CN104711123B - A kind of device that natural borneol is slightly carried from borneol camphor tree - Google Patents
A kind of device that natural borneol is slightly carried from borneol camphor tree Download PDFInfo
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- CN104711123B CN104711123B CN201510113447.4A CN201510113447A CN104711123B CN 104711123 B CN104711123 B CN 104711123B CN 201510113447 A CN201510113447 A CN 201510113447A CN 104711123 B CN104711123 B CN 104711123B
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- extractor
- borneol
- condensers
- camphor tree
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Abstract
The invention discloses a kind of device that natural borneol is slightly carried from borneol camphor tree, including extractor, No. 1 condenser, No. 2 condensers, oil water separator, moisture trap, No. 3 condensers and receiver；Steam outlet pipe is provided with the top of extractor, steam outlet pipe is connected with oil water separator, moisture trap respectively by pipeline, the second valve is provided with the pipeline being connected with moisture trap, the first valve, No. 1 condenser and No. 2 condensers are provided with the pipeline being connected with oil water separator；Moisture trap is connected by pipeline with No. 3 condensers, and No. 3 condensers are connected with receiver.The device that natural borneol is slightly carried from borneol camphor tree of the present invention, in thick refining, when steam flow is gushed out from extractor, separately separated, allow three kinds of essential oil, natural borneol, water materials in thick refining while separate.Natural borneol purity more than 10% so can be both improved, essential oil purity can be also improved while water is separated to more than 90%.
Description
Technical field
The present invention relates to natural borneol extractive technique field, and in particular to a kind of dress that natural borneol is slightly carried from borneol camphor tree
Put.
Background technology
The existing method that natural borneol is slightly carried from borneol camphor tree, it is water-boiling method, i.e., directly extracts day by the way of boiling
Right borneol, this method is cumbersome, and energy consumption is big, and treating capacity is small, it is impossible to fully meets existing industrialized use demand.
The content of the invention
Goal of the invention：For the deficiencies in the prior art, the present invention proposes that one kind slightly carries natural borneol from borneol camphor tree
Device, for rapid, high volume extract natural borneol, meet the needs of largely producing natural borneol.
Technical scheme：In order to realize foregoing invention purpose, the technical solution adopted by the present invention is：
A kind of device that natural borneol is slightly carried from borneol camphor tree, including extractor, No. 1 condenser, No. 2 condensers, profit point
From device, moisture trap, No. 3 condensers and receiver；Be provided with steam outlet pipe at the top of extractor, steam outlet pipe by pipeline respectively with
Oil water separator, moisture trap are connected, and the second valve is provided with the pipeline being connected with moisture trap, with water-oil separating
The connected pipeline of device is provided with the first valve, No. 1 condenser and No. 2 condensers；Moisture trap passes through pipeline and No. 3 condensers
It is connected, No. 3 condensers are connected with receiver.
Visor is set at the top of the described extractor, for observing extractor.
Described extractor is used to deposit the borneol camphor tree raw material after crushing, and steam pipe coil is distributed in extractor, is being extracted
Tank is externally provided with heating jacket, and material outlet is provided with extraction pot bottom.
No. 3 described condensers have two or more, are connected in parallel between moisture trap and receiver.
No. 3 described condensers use internal dual coil pipes condensation, middle more stomata shuntings and external jacket condensation structure, use
Ethylene glycol carries out freezing processing as freezing liquid, by freezing unit, it is ensured that in condenser the temperature of water be maintained at 0 DEG C ~ 5 DEG C it
Between.
Described extractor is 10m3Extractor.
Beneficial effect：Compared with prior art, the device of the invention that natural borneol is slightly carried from borneol camphor tree, in thick refining,
When steam flow is gushed out from extractor, separately separated, allow three kinds of essential oil, natural borneol, water materials in thick refining while separate.
Natural borneol purity more than 10% so can be both improved, essential oil purity can be also improved while water is separated to more than 90%.Essential oil
While separation and Extraction, both saved the energy expenditure of subsequent extracted, and can also increase added value, so-called killing three birds with one stone.It is meanwhile logical
Overtesting, extraction time is shortened half, yield improves 10%, and power consumption reduces 65%, and discharge of wastewater can be reduced with steam
99%, domestic production capacity technologies are also exaggerated 20 times by the technique.
Brief description of the drawings
Fig. 1 is the structural representation for the device that natural borneol is slightly carried from borneol camphor tree.
