CN1947606A - Additives for modifying reproduced tobacco leaves, prepn. method and use thereof - Google Patents
Additives for modifying reproduced tobacco leaves, prepn. method and use thereof Download PDFInfo
- Publication number
- CN1947606A CN1947606A CN 200610048738 CN200610048738A CN1947606A CN 1947606 A CN1947606 A CN 1947606A CN 200610048738 CN200610048738 CN 200610048738 CN 200610048738 A CN200610048738 A CN 200610048738A CN 1947606 A CN1947606 A CN 1947606A
- Authority
- CN
- China
- Prior art keywords
- modifying
- additives
- tobacco leaves
- reproduced
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
A modifying additive for preparing the tobacco leaf sheet by paper-making method is prepared through proportionally adding acidic proteinase, composite pectase, composite neutral cellulase and neutral lipase in water, stirring, filtering and taking clear liquid. It can be used to treat tobacco stems for improving the flavouring component in liquid extract and the physical properties of tobacco stem and the looseness of tobacco leaf sheet.
Description
Technical field
The invention belongs to tobacco leaf reconstruction technique field, be specifically related to a kind of property-modifying additive that can effectively improve the papermaking-method reconstituted tobaccos suction quality.Simultaneously, the invention still further relates to a kind of preparation method and using method of described property-modifying additive.
Background technology
At present, World tobacco industry is more and more general to the use of papermaking-method reconstituted tobaccos, this mainly be because, papermaking-method reconstituted tobaccos have other kind reconstituted tobacco incomparable advantage: good as filling capacity, physical and mechanical properties is good, human intervention is strong, tar content is low, is convenient to storage and transportation etc.The raw materials used tobacco waste that is mainly of papermaking-method reconstituted tobaccos, wherein about 50% is offal.Owing to the perfume quantity that offal itself is contained is less, the lignin amount is bigger, and fragrance is flat, the hot sense of flue gas is heavier, therefore, and all the time, how to reduce papermaking-method reconstituted tobaccos assorted gas content, optimize mouthfeel, just become numerous tobacco manufacturing enterprise and urgently wish the technical barrier that solves.Address this problem, the most effective way is exactly an advantage of utilizing the papermaking-method reconstituted tobaccos human intervention strong, sets about from production link, improves the suction quality of reconstituted tobacco by the improved production technological parameter.
Typical papermaking-method reconstituted tobaccos technological process comprises: prescription design, raw material are prepared, extraction concentrates, slurrying is manufactured paper with pulp and coating is cut.People can select to set about changing from each process procedure of producing the qualitative characteristics of product, and extraction enriching section wherein is a very important process section, separates the odor characteristic and suction quality that the fragrance component that obtains has determined the reconstituted tobacco product to a great extent by extracting.Simultaneously, if extraction concentration technique handle well, not only favourable, and also will bring wholesome effect to follow-up slurrying, the process of manufacturing paper with pulp to the physical and chemical index and the suction quality thereof of papermaking-method reconstituted tobaccos.But the technique effect of existing extraction concentration technique still can not be satisfactory.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of additives for modifying reproduced tobacco leaves is provided, extraction enriching section at papermaking-method reconstituted tobaccos, the utilization biological enzyme formulation is handled offal, make macromolecular substances such as pectin in the offal, protein, degrade, change into small-molecule substance, thereby improve the aroma component of extract, make the extraction of active ingredient more complete.Simultaneously, improve the physical behavior of offal, beating energy consumption is reduced, drainability was good when online was manufactured paper with pulp, and improved the gas porosity of sheet base.
Another object of the present invention is to provide a kind of method for preparing described additives for modifying reproduced tobacco leaves.
The present invention also aims to provide a kind of method of utilizing described additives for modifying reproduced tobacco leaves to improve the papermaking-method reconstituted tobaccos quality.
Purpose of the present invention is achieved by the following technical programs.
A kind of additives for modifying reproduced tobacco leaves is made up of the raw material of following weight parts: 1～3 part of acid protease, 1.5～3 parts of compound pectinases, 0.5～1 part of compound neutral cellulase, 0.1～1 part of neutral lipase.
In order to reach better effect, the enzyme activity of various enzymes is preferably respectively in the raw material: acid protease enzyme activity 9～110,000 u/g, compound pectinase enzyme activity 250～3,000,000 u/g, compound neutral cellulase enzyme activity 9～110,000 u/g, neutral lipase enzyme activity 3500～4500u/g.
A kind of preparation method of additives for modifying reproduced tobacco leaves takes by weighing each raw material by described weight portion, places 90～100 parts water to mix raw material and stirs 13～17 minutes, and filtered, and gets clear liquid and is required property-modifying additive.
