CN201063028Y - Flash point tester for minisize oil plants - Google Patents

Flash point tester for minisize oil plants Download PDF

Info

Publication number
CN201063028Y
CN201063028Y CNU2006201243707U CN200620124370U CN201063028Y CN 201063028 Y CN201063028 Y CN 201063028Y CN U2006201243707 U CNU2006201243707 U CN U2006201243707U CN 200620124370 U CN200620124370 U CN 200620124370U CN 201063028 Y CN201063028 Y CN 201063028Y
Authority
CN
China
Prior art keywords
circuit
cup
naphthaometer
sample cup
oil plant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNU2006201243707U
Other languages
Chinese (zh)
Inventor
刘慧颖
韦锐
肖伟强
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Yangguang Scientific Instrument Manufacturing Co Ltd
Oil Research Institute of General Logistic Department of PLA
Original Assignee
Shanghai Yangguang Scientific Instrument Manufacturing Co Ltd
Oil Research Institute of General Logistic Department of PLA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Yangguang Scientific Instrument Manufacturing Co Ltd, Oil Research Institute of General Logistic Department of PLA filed Critical Shanghai Yangguang Scientific Instrument Manufacturing Co Ltd
Priority to CNU2006201243707U priority Critical patent/CN201063028Y/en
Application granted granted Critical
Publication of CN201063028Y publication Critical patent/CN201063028Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)

Abstract

The utility model relates to a mini oil flash-point tester, which employs a sealing sample cup, a heater arranged outside the cup, an electric arc igniting electrode arranged inside the cup, a plasma testing probe and a temperature sensor and an insulation cover of the sample cup; centering on MCU, the utility model also comprises a keyboard, a display, a R 232 interface, a controlling inspection circuit of an actuator, a temperature-controlling circuit, a flash-fire inspecting circuit and an electric arc igniting circuit; the flash-point value is tested through interval ignition divided according to the temperature and testing the variation of ionization of burning gas; a casing of the utility model uses aluminum alloy materials and is coated with anticorrosion coating, and an anti-shock device is arranged at the casing. The mini oil flash-point tester of the utility model employs the control of a micro-processor, which realizes automatic operation; besides, the sealing sample cup has small volume and uses small quantity of the sample; the plasma testing way has high sensitivity and the test is rapid, thereby the high-effective mini oil flash-point tester is simple, reliable and portable.

