CN201990619U - Lentinan extraction, separation, purification and concentration device - Google Patents
Lentinan extraction, separation, purification and concentration device Download PDFInfo
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- CN201990619U CN201990619U CN2011200692786U CN201120069278U CN201990619U CN 201990619 U CN201990619 U CN 201990619U CN 2011200692786 U CN2011200692786 U CN 2011200692786U CN 201120069278 U CN201120069278 U CN 201120069278U CN 201990619 U CN201990619 U CN 201990619U
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
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Abstract
The utility model discloses a lentinan extraction, separation, purification and concentration device which comprises an extraction tank, a separation and purification system and a concentration system, and is characterized in that a microwave device and an ultrasonic device are arranged on the extraction tank; the separation and purification system is a ceramic membrane separation device; and the concentration system is a reverse osmosis concentration device. The lentinan extraction, separation, purification and concentration device adopts ultrasonic-microwave collaborative extraction, integrates the characteristics of microwave and ultrasonic extraction, makes up for the defects of the respective ultrasonic and microwave extraction, and has the advantages that: the vibration is uniform, the action in a sample medium is consistent, the treatment capacity is large and the like; and lentinan extract receives ceramic membrane separation and purification as well as reverse osmosis concentration, and compared with plate frame filtration, ion exchange separation and purification as well as evaporation and concentration, the method has good energy-saving and separation and purification effects as well as high impurity removal rate, so that the pressure of follow-up refining is greatly reduced.
Description
Technical field
The present invention relates to field of plant extraction, particularly relate to a kind of extraction, separation and purification and concentrating unit of lentinan.
Background technology
The plant milk extract industry is the year eighties 20th century along with natural health industry development in the world and the raw material industrial field that breaks up out, extensively adopting technology, equipment and the material of aspects such as modern pharmaceutical, chemical industry, healthcare products, food, is a product diversification, application diversification, technical modernization, the international industrial field that good development prospect is arranged in market.Plant milk extract be meant natural phant through extraction and the material that contains effective ingredient, also be the main raw material of plant amedica preparation, and can be widely used in industries such as nutritious supplementary, protective foods, makeup, be the core product on the natural medicaments health-product market.
Lentinan is extraction from the Mycophyta mushroom fruiting body of cultivation, separation, the resulting single polysaccharide of purifying.Has special advantage as antitumor drug: can regulate immunologic function, and make that dosage is low, curative effect is better, toxic side effect is little etc.Mainly do the treatment of malignant tumours such as Digestive tract.Usually be used, exempt the untoward reaction that curative effect produced with chemotherapeutics.Be particularly suitable for the Patients with Gastric Cancer that to perform the operation or to recur, improve patient's life treatment, prolong patient's life.
Traditional lentinan extracting method is a water extraction and alcohol precipitation method, though its technology is simple, extraction yield is low, and the extraction yield of lentinan only is 4%, adopts hot water extraction (80-100 ℃) in addition.He Yingna is 200910074445.3 at application number, a kind of method that adopts dilute acid soln to extract lentinan from champignon stems is disclosed in the application for a patent for invention of patent name for " a kind of method of extracting lentinan from champignon stems ", this method can significantly improve the extraction yield of lentinan, shorten extraction time, reduce energy consumption, but the present invention adopts dilute acid soln to extract lentinan, reaches the refining bigger difficulty of having brought for the later separation purifying.
Summary of the invention
The objective of the invention is at the problems referred to above, it is good to relate to a kind of extraction yield height, separation, purification effect, the extraction of the simple a kind of lentinan of operational path, separation and purification and concentrating unit.
For achieving the above object, technical scheme proposed by the invention is: a kind of extraction of lentinan, separation and purification and concentrating unit, comprise: extractor, separation and purification system, concentration systems, it is characterized in that, microwave device and ultrasonic unit are installed on the described extractor; Described separation and purification system is the ceramic membrane tripping device; Described concentration systems is reverse osmosis concentrated compression apparatus, and described extractor links to each other with the ceramic membrane tripping device by pipeline, and the ceramic membrane tripping device links to each other with reverse osmosis concentrated compression apparatus by the dialysis pipeline.
