CN104711123A - Device for crudely extracting natural borneol from cinnamomum camphora - Google Patents
Device for crudely extracting natural borneol from cinnamomum camphora Download PDFInfo
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- CN104711123A CN104711123A CN201510113447.4A CN201510113447A CN104711123A CN 104711123 A CN104711123 A CN 104711123A CN 201510113447 A CN201510113447 A CN 201510113447A CN 104711123 A CN104711123 A CN 104711123A
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- extractor
- condensers
- condenser
- water separator
- camphor tree
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Abstract
The invention discloses a device for crudely extracting natural borneol from cinnamomum camphora. The device comprises an extraction tank, a condenser I, a condenser II, an oil-water separator, a gas-water separator, a condenser III and a receiver, wherein a vapor outlet pipe is arranged at the top of the extraction tank and connected with the oil-water separator and the gas-water separator through pipelines respectively; a second valve is arranged on a pipeline connected with the gas-water separator; a first valve, the condenser I and the condenser II are arranged on a pipeline connected with the oil-water separator; the gas-water separator is connected with the condenser III through a pipeline, and the condenser III is connected with the receiver. According to the device for crudely extracting the natural borneol from the cinnamomum camphora, during crude extraction, when vapor flow pours out of the extraction tank, separation is performed independently, and three matters, namely essential oil, the natural borneol and water are simultaneously separated during crude extraction, so that the purity of the natural borneol can be increased by higher than 10% and the purity of the essential oil also can be increased to higher than 90% while the water is separated.
Description
Technical field
The present invention relates to natural Broneolum Syntheticum extractive technique field, be specifically related to a kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree.
Background technology
The existing method slightly carrying natural Broneolum Syntheticum from borneol camphor tree is water-boiling method, namely directly adopts the mode of poach to extract natural Broneolum Syntheticum, the method complex operation, and energy consumption is large, and treatment capacity is little, can not meet existing industrialized user demand completely.
Summary of the invention
Goal of the invention: for the deficiencies in the prior art, the present invention proposes a kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree, extracts natural Broneolum Syntheticum for rapid, high volume, meets a large amount of demand of producing natural Broneolum Syntheticum.
Technical scheme: in order to realize foregoing invention object, the technical solution used in the present invention is:
Slightly carry a device for natural Broneolum Syntheticum from borneol camphor tree, comprise extractor, No. 1 condenser, No. 2 condensers, water-and-oil separator, air water separator, No. 3 condensers and receptors; Steam outlet pipe is provided with at extractor top, steam outlet pipe is connected with water-and-oil separator, air water separator respectively by pipeline, the pipeline be connected with air water separator is provided with the second valve, the pipeline be connected with water-and-oil separator is provided with the first valve, No. 1 condenser and No. 2 condensers; Air water separator is connected with No. 3 condensers by pipeline, and No. 3 condensers are connected with receptor.
Visor is established at described extractor top, for observing extractor.
Described extractor is for depositing the borneol camphor tree raw material after pulverizing, and distribute steam coils in extractor, is provided with heating jacket, bottom extractor, is provided with material outlet outside extractor.
No. 3 described condensers have two or more, are connected in parallel between air water separator and receptor.
No. 3 described condensers adopt inner dual coil pipes condensation, middle many pore shuntings and external jacket condensation structure, and spent glycol, as refrigerating fulid, carries out freezing treatment by freezing unit, guarantees that in condenser, the temperature of water remains between 0 DEG C ~ 5 DEG C.
Described extractor is 10m
3extractor.
Beneficial effect: compared with prior art, the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree of the present invention, when slightly refining, when steam flow is gushed out from extractor, is separately separated, and allows essential oil, natural Broneolum Syntheticum, water three kinds of materials be separated when thick refining simultaneously.So both can improve natural Broneolum Syntheticum purity more than 10%, while water is separated, also can improve essential oil purity to more than 90%.Separation and Extraction while essential oil, had both saved the energy expenditure of subsequent extracted, also can increase added value, so-called killing three birds with one stone.Meanwhile, by test, extraction time is shortened half, yield improves 10%, and power consumption reduces 65%, and use steam can reduce discharge of wastewater 99%, this technique is also exaggerated 20 times domestic production capacity technologies.
