CN102565127A - Open flashing point automatic detection device for petroleum and petroleum products - Google Patents

Open flashing point automatic detection device for petroleum and petroleum products Download PDF

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Publication number
CN102565127A
CN102565127A CN2010105933774A CN201010593377A CN102565127A CN 102565127 A CN102565127 A CN 102565127A CN 2010105933774 A CN2010105933774 A CN 2010105933774A CN 201010593377 A CN201010593377 A CN 201010593377A CN 102565127 A CN102565127 A CN 102565127A
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CN
China
Prior art keywords
point
automatic detection
detection device
petroleum products
flash
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Pending
Application number
CN2010105933774A
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Chinese (zh)
Inventor
王根忠
袁普俊
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JIANGFEN ELECTRICAL ANALYZERS CO Ltd JIANGSU
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JIANGFEN ELECTRICAL ANALYZERS CO Ltd JIANGSU
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Application filed by JIANGFEN ELECTRICAL ANALYZERS CO Ltd JIANGSU filed Critical JIANGFEN ELECTRICAL ANALYZERS CO Ltd JIANGSU
Priority to CN2010105933774A priority Critical patent/CN102565127A/en
Publication of CN102565127A publication Critical patent/CN102565127A/en
Pending legal-status Critical Current

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Abstract

The invention discloses an open flashing point automatic detection device for petroleum and petroleum products, mainly comprising an automatic detecting arm, a sequence feeding disc, sample detecting cups, a heating device, a power-driven device and a control and detection circuit, wherein the automatic detecting arm is provided with a lifting screw at the tail end, with a temperature sensor, a flashing point detecting anode and cathode at the head end, and with a gas ignition arm, a high voltage ignition anode and an ignition detecting sensor; there are 6-10 sample detecting cups circumferentially and uniformly arranged on the feeding disc; the heating device is arranged below the feeding disc and provided with a lifting mechanism. The device is used for automatic detection of the petroleum and petroleum products open flashing point, has simple operation, high degree of automation, accurate and reliable measurement, and has obvious improvement compared to the existing artificial detection device.