The present invention also provides a kind of using method of additives for modifying reproduced tobacco leaves, and this method may further comprise the steps:
1. get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, keeping temperature is 35～45 ℃, leaves standstill and handles 2～4 hours;
2. the water that adds 1.2～4.2 parts again floods down at 70 ℃ then and extracted 20～30 minutes;
3. after extracting end, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, and solid portion is pulled an oar, is copied sheet, concentrate is returned be coated onto on the sheet base, and oven dry is cut in flakes, promptly obtains required reconstituted tobacco finished product.
Compared with prior art, the present invention has the following advantages:
1, the extraction process section of producing at reconstituted tobacco, the utilization biological enzyme formulation is handled offal, decompose by part compositions such as the cellulose in the offal, pectin and protein, make the offal short texture, be beneficial to and carry out fiber and discongest, reduce beating energy consumption, at the drainability of the online section of manufacturing paper with pulp, make the sheet base more soft, loose when the raising sheet is base molded.
2, make the extraction of active ingredient of DDGS more complete, the loss of aroma component when reducing online and manufacturing paper with pulp.Enzyme is handled and is impelled offal to decompose latent fragrant composition such as the tobacco that produces reduced sugar, amino acid simultaneously, has increased the fragrant component content of diving in the extract, and fragrance component composition mode obtains certain adjustment in the extract thereby make, and has promoted the suction quality of reconstituted tobacco product.
3, production process can not brought negative effect to tobacco itself and white-water system, make that sewage disposal is easier to be carried out, the processing environment gentleness does not cause any damage to equipment, do not need additionally to increase equipment on the production line yet, can satisfy the technological requirement of green, environmental protection fully.
The specific embodiment
By specific embodiment given below, can further be well understood to the present invention, but they not limitation of the invention
Embodiment 1
Take by weighing 1 part of acid protease, 1.5 parts of compound pectinases, 0.1 part of 0.5 part of compound neutral cellulase and neutral lipase.Place 90 parts water to mix raw material and stirred 13 minutes, and filtered, get clear liquid and promptly obtain additives for modifying reproduced tobacco leaves of the present invention.The water of 0.1 part of property-modifying additive and 1.8 parts is mixed, add 1 part of tobacco stalk raw material then, keeping temperature is 35 ℃, leaves standstill and handles 2 hours; The water that adds 1.2 parts again floods down at 70 ℃ then and extracted 20 minutes; After extracting end, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, and solid portion is pulled an oar, is copied sheet, concentrate is returned be coated onto on the sheet base, and oven dry is cut in flakes, promptly obtains required reconstituted tobacco finished product.
Embodiment 2
Repeat embodiment 1, following difference is arranged: take by weighing 2 parts of acid proteases, 2 parts of compound pectinases, 0.75 part of compound neutral cellulase, 0.5 part of neutral lipase.Place 95 parts water to mix raw material and stirred 15 minutes, and filtered, get clear liquid and promptly obtain additives for modifying reproduced tobacco leaves of the present invention.
Embodiment 3
Repeat embodiment 1, following difference is arranged: take by weighing 3 parts of acid proteases, 3 parts of compound pectinases, 1 part of compound neutral cellulase, 1 part of neutral lipase.Place 100 parts water to mix raw material and stirred 17 minutes, and filtered, get clear liquid and promptly obtain additives for modifying reproduced tobacco leaves of the present invention.
Embodiment 4
Repeat embodiment 1, following difference is arranged: keeping temperature is 40 ℃, leaves standstill and handles 3 hours, adds 2.2 parts water again, floods down at 70 ℃ then and extracts 25 minutes;
Embodiment 5
Repeat embodiment 1, following difference is arranged: keeping temperature is 45 ℃, leaves standstill and handles 4 hours, adds 3.2 parts water again, floods down at 70 ℃ then and extracts 30 minutes.
Embodiment 6
Repeat embodiment 1, following difference is arranged: keeping temperature is 45 ℃, leaves standstill and handles 4 hours, adds 4.2 parts water again, floods down at 70 ℃ then and extracts 30 minutes.
Embodiment 7
Repeat embodiment 1, following difference is arranged: wherein the enzyme activity of acid protease is 90,000 u/g, and the enzyme activity of compound pectinase is 2,500,000 u/g, and the enzyme activity of compound neutral cellulase is 90,000 u/g, and the enzyme activity of neutral lipase is 3500u/g.