Embodiment
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
The device of natural borneol is slightly carried from borneol camphor tree, as shown in figure 1, including 2, No. 1 extractor 1, the first valve condensers
3rd, No. 2 condensers 4, oil water separator 5,6, No. 3 condensers 7 of moisture trap and receiver 8.Extractor 1, which is used to deposit, to be crushed
Borneol camphor tree raw material afterwards, visor is provided with the top of extractor 1, for observing extractor 1, is distributed in extractor 1
Steam pipe coil, for being heated in tank, heating jacket to be externally provided with extractor 1, material outlet is provided with the bottom of extractor 1,
The top of extractor 1 is provided with steam outlet pipe, and steam outlet pipe is connected with oil water separator 5, moisture trap 6 respectively by pipeline, with gas
The connected pipeline of separator 6 is provided with the second valve 9, and the first valve 2,1 is provided with the pipeline being connected with oil water separator 5
Number condenser 3 and No. 2 condensers 4.Moisture trap 6 is connected by pipeline with No. 3 condensers 7, No. 3 condensers 7 and receiver 8
It is connected, wherein, No. 3 condensers 7 have two or more, are connected in parallel between moisture trap 6 and receiver 8.
Due to containing all kinds of heterogeneity impurity mixtures such as amine leaf essential oil, lipid in borneol camphor tree branches and leaves, work as natural borneol
Vaporization distillation when, if received together, can bring purity during refining be difficult to improve the problem of.So the present invention devise it is above-mentioned
Task equipment, in thick refining, when steam flow is gushed out from extractor 1, separately separated by control valve, allow essential oil, natural
Three kinds of borneol, water materials separate simultaneously in thick refining.Natural borneol purity more than 10% so can be both improved, the same of water separation
When can also improve essential oil purity to more than 90%.Separation and Extraction while essential oil, the energy expenditure of subsequent extracted was both saved, also
Added value, so-called killing three birds with one stone can be increased.
Wherein, No. 3 condensers 7 use internal dual coil pipes condensation, middle more stomata shuntings and external jacket condensation structure, use
Ethylene glycol carries out freezing processing as freezing liquid, by freezing unit, it is ensured that in condenser the temperature of water be maintained at 0 DEG C ~ 5 DEG C it
Between, it can adjust according to the actual requirements.When built-in double plate pipe device can ensure that the thermal current with borneol enters condenser, rapid condensation
Into solid-state.Middle more stomata shuntings, it is to mitigate to cause instantaneous temperature inside condenser too high when a large amount of thermal currents enter condenser,
Shunted using more stomatas, thermal current can be helped to import condenser and uniformly cooled down from all directions, borneol is improved and carry yield.External jacket
Device：The moment is full of coolant in chuck, is 10m to strengthen the constant of condenser internal temperature3Extractor is in 35 ~ 40min
Complete extraction and sufficiently guarantee is provided.
No. 3 condensers 7 are specially to design the autocratic cold of research and development for natural borneol Large Copacity extractor rapid extraction
Condenser, advantage are：Can meet the needs of high-capacity industrial metaplasia production；Quick cooling can improve the acceptance rate of natural borneol, from
And improve the relative amount of natural borneol；Uniformly cooling both ensure that receiving efficiency, while improve the purity of natural borneol.
Embodiment 2
This slightly puies forward the method for natural borneol from borneol camphor tree, using the character of high steam and natural borneol, with high pressure
Superheated steam, under 180 DEG C of states, directly act on branches and leaves.Because natural borneol boiling point is at 212 DEG C or so, can allow natural
Borneol vaporization distillation.Under high sealing state, condensation-crystallization is carried out by autocratic condenser, extracts natural borneol.Concrete technology
Comprise the following steps：
1）Borneol camphor tree branches and leaves are crushed, the particle length after crushing is no more than 10cm；It is preferred that 3-5cm.
2）Borneol camphor tree branches and leaves after crushing are added into extractor, branches and leaves, temperature control are directly acted on using high pressure superheated steam
180 DEG C, extract 35 ~ 40 minutes；
3）The natural borneol after gasification is condensed with condenser, collects natural borneol；Obtain accessory substance essential oil simultaneously
And water.
The technology instead of the conventional method originally distilled with water, extraction time be shortened half, yield improves
10%, power consumption reduces 65%, can reduce discharge of wastewater 99% with steam, the technique is also exaggerated domestic production capacity technologies
20 times.