Description

Oil and petroleum products open flash point automatic detection device
Technical field
The present invention relates to a kind of automatic sequence sample detection device, be used for detecting automatically the open flash point of oil and petroleum products.
Background technology
GB GB/T261-83 strict regulations the detection method of open flash point of oil and petroleum products.Under the condition of these strict regulations, traditional assay method utilizes combustible gas to carry out the manual firing exactly, scanning, and artificial temperature adjustment, the moment of manual observation sample generation flash-point is by the sample flash temperature value of the mercury slug indication of thermometer.The apparatus and method complex operation of this manual detection, measuring error is big, uses inconvenient.
Summary of the invention
The object of the present invention is to provide a kind of easy and simple to handle, automaticity is high, measure oil and petroleum products open flash point automatic detection device accurately and reliably.
Technical scheme of the present invention is: oil and petroleum products open flash point automatic detection device; Mainly constitute by automatic detection arm, sequence sample introduction dish, sample detection cup, heating arrangement, Power Drive Unit and control and testing circuit; Said automatic detection arm tail end is provided with the lifting screw perpendicular to sequence sample introduction dish; Head is provided with gas ignition arm, the high-tension ignition utmost point, temperature sensor, flash-point detection anode and negative electrode, and it is 6~10 that said sample detects cup, evenly is arranged on the sequence sample introduction dish by circumferencial direction; Said heating arrangement is positioned at sequence sample introduction dish below, and has elevating mechanism.
Further scheme is: said Power Drive Unit is motor one cogwheel gearing; Said flash-point detects anode for being mutually 120 0Three of Y shape detect pins, process by platinum wire or chromium steel silk, it is the aluminium ring that flash-point detects negative electrode; Distance is 7mm between said detection pin needle point and the aluminium ring, and current potential is 10KV; The igniting position is provided with the igniting detecting sensor in this device.
The course of work of this device is: sample (liquid or thick liquid) is respectively charged into individual (n=6~10) sample of n detects a groove line (quantitatively volume) of extremely stipulating in the cup, put into sample by numbering and detect cup.Start instrument, let instrument be in original state to be detected.Next, on the panel of control device, configure the flash temperature value (be also referred to as preflashing point temperature value, this value is than low 10 ℃ of actual flash-point value usually) that each sample is pre-estimated.The actuating unit working routine is positioned at the beneath well heater of sample detection cup sample is heated automatically.The rate of heat addition of this moment is higher, generally is set at 6~10 ℃ (programmed control).Specimen temperature is by the specimen temperature sensor.When specimen temperature reaches preflashing point temperature value; The gas control valve of gas ignition arm is opened; High-tension ignition limit fire; The end of gas ignition arm produces the high flare of 2mm immediately, and the motor that drives the gas ignition arm makes the gas ignition arm detect between the cup and the high-tension ignition utmost point at sample and does periodic horizontal backswing campaign.In this process, make the rate of heat addition slow down, generally be set at 1~2 ℃ (programmed control).When the medium between flash-point detection anode and negative electrode is air or oil and Air mixing gas; Flash-point detects between anode and the negative electrode and does not produce pulse; In case sample produces scintillation, promptly specimen temperature reaches flash temperature, and the medium that flash-point detects between anode and the negative electrode just becomes flame; Flash-point detects between anode and the negative electrode and produces pulse, and device can detect the signaling point that the sample flash-point takes place immediately.Device control circuit reads the specimen temperature value that the specimen temperature sensor is experienced rapidly, stores the concurrent order of losing one's life of this value, closes gas control valve.
And then, instrument under the order of programmed instruction, the elevating mechanism of the automatic detection arm that rises simultaneously and decline sample heating arrangement, its position is by the control of photoelectricity or contact switch.After this command execution, next instrument carries out the rotating mechanism of interval stage by stage of sample introduction dish, treats that the sample introduction dish turns over 360 0After the angle of/n, programmed instruction command device descend simultaneously automatic detection arm and rising sample heating arrangement, next, instrument repeats the testing of second sample.Directly all accomplish from n sample analysis, computer writes down the flash-point value of n sample automatically, and the request printing lets the user freely select.Instrument lets instrument get into the detected state of next cycle automatic rise detection arm and decline sample heating arrangement.
Scintillation when taking place in sample; Certain top position that generally is positioned at sample detection cup groove occurs at random; Pattern is that half sample detects about the cup round mouth, and existing open flash point detection device generally only has place flash-point detection position point, easily omission sample flash-point origination point.This pick-up unit guarantees that along sample three the flash-point detection position points that detected cup round mouth place uniform Design sample captures the flash of light origination point accurately in the moment that scintillation takes place.
The gas ignition arm through the constraint of fine motion contact switch, is done horizontal backswing campaign under the driving of drive motor.The end of gas ignition arm produces the high flare of 2mm.Sometimes, under unexpected situation, the flare that 2mm is high can extinguish.When the backswing of the end of gas ignition arm to igniting during detecting sensor, the igniting detecting sensor will detect flare to be extinguished, and restarts the high-tension ignition utmost point and produces flare.Directly after sample produces scintillation, close the igniting source of the gas, stop scanning.
Flash-point detects anode and detects being directly proportional with the current potential Vi that flash-point detects between the negative electrode with flash-point detection anode apart from a between the negative electrode with flash-point.Vi is about 10KV in this device, about a=7mm, detects effective.
Description of drawings
Fig. 1 is a structural representation of the present invention;
Fig. 2 is automatic detection arm structural representation.
Embodiment
Referring to accompanying drawing; Oil and petroleum products open flash point automatic detection device detect cup 4, heating arrangement 7, Power Drive Unit 10, support 2 and control by automatic detection arm 6, sequence sample introduction dish 3, sample and control circuit (not drawing among the figure) constitutes; Automatically the detection arm tail end is provided with the lifting screw 5 perpendicular to the sample introduction dish, and head is provided with temperature sensor 11, is mutually 120 0Three of Y shape detect pins 12, aluminium ring 13; Detecting pin is processed by platinum wire; Distance is 7mm between needle point and the aluminium ring, and current potential is 10KV, and detection arm head relevant position is provided with gas ignition arm, the high-tension ignition utmost point and igniting detecting sensor automatically; Six samples detect cup and evenly are arranged on the sequence sample introduction dish by circumferencial direction; The heating arrangement 7 that has elevating mechanism 9 is arranged on sample introduction dish below, and each sample cup can go to the relevant position of heating arrangement successively under Power Drive Unit 10 drives, and Power Drive Unit is made up of motor 1, gear set 8 and bearing etc.