Accompanying drawing explanation
Fig. 1 is the structural representation of the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
Slightly carry the device of natural Broneolum Syntheticum from borneol camphor tree, as shown in Figure 1, comprise extractor 1, first valve 2, No. 1 condenser 3, No. 2 condensers 4, water-and-oil separator 5, air water separator 6, No. 3 condensers 7 and receptor 8.Extractor 1 is for depositing the borneol camphor tree raw material after pulverizing, extractor 1 top is provided with visor, for observing extractor 1, distribute steam coils in extractor 1, for heating in tank, heating jacket is provided with outside extractor 1, material outlet is provided with bottom extractor 1, steam outlet pipe is provided with at extractor 1 top, steam outlet pipe by pipeline respectively with water-and-oil separator 5, air water separator 6 is connected, the pipeline be connected with air water separator 6 is provided with the second valve 9, the pipeline be connected with water-and-oil separator 5 is provided with the first valve 2, No. 1 condenser 3 and No. 2 condensers 4.Air water separator 6 is connected with No. 3 condensers 7 by pipeline, and No. 3 condensers 7 are connected with receptor 8, and wherein, No. 3 condensers 7 have two or more, are connected in parallel between air water separator 6 and receptor 8.
Owing to containing all kinds of heterogeneity impurity mixtures such as amine leaf essential oil, lipid in borneol camphor tree branches and leaves, when natural Broneolum Syntheticum vaporization distillation, if received together, purity during refining can be brought to be difficult to the problem improved.So the present invention devises above-mentioned task equipment, when slightly refining, when steam flow is gushed out from extractor 1, being separately separated by by-pass valve control, allowing essential oil, natural Broneolum Syntheticum, water three kinds of materials be separated when thick refining simultaneously.So both can improve natural Broneolum Syntheticum purity more than 10%, while water is separated, also can improve essential oil purity to more than 90%.Separation and Extraction while essential oil, had both saved the energy expenditure of subsequent extracted, also can increase added value, so-called killing three birds with one stone.
Wherein, No. 3 condensers 7 adopt inner dual coil pipes condensation, middle many pore shuntings and external jacket condensation structure, and spent glycol, as refrigerating fulid, carries out freezing treatment by freezing unit, guarantee that in condenser, the temperature of water remains between 0 DEG C ~ 5 DEG C, can adjust according to the actual requirements.When built-in dual coil pipes device can ensure to be with the hot gas flow of borneol to enter condenser, be condensed into rapidly solid-state.Middle many pore shuntings, are alleviate when a large amount of hot gas flow enters condenser to cause the inner instantaneous temperature of condenser too high, adopt many pores to shunt, hot gas flow can be helped to import condenser Homogeneous cooling from all directions, improve borneol and carry yield.External jacket device: in chuck, the moment is full of cooling fluid, to strengthen the constant of condenser internal temperature, is 10m
3extractor completes extraction and provides sufficient guarantee in 35 ~ 40min.
These No. 3 condensers 7 are autocratic condensers of the specialized designs research and development for natural Broneolum Syntheticum Large Copacity extractor rapid extraction, and advantage is: can meet the demand that high-capacity industrialization is produced; Quick cooling can improve the acceptance rate of natural Broneolum Syntheticum, thus improves the relative content of natural Broneolum Syntheticum; Homogeneous cooling both ensure that receiving efficiency, improve the purity of natural Broneolum Syntheticum simultaneously.
Embodiment 2
Slightly should put forward the method for natural Broneolum Syntheticum from borneol camphor tree, utilize the proterties of high pressure steam and natural Broneolum Syntheticum, and use high pressure superheated steam, under 180 DEG C of states, directly act on branches and leaves.Because natural Broneolum Syntheticum boiling point is at about 212 DEG C, natural Broneolum Syntheticum can be allowed to vaporize and to distil.Under high sealing state, carry out condensation-crystallization by autocratic condenser, extraction natural Broneolum Syntheticum.Concrete technology comprises the following steps:
1) pulverize borneol camphor tree branches and leaves, the particle length after pulverizing is no more than 10cm; Preferred 3-5cm.
2) the borneol camphor tree branches and leaves after pulverizing are added extractor, adopt high pressure superheated steam to directly act on branches and leaves, temperature control 180 DEG C, extract 35 ~ 40 minutes;
3) with condenser, condensation is carried out to the natural Broneolum Syntheticum after gasification, collect natural Broneolum Syntheticum; Obtain by product essential oil and water simultaneously.
This Technology instead of originally by the traditional method of water distillation, and extraction time is shortened half, and yield improves 10%, and power consumption reduces 65%, and use steam can reduce discharge of wastewater 99%, this technique is also exaggerated 20 times domestic production capacity technologies.