Claims (4)
1. a kind of device that natural borneol is slightly carried from borneol camphor tree, it is characterised in that including extractor (1), No. 1 condenser (3), 2
Number condenser (4), oil water separator (5), moisture trap (6), No. 3 condensers (7) and receiver (8)；Pushed up in extractor (1)
Portion is provided with steam outlet pipe, and steam outlet pipe is connected with oil water separator (5), moisture trap (6) respectively by pipeline, with gas-water separation
The connected pipeline of device (6) is provided with the second valve (9), and the first valve is provided with the pipeline being connected with oil water separator (5)
(2), No. 1 condenser (3) and No. 2 condensers (4)；Moisture trap (6) is connected by pipeline with No. 3 condensers (7), and No. 3 cold
Condenser (7) is connected with receiver (8)；Described No. 3 condensers (7) use internal dual coil pipes condensation, middle more stomatas shuntings and
External jacket condensation structure, spent glycol carry out freezing processing, it is ensured that water in condenser as freezing liquid by freezing unit
Temperature is maintained between 0 DEG C~5 DEG C；Described extractor (1) is used to deposit the borneol camphor tree raw material after crushing, in extractor (1)
Interior distribution steam pipe coil, heating jacket is externally provided with extractor (1), material outlet is provided with extractor (1) bottom.
2. the device according to claim 1 that natural borneol is slightly carried from borneol camphor tree, it is characterised in that：In described extractor
(1) visor is set on top, for observing extractor (1).
3. the device according to claim 1 that natural borneol is slightly carried from borneol camphor tree, it is characterised in that：No. 3 described condensations
Device (7) has two or more, is connected in parallel between moisture trap (6) and receiver (8).
4. the device according to claim 1 that natural borneol is slightly carried from borneol camphor tree, it is characterised in that：Described extractor
(1) it is 10m3Extractor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510113447.4A CN104711123B (en) | 2015-03-16 | 2015-03-16 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510113447.4A CN104711123B (en) | 2015-03-16 | 2015-03-16 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
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| Publication Number | Publication Date |
|---|---|
| CN104711123A CN104711123A (en) | 2015-06-17 |
| CN104711123B true CN104711123B (en) | 2018-02-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510113447.4A Active CN104711123B (en) | 2015-03-16 | 2015-03-16 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI767710B (en) * | 2021-05-18 | 2022-06-11 | 台大龍腦生物科技股份有限公司 | Intelligent device for extracting natural borneol from borneo camphor |
| CN113860998A (en) * | 2021-10-28 | 2021-12-31 | 湖南复新龙脑农业科技发展有限公司 | Process for separating natural borneol of borneol camphor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| CN101279893A (en) * | 2008-05-26 | 2008-10-08 | 湖南省新晃县龙脑开发有限责任公司 | Efficient extracting device for natural borneol |
| CN102319517A (en) * | 2011-09-02 | 2012-01-18 | 江苏斯威森生物医药工程研究中心有限公司 | Extraction tank |
| CN103480169A (en) * | 2012-06-11 | 2014-01-01 | 拉曼大学 | Method to extract borneol from the exudates of dryobalanops aromatica |
| CN103601619A (en) * | 2013-11-01 | 2014-02-26 | 宜昌万森生态科技发展有限公司 | Extraction method and extraction equipment of natural borneol |
| CN204607960U (en) * | 2015-03-16 | 2015-09-02 | 江苏金叶子生物科技有限公司 | A kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree |
-
2015
- 2015-03-16 CN CN201510113447.4A patent/CN104711123B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| CN101279893A (en) * | 2008-05-26 | 2008-10-08 | 湖南省新晃县龙脑开发有限责任公司 | Efficient extracting device for natural borneol |
| CN102319517A (en) * | 2011-09-02 | 2012-01-18 | 江苏斯威森生物医药工程研究中心有限公司 | Extraction tank |
| CN103480169A (en) * | 2012-06-11 | 2014-01-01 | 拉曼大学 | Method to extract borneol from the exudates of dryobalanops aromatica |
| CN103601619A (en) * | 2013-11-01 | 2014-02-26 | 宜昌万森生态科技发展有限公司 | Extraction method and extraction equipment of natural borneol |
| CN204607960U (en) * | 2015-03-16 | 2015-09-02 | 江苏金叶子生物科技有限公司 | A kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree |
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| CN104711123A (en) | 2015-06-17 |
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