CN202751834U - Improved type multifunctional extractor - Google Patents
Improved type multifunctional extractor Download PDFInfo
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- CN202751834U CN202751834U CN 201220450977 CN201220450977U CN202751834U CN 202751834 U CN202751834 U CN 202751834U CN 201220450977 CN201220450977 CN 201220450977 CN 201220450977 U CN201220450977 U CN 201220450977U CN 202751834 U CN202751834 U CN 202751834U
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- extractor
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- thermometer
- tube
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- 239000000284 extract Substances 0.000 claims abstract description 39
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 238000010992 reflux Methods 0.000 claims description 12
- 239000000126 substance Substances 0.000 abstract description 8
- 230000003647 oxidation Effects 0.000 abstract description 6
- 238000007254 oxidation reaction Methods 0.000 abstract description 6
- 238000009833 condensation Methods 0.000 abstract description 4
- 230000005494 condensation Effects 0.000 abstract description 4
- 238000000605 extraction Methods 0.000 description 16
- 239000002904 solvent Substances 0.000 description 13
- 239000000203 mixture Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 9
- 238000002386 leaching Methods 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
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Abstract
The utility model provides an improved type multifunctional extractor and belongs to the class of chemical apparatus. The improved type multifunctional extractor comprises a thermometer, a round-bottom flask and an extractor, wherein the extractor is communicated with the thermometer and the round-bottom flask through a seat tube of the extractor. A communicating port on the upper portion of the seat tube of the extractor is provided with the thermometer which is used to control and observe heating temperature, and a communicating port on the lower portion of the seat tube of the extractor is provided with the round-bottom flask which is used to heat extracting solution. An inner cavity of the extractor is provided with a backflow condensation tube which is used to directly achieve cooling of extracts, an upper branch tube which is communicated with the backflow condensation tube on the upper portion and a lower branch tube which is communicated with a collector on the lower portion are branched by a communicating port in the middle of the seat tube of the extractor, the collector which is communicated with the lower branch tube is communicated with a separator on the lower portion. The improved type multifunctional extractor has the advantages of being short in extracting time, easy to separate, high in quality of extracts, and small in probability due to the fact that the extracting time is short and extracted components take oxidation or other chemical changes.
Description
Technical field
The utility model relates to the chemical apparatuses class, particularly a kind of Improvement type multi-functional extractor, and espespecially extraction time is short so that the Improvement type multi-functional extractor that possibility is little, extract quality is high of the component generation oxidation that extracts or other chemical changes.
Background technology
Traditional distillation extracting method is widely used in a small amount of separation and extraction process in laboratory.Multi-functional extractor is improved original distillation extractor, being applicable to a small amount of multi-phase multi-component in laboratory separates, yet extract product in the leaching process and easily form mixture with the extraction solvent, for example traditional method is extracted volatile oil from the armaticity plant, because extraction tube is passed by length, causes the extract loss large, extract the often azeotropic mixture of extract and solvent of product, enter traditional extraction flask, still need to use the separatory funnel secondary separation, cause the secondary waste.In this process, because operation is relatively loaded down with trivial details, so that operating efficiency is low.Not only extraction rate is slow, and the mixture quality that extracts is low, and oxidation or other chemical changes may occur the component part of taking-up.Compare soxhlet extraction, its used instrument is complicated, and heating extraction time is long, may cause target extract component that oxidation or other chemical changes partly occur, the extraction that is not suitable for some low boiling component with separate.
The utility model content
The purpose of this utility model is to provide a kind of Improvement type multi-functional extractor, it is long that the solution conventional method is extracted pipeline relatively, in leaching process, the extract loss is large, extract the often azeotropic mixture of extract and solvent of product, and enter traditional extraction flask, and still need to use the separatory funnel secondary separation, cause the problem of secondary waste.
The utility model specifically comprises: thermometer, round-bottomed flask, extractor, this extractor comprise extractor seat pipe, reflux condensing tube, upper arm, lower branch line, collector and separator.Wherein:
Extractor is connected with thermometer and round-bottomed flask respectively by extractor seat pipe: this extractor seat pipe top connected entrance is equipped with for control and observes the thermometer of heating-up temperature, and this extractor seat pipe bottom connected entrance is equipped with the round-bottomed flask for the heating extract;
The extractor inner chamber is provided with for the extract reflux condensing tube of directly realizing cooling, one connected entrance at extractor seat pipe middle part branches out the upper arm that is connected with the reflux condensing tube on top and the lower branch line that is connected with lower tank, and collector is connected with the separator of bottom.