Further,, it is characterized in that also being equipped with in the described extractor a plurality of traverse baffles, to improve the hydraulic detention time of extracting solution in extractor as a kind of optimal way of the present utility model.
Further, described ceramic membrane tripping device comprises that the head tank, valve, dehvery pump, ceramic film component, the ceramic film component concentrated solution outlet that link to each other successively by feed pipe link to each other with head tank by reflux line.
Further, described reverse osmosis concentrated compression apparatus comprises concentration tank, valve, dehvery pump, security personnel's strainer, high-pressure pump, the reverse osmosis membrane assembly that connects successively by feed pipe; Described reverse osmosis membrane assembly dialyzate outlet links to each other with dialysate tank by the dialysis pipeline, and concentrated solution outlet links to each other with concentration tank by concentrating pipeline; Described ceramic film component dialyzate outlet links to each other with concentration tank by the dialysis pipeline.
Further, the ceramic membrane of installing in the described ceramic membrane tripping device separates the aperture: 0.05 μ m-0.2 μ m.
Further,, on described reflux line and the concentrated pipeline interchanger is installed all, can realizes feed liquid is heated or lowers the temperature as a kind of optimal way of the present utility model.
In sum, it is one that device described in the utility model adopts the collaborative extraction collection of ultrasonic-microwave microwave, ultrasonic extraction characteristics, remedied the independent respectively deficiency of extracting of ultrasonic wave and microwave, and has the effect unanimity of receiving in vibration homogenizing, the sample media, advantages such as treatment capacity is big, the lentinan extracting solution adopts ceramic membrane separation and purification and reverse osmosis concentration, with respect to Plate Filtration, ion-exchange separation, purifying, evaporation concentration, have energy-conservation, separation and purification is effective, the removal of impurity height has significantly reduced follow-up purified pressure.
Description of drawings
Fig. 1 is the utility model structure drawing of device.
Embodiment
Below in conjunction with the drawings and specific embodiments, the utility model is described further.
Shown in Fig. 1 structure drawing of device of the present utility model, a kind of extraction of lentinan, separation and purification and concentrating unit, comprise: microwave device 101 and ultrasonic unit 102 are installed on extractor 1, the extractor 1, and a plurality of traverse baffles 103 are installed also in the extractor 1, to improve the residence time of extracting solution in extractor 1, strengthen microwave and action of ultrasonic waves time, improve yield.Extracting solution in the extractor 1 links to each other with head tank 201 in the ceramic membrane tripping device 2 by pipeline 104.Ceramic membrane tripping device 2 comprises that the head tank 201, valve 202, dehvery pump 203, ceramic film component 205, ceramic film component 205 concentrated solution outlets that link to each other successively by feed pipe 204 link to each other with head tank 201 by reflux line 207, and the outlet of ceramic film component 205 dialyzates links to each other with concentration tank 301 in the reverse osmosis concentrated compression apparatus 3 by the pipeline 206 of dialysing.The ceramic membrane of installing in the ceramic film component 205 separates the aperture: 0.05 μ m-0.2 μ m.Reverse osmosis concentrated compression apparatus 3 comprises concentration tank 301, valve 302, dehvery pump 303, security personnel's strainer 305, high-pressure pump 306, the reverse osmosis membrane assembly 307 that connects successively by feed pipe 304; The outlet of reverse osmosis membrane assembly 307 dialyzates links to each other with dialysate tank 309 by dialysis pipeline 308, and concentrated solution outlet links to each other with concentration tank 301 by concentrating pipeline 310.Also be separately installed with interchanger 208 and interchanger 311 on the concentrated pipeline 207 of ceramic membrane tripping device 2 and reverse osmosis concentrated compression apparatus 3 and the concentrated pipeline 310 in addition.