Embodiment 8
Repeat embodiment 1, following difference is arranged: wherein the enzyme activity of acid protease is 100,000 u/g, and the enzyme activity of compound pectinase is 2,800,000 u/g, and the enzyme activity of compound neutral cellulase is 100,000 u/g, and the enzyme activity of neutral lipase is 4000u/g.
Embodiment 9
Repeat embodiment 1, following difference is arranged: wherein the enzyme activity of acid protease is 110,000 u/g, and the enzyme activity of compound pectinase is 3,000,000 u/g, and the enzyme activity of compound neutral cellulase is 110,000 u/g, and the enzyme activity of neutral lipase is 4500u/g.
Application Example 1
With additive treating of the present invention Qujing offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 35 ℃ of insulation degradeds 2 hours down, the water that adds 3.2 parts again floods down at 70 ℃ then and extracted 20 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS01 (1).Beat cigarette, smoke panel test.
Application Example 2
With additive treating of the present invention Qujing offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 40 ℃ of insulation degradeds 2 hours down, the water that adds 3.2 parts again floods down at 70 ℃ then and extracted 30 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS01 (2).Beat cigarette, smoke panel test.
Application Example 3
With additive treating of the present invention Yuxi offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 40 ℃ of insulation degradeds 3 hours down, the water that adds 4.2 parts again floods down at 70 ℃ then and extracted 30 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS02 (1).Beat cigarette, smoke panel test.
Application Example 4
With additive treating of the present invention Yuxi offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 45 ℃ of insulation degradeds 3 hours down, the water that adds 4.2 parts again floods down at 70 ℃ then and extracted 30 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS02 (2).Beat cigarette, smoke panel test.
Application Example 5
With additive treating of the present invention Red River offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 40 ℃ of insulation degradeds 4 hours down, the water that adds 3.2 parts again floods down at 70 ℃ then and extracted 20 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS03 (1).Beat cigarette, smoke panel test.
Application Example 6
With additive treating of the present invention Red River offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 45 ℃ of insulation degradeds 4 hours down, the water that adds 3.2 parts again floods down at 70 ℃ then and extracted 20 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after RS03 (2).Beat cigarette, smoke panel test.
Application Example 7
With additive treating of the present invention Shandong offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 35 ℃ of insulation degradeds 3 hours down, the water that adds 4.2 parts again floods down at 70 ℃ then and extracted 30 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after Shandong test 1.Beat cigarette, smoke panel test.
Application Example 8
With additive treating of the present invention Shandong offal: get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, 45 ℃ of insulation degradeds 3 hours down, the water that adds 3.2 parts again floods down at 70 ℃ then and extracted 30 minutes; After extraction finishes, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, analyzes, and solid portion is pulled an oar, is copied sheet, analysis, concentrate is returned be coated onto on the sheet base, dries, and cuts in flakes, promptly obtains required reconstituted tobacco finished product, called after Shandong test 2.Beat cigarette, smoke panel test.
The assay of Application Example 1～8 test specimen sheet base, stalk cream and finished product sees Table 1, table 2, table 3.
This technological parameter of table 1 is to the influence of sheet base physical index
| The sample name | Beat oar degree (° SR) | Tension stress (N) | Breaking length (mm) | Air permeability (mL/m 2·Pa·S) |
| Contrast RS01 | 25.0 | 8.0 | 1.0 | 0.174 |
| Test RS01 (1) | 24.5 | 7.5 | 0.9 | 0.220 |
| Test RS01 (2) | 24.7 | 8.0 | 1.0 | 0.217 |
| Contrast RS02 | 25.2 | 8.0 | 1.1 | 0.190 |
| Test RS02 (1) | 25.0 | 7.6 | 1.0 | 0.226 |
| Test RS02 (2) | 25.3 | 8.4 | 1.9 | 0.96 |
| Contrast RS03 | 21.0 | 7.6 | 0.9 | 0.230 |
| Test RS03 (1) | 22.0 | 7.2 | 0.9 | 0.250 |
| Test RS03 (2) | 21.0 | 7.6 | 1.0 | 0.24 |
| The Shandong contrast | 24.5 | 7.7 | 0.9 | 0.182 |
| Shandong test 1 | 26.3 | 8.3 | 1.0 | 0.186 |
| Shandong test 2 | 26.5 | 8.5 | 1.1 | 0.183 |
Table 1 data show: the sample of handling through this technological parameter, and the physical index of sheet base is not only had negative interaction, and slightly raising aspect air permeability, the tension stress, make the sheet base more soft loose.