Operation principle: extract and extraction solvent are put into flask, by the control heating-up temperature extract and partial solvent in the flask are steamed simultaneously, the azeotropic mixture that produces enters extractor on the way, wherein steam can enter reflux condensing tube by upper arm, steam is formed water in the chance condensation of condenser pipe place and is flowed directly into the collector that is connected with lower branch line, has guaranteed that a large amount of steams is collected; Before the arm, the steam that a part has been distilled out of in extractor seat pipe may be met cold and be flowed back to round-bottomed flask on steam enters, and the steam that another part is collected can also enter into collector by lower branch line; In still-process, extract solvent and may form azeotropic mixture with extract and enter lower tank, enter the azeotropic mixture cooling of collector after, layering, the collector below has the separatory piston, by piston with the azeotropic mixture that extracts separately.In the whole leaching process, the azeotropic mixture amount that extracts often seldom if change separatory funnel over to again then may cause the significant wastage of extracting product, is directly separated in the arm of extractor, directly extracts object, has avoided waste
The scope of application of the present utility model: be applicable to the extract consumption large, extract the few solvent of product; In the leaching process, solvent may together steam with extract, need to manually carry out the secondary separation solvent; Extract need be avoided long-time heating as far as possible, and in the heating process, oxidation or other chemical changes may occur the part component, for example extracts the situation of volatile oil from fragrant plant.
The utility model has the advantage of:
One, the utility model is improved on the basis of original distilling apparatus and is formed, the a plurality of devices such as still head, condenser pipe, knockout that are original extractor reconfigure, it is short to have extraction time after the improvement, for example can finish extraction in 10 minutes in heating.
Two, be easy to separate, extract directly separates by separator with the azeotropic mixture that solvent forms, and directly keeps the target extract, and extraction rate is fast, and is simple, convenient, and efficiency is high.
Three, extract quality is high, because extraction time is short so that the possibility of the component generation oxidation that extracts or other chemical changes is little.
Description of drawings
Fig. 1 is apparatus structure schematic diagram of the present utility model.
Sequence number implication in the accompanying drawing: 1. thermometer, 2. round-bottomed flask, 3. arm on extractor, 30. extractor seat pipes, 31. reflux condensing tubes, 32., 33. lower branch lines, 34. collectors, 35. separators, 4. steam.
The specific embodiment
The utility model Improvement type multi-functional extractor includes: thermometer 1, round-bottomed flask 2 and extractor 3, extractor 3 include extractor seat pipe 30, reflux condensing tube 31, upper arm 32, lower branch line 33, collector 34 and separator 35.Its concrete structure is: extractor 3 is connected with thermometer 1 and round-bottomed flask respectively by extractor seat pipe 30, the top connected entrance of its extractor seat pipe 30 is equipped with for control and observes the thermometer 1 of heating-up temperature, the bottom connected entrance of extractor seat pipe 30 is equipped with the round-bottomed flask 2 for the extract heating, the top of extractor 3 inner chambers is provided with reflux condensing tube 31, be used for directly realizing the extract of cooling, the tube wall periphery of this condenser pipe 31 branches out upper arm 32 and 33 two branched pipes of lower branch line by cooling medium circulation (shown in the accommodating cavity of the condenser pipe of condenser pipe 31 structure divisions and extractor 3 housings formation and upper and lower medium are imported and exported as shown) with the extractor seat pipe 30 that round-bottomed flask 2 is connected with thermometer 1, arm 32 is connected with reflux condensing tube 31 on it, lower branch line 33 is connected with collector 34, and collector 34 is connected with the separator 35 of bottom.