During concrete enforcement, the champignon stems powder extracts under the synergy of ultrasonic wave and microwave in extractor 1, extracting solution is directly by in 104 incoming stock jars 201 in the pipeline, extracting solution in the head tank 201 pumps in the ceramic film component 205 through dehvery pump 203, impurity such as solid are held back by ceramic membrane, in 207 incoming stock jars 201 of reflux lines, carry out circulating filtration; Too high or too low as feed temperature, can lower the temperature or heat up by interchanger 208, the lentinan dialyzate then enters in the concentration tank 301 by dialysis pipeline 206, lentinan dialyzate in the concentration tank 301 is by feed pipe 304, and through dehvery pump 303 defeated material, security personnel's strainer 305 filters, pump in the reverse osmosis membrane assembly 307 through high-pressure pump 306 again, water molecules sees through reverse osmosis membrane and enters in the dialysate tank through dialysis pipeline 308, the lentinan concentrated solution then enters in the concentration tank 301 by concentrating pipeline 301, it is concentrated to circulate, reach requirement until cycles of concentration, then enter next refining link, too high or too low as feed temperature, can lower the temperature or heat up by interchanger 311.
Although specifically show and introduced the utility model in conjunction with preferred embodiment; but the those skilled in the art should be understood that; in the spirit and scope of the present utility model that do not break away from appended claims and limited; in the form and details the utility model is made various variations, be protection domain of the present utility model.
Claims (7)
1. the extraction of a lentinan, separation and purification and concentrating unit comprise: extractor (1), separation and purification system, concentration systems, it is characterized in that, and microwave device (102) and ultrasonic unit (103) are installed on the described extractor (1); Described separation and purification system is ceramic membrane tripping device (2); Described concentration systems is reverse osmosis concentrated compression apparatus (3), and described extractor (1) links to each other with ceramic membrane tripping device (2) by pipeline (104), and ceramic membrane tripping device (2) links to each other with reverse osmosis concentrated compression apparatus (3) by dialysis pipeline (206).
2. the extraction of a kind of lentinan according to claim 1, separation and purification and concentrating unit is characterized in that also being equipped with in the described extractor (1) a plurality of traverse baffles (104).
3. the extraction of a kind of lentinan according to claim 1 and 2, separation and purification and concentrating unit is characterized in that described ceramic membrane tripping device (2) comprises that the head tank (201), valve (202), dehvery pump (203), ceramic film component (205), ceramic film component (205) concentrated solution outlet that link to each other successively by feed pipe (204) link to each other with head tank (201) by reflux line (207).
4. the extraction of a kind of lentinan according to claim 1 and 2, separation and purification and concentrating unit is characterized in that described reverse osmosis concentrated compression apparatus (3) comprises concentration tank (301), valve (302), dehvery pump (303), security personnel's strainer (305), high-pressure pump (306), the reverse osmosis membrane assembly (307) that connects successively by feed pipe (304); The outlet of described reverse osmosis membrane assembly (307) dialyzate links to each other with dialysate tank (309) by dialysis pipeline (308), concentrated solution outlet links to each other with concentration tank (301) by concentrating pipeline (310), and the outlet of described ceramic film component (201) dialyzate links to each other with concentration tank (301) by dialysis pipeline (206).
5. the extraction of a kind of lentinan according to claim 1 and 2, separation and purification and concentrating unit is characterized in that the ceramic membrane of installing in the described ceramic membrane tripping device (2) separates the aperture and is: 0.05 μ m-0.2 μ m.
6. the extraction of a kind of lentinan according to claim 3, separation and purification and concentrating unit is characterized in that all being equipped with on described reflux line (207) and the concentrated pipeline interchanger (208).