Table 2 is handled the aroma component analysis of sample and control sample DDGS
| Sequence number | Retention time | Aroma component compound title | Contrast Qujing stalk cream | Test Qujing stalk cream |
| 1 | 2.43 | 3-hydroxyl-2-butanone | 0.963 | 0.985 |
| 2 | 2.79 | Pyridine | 1.317 | 5.344 |
| 3 | 3.48 | Bread ketone | 0.674 | 2.171 |
| 4 | 3.72 | Methylpyrazine | 0.197 | 0.752 |
| 5 | 3.85 | Furfural | 5.169 | 7.786 |
| 6 | 4.15 | Furfuryl alcohol | 1.782 | 11.176 |
| 7 | 4.65 | 2-cyclopentene-1, the 4-diketone | 1.117 | 3.112 |
| 8 | 5.01 | 3-(methyl mercapto)-propionic aldehyde | 0.094 | 0.310 |
| 9 | 5.11 | 1-(2-furyl)-ethyl ketone | 0.448 | 1.284 |
| 10 | 5.15 | Butyrolactone | 1.495 | 4.281 |
| 11 | 5.78 | The 2-pyridine carboxaldehyde | 0.215 | 0.241 |
| 12 | 5.84 | Furancarboxylic acid | 0.542 | 1.214 |
| 13 | 5.99 | Benzaldehyde | 0.293 | 0.283 |
| 14 | 6.04 | 5 methyl furfural | 0.632 | 3.332 |
| 15 | 6.18 | 2-methyl trisulfide thing | - | 0.263 |
| 16 | 6.30 | Phenol | - | 0.733 |
| 17 | 6.81 | The 1H-pyrrole-2-aldehyde | - | 0.545 |
| 18 | 7.18 | 2-hydroxy-3-methyl-2-cyclopentene-1-ketone | 0.097 | 0.631 |
| 19 | 7.33 | Phenmethylol | 0.438 | 8.613 |
| 20 | 7.53 | Phenylacetaldehyde | 4.229 | 10.973 |
| 21 | 7.81 | 1-(1H-pyrroles-2-yl)-ethyl ketone | 2.271 | 2.814 |
| 22 | 8.83 | Benzyl carbinol | 0.230 | 6.627 |
| 23 | 9.36 | The polyhydroxy pyrans | - | 6.557 |
| 25 | 12.11 | Indoles | 0.202 | 0.326 |
| 26 | 12.46 | 2-methoxyl group-4-vinylphenol | 1.063 | 3.580 |
| 27 | 13.29 | Solanone | 9.498 | 7.155 |
| 28 | 13.64 | The BETA-damascenone | 1.419 | 0.978 |
| 29 | 14.28 | The dehydrogenation nornicotine | 0.279 | 0.210 |
| 30 | 16.12 | 2,3 '-bipyridyl | 0.412 | 1.141 |
| 31 | 16.18 | Dihydroactinidiolide | 0.404 | 0.520 |
| 32 | 17.11 | Megastigmatrienone B | 0.159 | 0.650 |
| 33 | 18.06 | Megastigmatrienone D | 0.139 | 0.680 |
| 34 | 18.39 | 3-oxo-ALPHA-ionol | - | 0.696 |
| 35 | 21.61 | Neophytadiene | - | 13.531 |
| 36 | 21.89 | Pentadecanoic acid | - | 1.409 |
| 37 | 22.86 | Methyl palmitate | - | 3.401 |
| 38 | 23.43 | Hexadecylic acid | 0.511 | 121.856 |
Table 2 has been enumerated the fragrance component variation of Qujing stalk cream contrast with the test specimen DDGS, the result shows, handle the stalk cream that makes by process of the present invention and parameter, the content comparison of main aroma component such as hexadecylic acid, neophytadiene, Megastigmatrienone D, solanone, bread ketone, furfural product in the same old way increases, and this processing mode has contribution to improving the coating fluid total quality.
Table 3 property-modifying additive is to the influence of papermaking-method reconstituted tobaccos integral suction quality
| The sample name | Fragrance matter | Perfume quantity | Concentration | Excitant | Assorted gas | Pleasant impression | Strength | Flammability | Grey | Total points |
| 9 | 9 | 9 | 9 | 9 | 9 | 9 | 9 | 9 | 81 | |
| Contrast RS01 | 6 | 7 | 6 | 6 | 5 | 4 | 5 | 3 | 3 | 45 |
| Test RS01 (1) | 7 | 7 | 7 | 6 | 5 | 5 | 5 | 3 | 3 | 48 |
| Test RS01 (2) | 7 | 7 | 6 | 7 | 6 | 6 | 5 | 3 | 3 | 49 |
| Contrast RS02 | 8 | 8 | 8 | 7 | 5 | 6 | 6 | 3 | 3 | 54 |
| Test RS02 (1) | 8 | 8 | 9 | 7 | 5 | 6 | 6 | 3 | 3 | 55 |
| Contrast RS03 | 5 | 6 | 5 | 6 | 5 | 4 | 5 | 3 | 3 | 42 |
| Test RS03 (1) | 6 | 6 | 6 | 6 | 6 | 5 | 5 | 3 | 3 | 46 |
| Test RS03 (2) | 6 | 6 | 6 | 5 | 6 | 5 | 3 | 3 | 3 | 43 |
Table 3 is the result show, the integral suction quality of the treated reconstituted tobacco sample that is untreated has in various degree raising, especially improves obviously in fragrance matter, fragrance concentration and pleasant impression three broad aspect.