During work, extract and extraction solvent are put into flask 2, by the control heating-up temperature extract and partial solvent in the flask 2 are steamed simultaneously, the azeotropic mixture that produces enters extractor 3 on the way, wherein steam 4 can enter reflux condensing tube 31 by upper arm 32, steam is formed water in the chance condensation of condenser pipe 31 places and is flowed directly into the collector 34 that is connected with lower branch line 33, has guaranteed that a large amount of steams is collected; Before steam 4 enters arm 32, managing steam that 30 interior parts have been distilled out of at the extractor seat may meet cold and flow back to round-bottomed flask 2, the steam that another part is collected can also enter into collector 34 by lower branch line 33, in still-process, the extraction solvent may form azeotropic mixture with extract and enter lower tank 34, and under collector part layer, by a separator 35 that is connected with collector 34 bottoms, the separatory piston of this separator 35 separates, and directly extracts object.
Claims (1)
1. Improvement type multi-functional extractor, it is characterized in that comprising: thermometer (1), round-bottomed flask (2), extractor (3), this extractor (3) comprises extractor seat pipe (30), reflux condensing tube (31), upper arm (32), lower branch line (33), collector (34) and separator (35), wherein:
Extractor (3) is connected with thermometer (1) and round-bottomed flask (2) respectively by extractor seat pipe (30): this extractor seat pipe (30) top connected entrance is equipped with for control and observes the thermometer (1) of heating-up temperature, and this extractor seat pipe (30) bottom connected entrance is equipped with the round-bottomed flask (2) for the heating extract;
Extractor (3) inner chamber is provided with for the reflux condensing tube (31) of directly realizing the cooling extract, one connected entrance at extractor seat pipe (30) middle part branches out the upper arm (32) that is connected with the reflux condensing tube (31) on top and the lower branch line (33) that is connected with lower tank (34), and this collector (34) is connected with the separator (35) of bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220450977 CN202751834U (en) | 2012-09-06 | 2012-09-06 | Improved type multifunctional extractor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220450977 CN202751834U (en) | 2012-09-06 | 2012-09-06 | Improved type multifunctional extractor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202751834U true CN202751834U (en) | 2013-02-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220450977 Expired - Fee Related CN202751834U (en) | 2012-09-06 | 2012-09-06 | Improved type multifunctional extractor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202751834U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105435481A (en) * | 2015-12-21 | 2016-03-30 | 天津孚音生物科技发展有限公司 | Universal type distillation and water segregation component |
| CN105477899A (en) * | 2015-12-30 | 2016-04-13 | 大连德泽药业有限公司 | Automatic receiving control device for elemene industrial production |
| CN105536278A (en) * | 2015-12-21 | 2016-05-04 | 天津孚音生物科技发展有限公司 | Experimentally-used distillation water diversion assembly |
| CN105606423A (en) * | 2016-02-26 | 2016-05-25 | 河南中烟工业有限责任公司 | Extracting device and extracting method for volatile and semivolatile components in sample |
| CN109250730A (en) * | 2018-12-07 | 2019-01-22 | 吉首大学 | A kind of scalable extraction element of high efficiente callback manganese slag valuable constituent |
-
2012
- 2012-09-06 CN CN 201220450977 patent/CN202751834U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105435481A (en) * | 2015-12-21 | 2016-03-30 | 天津孚音生物科技发展有限公司 | Universal type distillation and water segregation component |
| CN105536278A (en) * | 2015-12-21 | 2016-05-04 | 天津孚音生物科技发展有限公司 | Experimentally-used distillation water diversion assembly |
| CN105477899A (en) * | 2015-12-30 | 2016-04-13 | 大连德泽药业有限公司 | Automatic receiving control device for elemene industrial production |
| CN105477899B (en) * | 2015-12-30 | 2017-11-03 | 大连德泽药业有限公司 | The automatic receiving control device of elemene industrialized production |
| CN105606423A (en) * | 2016-02-26 | 2016-05-25 | 河南中烟工业有限责任公司 | Extracting device and extracting method for volatile and semivolatile components in sample |
| CN109250730A (en) * | 2018-12-07 | 2019-01-22 | 吉首大学 | A kind of scalable extraction element of high efficiente callback manganese slag valuable constituent |
| CN109250730B (en) * | 2018-12-07 | 2023-08-15 | 吉首大学 | Telescopic extraction device for efficiently recycling valuable components of manganese slag |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130227 Termination date: 20210906 |
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| CF01 | Termination of patent right due to non-payment of annual fee |