7. the extraction of a kind of lentinan according to claim 4, separation and purification and concentrating unit is characterized in that all being equipped with on the described concentrated pipeline (310) interchanger (311).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2011200692786U CN201990619U (en) | 2011-03-16 | 2011-03-16 | Lentinan extraction, separation, purification and concentration device |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011200692786U CN201990619U (en) | 2011-03-16 | 2011-03-16 | Lentinan extraction, separation, purification and concentration device |
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| CN201990619U true CN201990619U (en) | 2011-09-28 |
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| CN2011200692786U Expired - Fee Related CN201990619U (en) | 2011-03-16 | 2011-03-16 | Lentinan extraction, separation, purification and concentration device |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN105001351A (en) * | 2015-08-31 | 2015-10-28 | 桂林茗兴生物科技有限公司 | Lentinan extraction method |
| CN103232553B (en) * | 2013-05-06 | 2015-11-25 | 陕西理工学院 | A kind of semi continuous extracts the apparatus and method of polyporusum bellatus |
| CN105475959A (en) * | 2015-11-26 | 2016-04-13 | 湖北省农业科学院农产品加工与核农技术研究所 | Method for preparing monosodium glutamate-free seasoning juice from domestic fungus precooked fluid |
| CN107137953A (en) * | 2017-05-31 | 2017-09-08 | 镇江虎瑞生物科技有限公司 | The dynamic extracting device that a kind of microwave is combined with ultrasonic wave |
| CN109370902A (en) * | 2018-12-12 | 2019-02-22 | 张家口康生物科技有限公司 | A kind of continuous extraction process of oat polypeptide |
| CN110613122A (en) * | 2019-10-11 | 2019-12-27 | 上海交通大学 | Drying pretreatment and preparation method for improving extraction rate of cerebroside in mushroom stems |
| CN111303309A (en) * | 2020-02-19 | 2020-06-19 | 王森林 | Microbial polysaccharide extraction element |
| CN112898448A (en) * | 2021-03-15 | 2021-06-04 | 贵州省工程复合材料中心 | Lentinan extraction system and extraction method |
| CN114271418A (en) * | 2020-09-26 | 2022-04-05 | 三原美乐绿色工程科技有限责任公司 | Leaching device and red date processing system thereof |
-
2011
- 2011-03-16 CN CN2011200692786U patent/CN201990619U/en not_active Expired - Fee Related
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103232553B (en) * | 2013-05-06 | 2015-11-25 | 陕西理工学院 | A kind of semi continuous extracts the apparatus and method of polyporusum bellatus |
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN105001351A (en) * | 2015-08-31 | 2015-10-28 | 桂林茗兴生物科技有限公司 | Lentinan extraction method |
| CN105475959A (en) * | 2015-11-26 | 2016-04-13 | 湖北省农业科学院农产品加工与核农技术研究所 | Method for preparing monosodium glutamate-free seasoning juice from domestic fungus precooked fluid |
| CN107137953A (en) * | 2017-05-31 | 2017-09-08 | 镇江虎瑞生物科技有限公司 | The dynamic extracting device that a kind of microwave is combined with ultrasonic wave |
| CN109370902A (en) * | 2018-12-12 | 2019-02-22 | 张家口康生物科技有限公司 | A kind of continuous extraction process of oat polypeptide |
| CN110613122A (en) * | 2019-10-11 | 2019-12-27 | 上海交通大学 | Drying pretreatment and preparation method for improving extraction rate of cerebroside in mushroom stems |
| CN111303309A (en) * | 2020-02-19 | 2020-06-19 | 王森林 | Microbial polysaccharide extraction element |
| CN111303309B (en) * | 2020-02-19 | 2021-12-14 | 洛阳市佳运医疗卫生用品有限公司 | Microbial polysaccharide extraction element |
| CN114271418A (en) * | 2020-09-26 | 2022-04-05 | 三原美乐绿色工程科技有限责任公司 | Leaching device and red date processing system thereof |
| CN112898448A (en) * | 2021-03-15 | 2021-06-04 | 贵州省工程复合材料中心 | Lentinan extraction system and extraction method |
| CN112898448B (en) * | 2021-03-15 | 2022-08-02 | 贵州省工程复合材料中心有限公司 | Lentinan extraction system and extraction method |
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Granted publication date: 20110928 Termination date: 20140316 |