Description

Miniature oil plant naphthaometer
Technical field
The utility model relates to a kind of oil plant testing tool, particularly relates to a kind of miniature, quick, safe portable minisize oil plant naphthaometer.
Background technology
Petrochemicals all need to measure the flash-point value of oil plant, existing flash-point detection technique is a kind of method of testing of classics, be by to a small amount of petroleum product samples, its ignition procedures is analyzed, draw the flash-point value parameter of oil product, promising usually manual and automatic two big classes are divided into flame ignition, electric heat ignition two big classes again from ignition way, generally be to carry out in the non-tight container, specimen in use quantity is big, security is relatively poor; Existing multiple flash-point detection means, or visualization artificial judgment, or use the thermocouple assay difference variation, or the variation of working pressure sensor pressure, all there is the detection speed defective of (about 30 minutes) slowly, generally only be adapted at carrying out in the laboratory.
The reagent contamination that causes of non-tight container also allows of no optimist in addition.And existing naphthaometer volume is big, is not easy to vehicle-mountedly and carry, and is not suitable for field work and mobile occasion, as the use of occasions such as refuelling station, oil depot, naval vessel.
The utility model content
For remedying above-mentioned deficiency, the utility model provide a kind of in airtight container, the miniature oil plant of the portable minisize fast naphthaometer that uses arc ignition, adopt plasma sensor to detect.
The miniature oil plant naphthaometer of the utility model, comprise the aluminium alloy casing, panel, display, keyboard, in casing, be provided with a seal sample cup, in described sample cup, a well heater is set, the arc ignition electrode, two detector probe and a temperature sensor, connect keyboard, display, the MCU of R232 interface connects an executor circuit, executor circuit connects temperature control circuit respectively, scintillation testing circuit and arc ignition circuit, described temperature control circuit, the scintillation testing circuit also is connected with MCU with the arc ignition circuit, described temperature control circuit connects described temperature sensor, described scintillation testing circuit connects described detector probe, arc ignition electrode under described arc ignition circuit connects, leave rim of a cup on the described sample cup, described rim of a cup has the tight flap that covers with matching.
The miniature oil plant naphthaometer of the utility model, described sample cup has muff.
The miniature oil plant naphthaometer of the utility model, described detector probe are two metal probes that separate installation.
The miniature oil plant naphthaometer of the utility model, described well heater are insulating mounting heating wire in stainless steel sleeve.
The miniature oil plant naphthaometer of the utility model, described casing adopts aluminum alloy materials, and is covered with corrosion-resistant coating.
The miniature oil plant naphthaometer of the utility model is added with bump protection ring between described sample cup and the casing.
The miniature oil plant naphthaometer of the utility model, the control of application microprocessor has realized automation mechanized operation, and the seal sample cup volumes is little, amount of samples is little, the plasma detection mode is highly sensitive, detection is quick, is a kind of efficient mini oil plant naphthaometer simple, reliable, easy to carry.
Description of drawings
Fig. 1 is the complete machine synoptic diagram of the miniature oil plant naphthaometer of the utility model;
Fig. 2 is the miniature oil plant naphthaometer of a utility model sample cup inner structure synoptic diagram;
Fig. 3 is the circuit block diagram of the miniature oil plant naphthaometer of the utility model.
Embodiment
For further setting forth the utility model, do more detailed explanation below in conjunction with embodiment.
Present embodiment is made up of sample cup 1, well heater 2, arc ignition electrode 3, scintillation detector probe 4, temperature sensor 7 and interlock circuit, sample cup 1 is put into the 3-5ml tested sample, put on well heater 2 and sealing, under the control of respective actuators circuit, sample in the cup is heated, when reaching uniform temperature, light the ignition mixed gas by arc ignition electrode 3, scintillation detector probe 4 is sent flash fire signal at this moment into MCU, and the temperature value during simultaneous temperature sensor 7 record scintillations is finished test.
Fig. 1 is the complete machine panel synoptic diagram of present embodiment, sees at casing 10 upper surfaces that from appearance sample cup 1, display 11 and keyboard 12 are arranged.Certainly this is not unique layout, shows to be a kind of arrangement mode among the figure.
The cut-open view of sample cup 1 is seen Fig. 2, and sample cup 1 has well heater 2, and well heater 2 also can be made the respective cups type, wraps in outside the sample cup 1; Wall of cup is provided with arc ignition electrode 3, scintillation detector probe 4 and temperature sensor 7; In order to keep temperature, energy efficient, the outer muff 8 that is surrounded by of cup; For reaching sealing, flap 5 with matching is arranged on the rim of a cup 6, this flap 5 is connected with rim of a cup 6, can adopt thread forms, also can adopt the form of buckle fastening, will reach sealing effectiveness in a word.
Sample cup 1 is connected with casing 10 by shock structure 9; for each parts that stretches out the sample cup 1 outside the casing 10; establish specially with protective cover 14; this protective cover 14 can be raised in use; the time spent does not close; with buckle 15 lockings, in case in carrying the way, damage arc ignition electrode 3, scintillation detector probe 4, the temperature sensor 7 on the sample cup 1 and be connected electric wire.
As Fig. 3, shown in Figure 1, be equipped with in the utility model machine and detect control circuit 18, form by scintillation testing circuit, arc ignition circuit, temperature control circuit, executive circuit and MCU, the output of MCU is connected respectively to arc ignition circuit, temperature control circuit and scintillation testing circuit through executive circuit, and detected flash fire signal of scintillation testing circuit and the detected temperature data of temperature control circuit are then directly sent into MCU.Detect control circuit and sample cup 1 part and separately settle, the temperature of avoiding well heater is to detecting the influence of control circuit.The output that detects control circuit 18 connects the R232 interface, in order to be connected with computing machine; The switch 17 that detects control circuit 18 is located at the back of casing 10.Just signal among the figure detects control circuit board 18 and poises, and this wiring board is on the support that is fixed in the casing 10 in the reality.
After beginning to detect, MCU connects the power supply of well heater 2 by actuator, begin heating, the temperature signal of simultaneous temperature sensor 7 is delivered to MCU after temperature control circuit amplifies sampling, when MCU detects temperature to a design temperature constantly, send firing command to the arc ignition circuit, send to the scintillation testing circuit simultaneously and detect instruction; After the arc ignition circuit is received firing command, send low pressure high-frequency arc strike electric current, on arc ignition electrode 3, pull out electric arc, cause the mixed gas detonation in the sample cup 1; With it simultaneously, scintillation detector probe 4 the increasing of gas ionization degree during by detonation detects flash fire signal, sends into MCU after amplifying sample conversion by the scintillation observation circuit, MCU receives flash fire signal, and the temperature value of noting at that time is exactly the flashing point of tested sample.
The oil plant that flashing point is high can not be lighted when heating-up temperature is not enough, and MCU does not receive flash fire signal, will give an order to continue to heat, the detection of lighting a fire once more when the higher temperature of the next one; Repeatedly igniting detects, till detecting the scintillation value.
Present embodiment is made miniature oil plant naphthaometer, adopts anticorrosion aluminium alloy casing.Durable, anticorrosion anti-salt protection against the tide, volume is small and exquisite, and adds vibration abatement, between sample cup 1 and casing 10, between circuit board and the casing 10.
The miniature oil plant naphthaometer of the utility model, leading indicator is as follows:
Flash-point test specification :-20 ℃-250 ℃
Programming rate: 1-12 ℃/minute
Sample size: 3-5ml
Measuring accuracy :≤3 ℃
Working environment :-10-45 ℃
Physical dimension: 164 * 340 * 160
Weight:<4kg
The miniature oil plant naphthaometer of the utility model, detects fewly with sample size at automaticity height, detection sensitivity height, does not externally leak naked light simultaneously, safe, be core with microprocessor, simple to operate, easy to use, volume is small and exquisite, very occasion such as suitable open-air oil depot is used.