Claims (5)

1. oil and petroleum products open flash point automatic detection device; It is characterized in that this device mainly detects cup, heating arrangement, Power Drive Unit and control by automatic detection arm, sequence sample introduction dish, sample and testing circuit constitutes; Said automatic detection arm tail end is provided with the lifting screw perpendicular to sequence sample introduction dish; Head is provided with gas ignition arm, the high-tension ignition utmost point, temperature sensor, flash-point detection anode and negative electrode, and it is 6~10 that said sample detects cup, evenly is arranged on the sequence sample introduction dish by circumferencial direction; Said heating arrangement is positioned at sequence sample introduction dish below, and has elevating mechanism.
2. by said oil of claim 1 and petroleum products open flash point automatic detection device, it is characterized in that said Power Drive Unit is motor one cogwheel gearing.
3. by said oil of claim 1 and petroleum products open flash point automatic detection device, it is characterized in that said flash-point detects anode for being mutually 120 0Three of Y shape detect pins, process by platinum wire or chromium steel silk, it is the aluminium ring that flash-point detects negative electrode.
4. by said oil of claim 3 and petroleum products open flash point automatic detection device, it is characterized in that distance is 7mm between said detection pin needle point and the aluminium ring, current potential is 10KV.
5. by said oil of claim 1 and petroleum products open flash point automatic detection device, it is characterized in that the igniting position is provided with the igniting detecting sensor in this device.
CN2010105933774A 2010-12-17 2010-12-17 Open flashing point automatic detection device for petroleum and petroleum products Pending CN102565127A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010105933774A CN102565127A (en) 2010-12-17 2010-12-17 Open flashing point automatic detection device for petroleum and petroleum products

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010105933774A CN102565127A (en) 2010-12-17 2010-12-17 Open flashing point automatic detection device for petroleum and petroleum products

Publications (1)

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CN102565127A true CN102565127A (en) 2012-07-11

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104914131A (en) * 2015-06-04 2015-09-16 上海出入境检验检疫局工业品与原材料检测技术中心 Automatic trace double-flash-point detection device
CN104990957A (en) * 2015-08-07 2015-10-21 太仓市隆纺油剂有限公司 Automatic opening type mineral oil flash point testing device
CN105116014A (en) * 2015-08-27 2015-12-02 泉州市全通光电科技有限公司 Automatic closed-cup flash point tester
CN105445325A (en) * 2015-12-30 2016-03-30 重庆精榜高分子材料有限公司 Opening type flash point test equipment for high polymer material
CN109323956A (en) * 2017-07-31 2019-02-12 泰奥星(天津)有限公司 Air release value analyzer
CN117890428A (en) * 2024-03-13 2024-04-16 乐山市通达交通勘察设计有限责任公司 Asphalt flash point detection device

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001174468A (en) * 1999-12-15 2001-06-29 Petroleum Energy Center Automatic testing system
CN2742434Y (en) * 2004-11-10 2005-11-23 鲁德林 Tester for petroleum flash point
CN2903982Y (en) * 2006-05-19 2007-05-23 淄博三泵科森仪器有限公司 Fully automatic open flushing point tester
CN101451969A (en) * 2007-11-29 2009-06-10 江苏江分电分析仪器有限公司 Open flash point detection device for petroleum and petroleum products
CN201945570U (en) * 2010-12-17 2011-08-24 江苏江分电分析仪器有限公司 Device for automatically detecting opening flash points of petroleum and petroleum product

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001174468A (en) * 1999-12-15 2001-06-29 Petroleum Energy Center Automatic testing system
CN2742434Y (en) * 2004-11-10 2005-11-23 鲁德林 Tester for petroleum flash point
CN2903982Y (en) * 2006-05-19 2007-05-23 淄博三泵科森仪器有限公司 Fully automatic open flushing point tester
CN101451969A (en) * 2007-11-29 2009-06-10 江苏江分电分析仪器有限公司 Open flash point detection device for petroleum and petroleum products
CN201945570U (en) * 2010-12-17 2011-08-24 江苏江分电分析仪器有限公司 Device for automatically detecting opening flash points of petroleum and petroleum product

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104914131A (en) * 2015-06-04 2015-09-16 上海出入境检验检疫局工业品与原材料检测技术中心 Automatic trace double-flash-point detection device
CN104990957A (en) * 2015-08-07 2015-10-21 太仓市隆纺油剂有限公司 Automatic opening type mineral oil flash point testing device
CN105116014A (en) * 2015-08-27 2015-12-02 泉州市全通光电科技有限公司 Automatic closed-cup flash point tester
CN105445325A (en) * 2015-12-30 2016-03-30 重庆精榜高分子材料有限公司 Opening type flash point test equipment for high polymer material
CN105445325B (en) * 2015-12-30 2019-05-24 重庆精榜高分子材料有限公司 The open type flash-point test equipment of high molecular material
CN109323956A (en) * 2017-07-31 2019-02-12 泰奥星(天津)有限公司 Air release value analyzer
CN117890428A (en) * 2024-03-13 2024-04-16 乐山市通达交通勘察设计有限责任公司 Asphalt flash point detection device
CN117890428B (en) * 2024-03-13 2024-05-14 乐山市通达交通勘察设计有限责任公司 Asphalt flash point detection device

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Application publication date: 20120711