of stopping of slide glass dish lower surface, shielding gas or cooling gas enter in this chamber from inferior inlet mouth, can only pass through this gap, along slide glass dish lower surface level, outwards flow, finally by vacuum pump, by end flange venting hole, taken away, prevent that shielding gas or cooling gas are with respect to the main air stream countercurrent flow, disorder is caused in gas field in reaction chamber.
In the present embodiment, the second heat insulation cylinder 8 of one concentric can also be set in the outside of the first heat insulation cylinder, make venting port between first, second heat insulation cylinder, and between first, second heat insulation cylinder, the top of venting port can also be horizontally disposed with all gas dash plates 9 of a vacuum, vacuum all evenly is provided with the first through hole on the gas dash plate, the setting of this first through-hole diameter, quantity, the flow velocity that enters the second heat insulation cylinder internal layer chamber with main air stream is proportional.Main air stream is after the substrate surface reaction, with the air-flow that enters the first heat insulation cylinder medial compartment from inferior inlet mouth, mix, by the equal buffering of gas dash plate of vacuum, finally by flange venting hole at the bottom of reaction chamber, by vacuum, originally taken away, through equal air-flows of gas dash plate, be dispersed, flow velocity is cushioned, to the reducing of limit that have the greatest impact of the gas field in reaction chamber.And, the below of whole heat insulation cylinder, lower than the equal installed position of gas dash plate of vacuum, its circumferential direction has a few circle the second through holes, can drain uniformly reactant gases.The diameter of the second through hole, the setting of quantity and adjustment, with the inboard little cavity formed of the second heat insulation cylinder and reaction chamber, and main air stream to flow to the flow velocity of this little cavity proportional.
Venting port can also at least evenly arrange 2, and the internal diameter of venting port is less than or equal to 40mm.In the present embodiment, the vacuum all below of gas dash plate is provided with the venting port that two internal diameters are 40mm, and they are arranged on the same diametric(al) of reaction chamber bottom, and effectively diffusing air current, drain air-flow uniformly.
The end that inferior inlet mouth is positioned at the reaction chamber bottom is provided with the magnetic fluid shrouding; shielding gas or cooling gas pass through time inlet mouth the time; buffering and dispersion through the magnetic fluid shrouding; enter uniformly the first heat insulation cylinder medial compartment; and through the gap between slide glass dish and the first heat insulation cylinder; oriented and ordered exhaust, solved the problem with the main air stream relative current.
The foregoing is only preferred embodiment of the present utility model; not in order to limit the utility model; all any modifications of doing within spirit of the present utility model and principle, be equal to and replace and improvement etc., within all should being included in protection domain of the present utility model.

Claims (6)

1. a MOCVD conversion unit, the reaction chamber (1), primary air inlet (2), venting port (3), slide glass dish (4), the heating component (5) that comprise sealing, and the inferior inlet mouth (6) of slide glass dish below, reaction chamber bottom, it is characterized in that, the below of the outside of described heating component, slide glass dish is provided with the first heat insulation cylinder (7), and described the first heat insulation cylinder and slide glass dish form a top circumferential direction and establish gapped the first cavity (14).
2. MOCVD conversion unit as claimed in claim 1, it is characterized in that, the outside of described the first heat insulation cylinder is provided with second heat insulation cylinder (8) of concentric, described venting port is between first, second heat insulation cylinder, and between first, second heat insulation cylinder, level is provided with all gas dash plates (9) of vacuum, described vacuum all gas dash plate is provided with the first through hole, and on described the first heat insulation cylinder, vacuum all evenly is provided with the second through hole in the below of gas dash plate.
3. MOCVD conversion unit as claimed in claim 2, it is characterized in that, air-flow velocity in the diameter of described the first through hole and quantity and the second heat insulation cylinder is proportional, and the air-flow velocity between the diameter of described the second through hole and quantity and the second heat insulation cylinder and reaction chamber inwall is proportional.
4. MOCVD conversion unit as described as claim 1 or 3, is characterized in that, described venting port at least evenly is provided with 2.
5. MOCVD conversion unit as claimed in claim 4, is characterized in that, the internal diameter of described venting port is less than or equal to 40mm.
6. MOCVD conversion unit as claimed in claim 5, is characterized in that, the end that described inlet mouth is positioned at bottom reaction chamber is provided with the magnetic fluid shrouding.
CN201320389770.0U 2013-07-02 2013-07-02 MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment Expired - Lifetime CN203373421U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201320389770.0U CN203373421U (en) 2013-07-02 2013-07-02 MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201320389770.0U CN203373421U (en) 2013-07-02 2013-07-02 MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment

Publications (1)

Publication Number Publication Date
CN203373421U true CN203373421U (en) 2014-01-01

Family

ID=49835967

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201320389770.0U Expired - Lifetime CN203373421U (en) 2013-07-02 2013-07-02 MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment

Country Status (1)

Country Link
CN (1) CN203373421U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104979248A (en) * 2015-07-09 2015-10-14 江苏德尔森传感器科技有限公司 Air supply mechanism for sensor monocrystalline silicon etching apparatus
CN108866511A (en) * 2018-09-04 2018-11-23 陆挚译 A kind of chemical vapor deposition unit
CN112410754A (en) * 2020-10-30 2021-02-26 北京北方华创微电子装备有限公司 Tail gas device and semiconductor process equipment
CN117604494A (en) * 2024-01-23 2024-02-27 楚赟精工科技(上海)有限公司 Chemical vapor deposition equipment

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104979248A (en) * 2015-07-09 2015-10-14 江苏德尔森传感器科技有限公司 Air supply mechanism for sensor monocrystalline silicon etching apparatus
CN104979248B (en) * 2015-07-09 2018-01-12 重庆德尔森传感器技术有限公司 The mechanism of supplying gas of sensor monocrystalline silicon etching device
CN108866511A (en) * 2018-09-04 2018-11-23 陆挚译 A kind of chemical vapor deposition unit
CN108866511B (en) * 2018-09-04 2020-08-28 金华职业技术学院 Chemical vapor deposition device
CN112410754A (en) * 2020-10-30 2021-02-26 北京北方华创微电子装备有限公司 Tail gas device and semiconductor process equipment
CN117604494A (en) * 2024-01-23 2024-02-27 楚赟精工科技(上海)有限公司 Chemical vapor deposition equipment
CN117604494B (en) * 2024-01-23 2024-05-17 楚赟精工科技(上海)有限公司 Chemical vapor deposition equipment

Similar Documents

Publication Publication Date Title
CN203373421U (en) MOCVD (Metal Oxide Chemical Vapor Deposition) reaction equipment
TWI507561B (en) Showerhead integrating intake and exhaust
CN111952233B (en) Edge purging device, base system and process chamber
CN106133874B (en) For being quickly cooled down the method and apparatus of substrate
TW201350618A (en) Vacuum film forming apparatus
CN107304474B (en) Reaction chamber and semiconductor processing equipment
KR20210148405A (en) Apparatus for increasing flux from an ampoule
JP7370499B1 (en) semiconductor process equipment
CN103649368A (en) Gas-injection apparatus, atomic layer deposition apparatus, and atomic layer deposition method using the apparatus
US20170233888A1 (en) Reactor gas panel common exhaust
CN216035807U (en) Precursor material packaging container for semiconductor
CN203429246U (en) Leakproof structure, reaction chamber and semiconductor processing equipment
CN219102149U (en) Vacuum valve resistant to plasma etching
CN108690906B (en) Stainless steel heat treatment process adopting vacuum bright heat treatment furnace
CN201343581Y (en) Extension device
CN113327875A (en) Vertical heat treatment equipment
CN220724332U (en) Uniform air inlet structure of vacuum chamber
CN217405208U (en) Exhaust device for dynamic superconducting magnet and dynamic superconducting magnet
CN221234446U (en) Packaging container capable of preventing non-gaseous material from flowing out and vapor deposition system
CN220202036U (en) Silicon wafer deposition furnace
CN218621036U (en) Air extractor and LPCVD tubular reactor of stable gas flow field
CN220116666U (en) Semiconductor process equipment and air inlet adjusting device thereof
CN201834966U (en) Water-cooling sandwich of metal organic chemical vapor deposition equipment
CN219156970U (en) Air exhaust pipeline device for carbon-carbon vapor deposition furnace
CN216843310U (en) Automatic air discharging and inlet isolating device for solution tank and storage tank

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CX01 Expiry of patent term

Granted publication date: 20140101

CX01 Expiry of patent term