Claims (6)

1. miniature oil plant naphthaometer, comprise aluminium alloy casing (10), panel (13), display (11), keyboard (12), it is characterized in that, in casing (10), be provided with a seal sample cup (1), in described sample cup (1), a well heater (2) is set, arc ignition electrode (3), two detector probe (4) and a temperature sensor (7), connect keyboard (12), display (11), MCU connection-the executor circuit of R232 interface (16), executor circuit connects temperature control circuit respectively, scintillation testing circuit and arc ignition circuit, described temperature control circuit, the scintillation testing circuit also is connected with MCU with the arc ignition circuit, described temperature control circuit connects described temperature sensor (7), described scintillation testing circuit connects described detector probe, arc ignition electrode (3) under described arc ignition circuit connects, leave rim of a cup (6) on the described sample cup (1), described rim of a cup (6) has the tight flap (5) that covers with matching.
2. according to the miniature oil plant naphthaometer of claim 1, it is characterized in that described sample cup (1) has muff (8).
3. according to the miniature oil plant naphthaometer of claim 2, it is characterized in that described detector probe (4) is two metal probes that separate installation.
4. according to the miniature oil plant naphthaometer of claim 3, it is characterized in that described well heater (2) is an insulating mounting heating wire (21) in stainless steel sleeve (22).
5. according to the miniature oil plant naphthaometer of claim 4, it is characterized in that described aluminium alloy casing (10) outside surface is covered with corrosion-resistant coating.
6. according to the miniature oil plant naphthaometer of claim 5, it is characterized in that being added with bump protection ring between described sample cup (1) and the casing (10).
CNU2006201243707U 2006-07-10 2006-07-10 Flash point tester for minisize oil plants Expired - Fee Related CN201063028Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2006201243707U CN201063028Y (en) 2006-07-10 2006-07-10 Flash point tester for minisize oil plants

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2006201243707U CN201063028Y (en) 2006-07-10 2006-07-10 Flash point tester for minisize oil plants

Publications (1)

Publication Number Publication Date
CN201063028Y true CN201063028Y (en) 2008-05-21

Family

ID=39451411

Family Applications (1)

Application Number Title Priority Date Filing Date
CNU2006201243707U Expired - Fee Related CN201063028Y (en) 2006-07-10 2006-07-10 Flash point tester for minisize oil plants

Country Status (1)