Claims (6)
1. slightly carry a device for natural Broneolum Syntheticum from borneol camphor tree, it is characterized in that, comprise extractor (1), No. 1 condenser (3), No. 2 condensers (4), water-and-oil separator (5), air water separator (6), No. 3 condensers (7) and receptors (8); Steam outlet pipe is provided with at extractor (1) top, steam outlet pipe is connected with water-and-oil separator (5), air water separator (6) respectively by pipeline, the pipeline be connected with air water separator (6) is provided with the second valve (9), the pipeline be connected with water-and-oil separator (5) is provided with the first valve (2), No. 1 condenser (3) and No. 2 condensers (4); Air water separator (6) is connected with No. 3 condensers (7) by pipeline, and No. 3 condensers (7) are connected with receptor (8).
2. the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree according to claim 1, is characterized in that: on described extractor (1) top, establish visor, for observing extractor (1).
3. the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree according to claim 1, it is characterized in that: described extractor (1) is for depositing the borneol camphor tree raw material after pulverizing, distribute steam coils in extractor (1), outside extractor (1), be provided with heating jacket, be provided with material outlet in extractor (1) bottom.
4. the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree according to claim 1, is characterized in that: No. 3 described condensers (7) have two or more, are connected in parallel between air water separator (6) and receptor (8).
5. the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree according to claim 1, it is characterized in that: No. 3 described condensers (7) adopt inner dual coil pipes condensation, middle many pore shuntings and external jacket condensation structure, spent glycol is as refrigerating fulid, carry out freezing treatment by freezing unit, guarantee that in condenser, the temperature of water remains between 0 DEG C ~ 5 DEG C.
6. the device slightly carrying natural Broneolum Syntheticum from borneol camphor tree according to claim 1, is characterized in that: described extractor (1) is 10m
3extractor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510113447.4A CN104711123B (en) | 2015-03-16 | 2015-03-16 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510113447.4A CN104711123B (en) | 2015-03-16 | 2015-03-16 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
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| CN104711123A true CN104711123A (en) | 2015-06-17 |
| CN104711123B CN104711123B (en) | 2018-02-23 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113860998A (en) * | 2021-10-28 | 2021-12-31 | 湖南复新龙脑农业科技发展有限公司 | Process for separating natural borneol of borneol camphor |
| TWI767710B (en) * | 2021-05-18 | 2022-06-11 | 台大龍腦生物科技股份有限公司 | Intelligent device for extracting natural borneol from borneo camphor |
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| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| CN101279893A (en) * | 2008-05-26 | 2008-10-08 | 湖南省新晃县龙脑开发有限责任公司 | Efficient extracting device for natural borneol |
| CN102319517A (en) * | 2011-09-02 | 2012-01-18 | 江苏斯威森生物医药工程研究中心有限公司 | Extraction tank |
| CN103480169A (en) * | 2012-06-11 | 2014-01-01 | 拉曼大学 | Method to extract borneol from the exudates of dryobalanops aromatica |
| CN103601619A (en) * | 2013-11-01 | 2014-02-26 | 宜昌万森生态科技发展有限公司 | Extraction method and extraction equipment of natural borneol |
| CN204607960U (en) * | 2015-03-16 | 2015-09-02 | 江苏金叶子生物科技有限公司 | A kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree |
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2015
- 2015-03-16 CN CN201510113447.4A patent/CN104711123B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| CN101279893A (en) * | 2008-05-26 | 2008-10-08 | 湖南省新晃县龙脑开发有限责任公司 | Efficient extracting device for natural borneol |
| CN102319517A (en) * | 2011-09-02 | 2012-01-18 | 江苏斯威森生物医药工程研究中心有限公司 | Extraction tank |
| CN103480169A (en) * | 2012-06-11 | 2014-01-01 | 拉曼大学 | Method to extract borneol from the exudates of dryobalanops aromatica |
| CN103601619A (en) * | 2013-11-01 | 2014-02-26 | 宜昌万森生态科技发展有限公司 | Extraction method and extraction equipment of natural borneol |
| CN204607960U (en) * | 2015-03-16 | 2015-09-02 | 江苏金叶子生物科技有限公司 | A kind of device slightly carrying natural Broneolum Syntheticum from borneol camphor tree |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI767710B (en) * | 2021-05-18 | 2022-06-11 | 台大龍腦生物科技股份有限公司 | Intelligent device for extracting natural borneol from borneo camphor |
| CN113860998A (en) * | 2021-10-28 | 2021-12-31 | 湖南复新龙脑农业科技发展有限公司 | Process for separating natural borneol of borneol camphor |
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| CN104711123B (en) | 2018-02-23 |
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