Country Link
CN (1) CN201063028Y (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105136853A (en) * 2015-07-24 2015-12-09 中国石油化工股份有限公司 Closed-cup flash point tester having disposable coaster and special-use press-compacting apparatus thereof
CN105445236A (en) * 2014-08-22 2016-03-30 上海出入境检验检疫局工业品与原材料检测技术中心 Cold filter plugging point tester
CN106468673A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of convenient flash point tester for minisize oil plants converging data
CN106468672A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants of drive charge function
CN106468674A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants with alarm function
CN106468675A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants with print record function
CN106468676A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of portable minisize oil plant naphthaometer
CN107340358A (en) * 2016-12-01 2017-11-10 上海化工研究院有限公司 A kind of chain-plate type substance combustion screening plant
CN107389855A (en) * 2017-07-19 2017-11-24 上海化工研究院有限公司 A kind of combustibility test device for tilting internal heat type liquid vapour
CN111766269A (en) * 2020-08-11 2020-10-13 合肥国轩高科动力能源有限公司 Automatic testing system and method for closed flash point of lithium ion battery electrolyte

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105445236A (en) * 2014-08-22 2016-03-30 上海出入境检验检疫局工业品与原材料检测技术中心 Cold filter plugging point tester
CN105136853A (en) * 2015-07-24 2015-12-09 中国石油化工股份有限公司 Closed-cup flash point tester having disposable coaster and special-use press-compacting apparatus thereof
CN106468673A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of convenient flash point tester for minisize oil plants converging data
CN106468672A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants of drive charge function
CN106468674A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants with alarm function
CN106468675A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of flash point tester for minisize oil plants with print record function
CN106468676A (en) * 2015-08-17 2017-03-01 哈尔滨市宏昌石油助剂有限公司 A kind of portable minisize oil plant naphthaometer
CN107340358A (en) * 2016-12-01 2017-11-10 上海化工研究院有限公司 A kind of chain-plate type substance combustion screening plant
CN107340358B (en) * 2016-12-01 2019-11-12 上海化工研究院有限公司 A kind of chain-plate type substance combustion screening plant
CN107389855A (en) * 2017-07-19 2017-11-24 上海化工研究院有限公司 A kind of combustibility test device for tilting internal heat type liquid vapour
CN107389855B (en) * 2017-07-19 2019-10-22 上海化工研究院有限公司 A kind of combustibility test device tilting internal heat type liquid vapour
CN111766269A (en) * 2020-08-11 2020-10-13 合肥国轩高科动力能源有限公司 Automatic testing system and method for closed flash point of lithium ion battery electrolyte

Similar Documents

Publication Publication Date Title
CN201063028Y (en) Flash point tester for minisize oil plants
CN102253083B (en) Detonation performance test method for high-energy imploding explosive
CN101718725B (en) Device for measuring sample thermo-physical property in situ
US4140004A (en) Apparatus for determining the explosion limits of a flammable gas
CN201156037Y (en) Pyrotechnic compound combustion and explosion performance detector
CN109060879B (en) Ultrahigh-speed ammunition throat liner ablation performance testing device and testing method
CN104535614A (en) Automatic measuring device and method for flash point of insulating oil special for electric power
CN203786068U (en) Visualized bidirectional ignition combustion chamber for experiment
CN114137024B (en) System and method for testing burnout characteristics of combustible fluid under variable temperature and variable humidity conditions
CN102042994A (en) Temperature test device for ignition point of explosive
CN104181199A (en) Ignition energy variable completely-transparent pipeline gas explosion experiment platform and method
CN107656031A (en) Gases at high pressure Impulsive load Testing Method of Safety for energetic material
CN201607417U (en) Unit for measuring ignition temperature of gunpowder
CN101451969B (en) Open flash point detection device for petroleum and petroleum products
CN112083040A (en) Method for testing flash point of flammable liquid under high-pressure environment
CN201449389U (en) Air mixture explosion testing device
CN106093298B (en) A kind of Propellant combustion gas composition test method
CN104792823A (en) Device for testing burning and explosion characteristics of gas phase in reaction process
CN108225134A (en) Sound, light, gas harvester after a kind of priming system explosion
CN202018246U (en) Output performance detecting system for ignition initiating explosive device
CN102565127A (en) Open flashing point automatic detection device for petroleum and petroleum products
CN102192691A (en) Quantification testing system for artillery primer output energy
CN201269817Y (en) Aerosol can combustion test instrument
CN208109739U (en) The micro full-automatic analyzer of close flash point
CN108918355B (en) Method for evaluating explosion sensitivity parameters of low-density polyethylene powder

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20080521

Termination date: 20100710