Claims (7)
1, a kind of additives for modifying reproduced tobacco leaves is made up of the raw material of following weight parts: 1～3 part of acid protease, 1.5～3 parts of compound pectinases, 0.1～1 part of 0.5～1 part of compound neutral cellulase and neutral lipase.
2, additives for modifying reproduced tobacco leaves according to claim 1 is characterized in that: the enzyme activity of acid protease is preferably 9～110,000 u/g.
3, additives for modifying reproduced tobacco leaves according to claim 1 is characterized in that: preferred 250～3,000,000 u/g of the enzyme activity of compound pectinase.
4, additives for modifying reproduced tobacco leaves according to claim 1 is characterized in that: the enzyme activity of compound neutral cellulase is preferably 9～110,000 u/g.
5, additives for modifying reproduced tobacco leaves according to claim 1 is characterized in that: the enzyme activity of neutral lipase is preferably 3500～4500u/g.
6, the preparation method of the described additives for modifying reproduced tobacco leaves of claim 1 is characterized in that: take by weighing each raw material by described weight portion, place 90～100 parts water to mix raw material and stirred 13～17 minutes, and filtered, get clear liquid and be required property-modifying additive.
7, the using method of the described additives for modifying reproduced tobacco leaves of claim 1, this method may further comprise the steps:
1. get 0.1 part of additives for modifying reproduced tobacco leaves of the present invention, add 1.8 parts water and mix, add 1 part of tobacco stalk raw material again, keeping temperature is 35～45 ℃, leaves standstill and handles 2～4 hours;
2. the water that adds 1.2～4.2 parts again floods down at 70 ℃ then and extracted 20～30 minutes;
3. after extracting end, Separation of Solid and Liquid, liquid partly carries out vacuum and concentrates, and solid portion is pulled an oar, is copied sheet, concentrate is returned be coated onto on the sheet base, and oven dry is cut in flakes, promptly obtains required reconstituted tobacco finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100487380A CN100534337C (en) | 2006-10-23 | 2006-10-23 | Additives for modifying reproduced tobacco leaves, preparation method and use method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100487380A CN100534337C (en) | 2006-10-23 | 2006-10-23 | Additives for modifying reproduced tobacco leaves, preparation method and use method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1947606A true CN1947606A (en) | 2007-04-18 |
| CN100534337C CN100534337C (en) | 2009-09-02 |
Family
ID=38017313
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100487380A Active CN100534337C (en) | 2006-10-23 | 2006-10-23 | Additives for modifying reproduced tobacco leaves, preparation method and use method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100534337C (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018278A (en) * | 2010-11-24 | 2011-04-20 | 华宝食用香精香料（上海）有限公司 | Method of reducing protein content in cut tobacco by enzymatic treatment |
| CN102860581A (en) * | 2012-09-07 | 2013-01-09 | 苏州昆蓝生物科技有限公司 | Method for processing tobacco stems by combining nano materials with a bio-enzyme technology |
| CN103315377A (en) * | 2013-06-25 | 2013-09-25 | 浙江中烟工业有限责任公司 | Method of preparing extracting solution of papermaking reconstituted tobacco |
| CN103494326A (en) * | 2013-10-21 | 2014-01-08 | 李祥麟 | Biological enzyme mixture impurity-removing and tobacco-alcoholization method |
| CN104041933A (en) * | 2014-06-05 | 2014-09-17 | 川渝中烟工业有限责任公司 | Method for processing reconstituted tobaccos through homogeneous and isogenous paper-making process |
| CN104489909A (en) * | 2014-11-20 | 2015-04-08 | 湖北中烟工业有限责任公司 | Method for improving tobacco stem extraction ratio |
| CN105029669A (en) * | 2015-08-11 | 2015-11-11 | 广西中烟工业有限责任公司 | Additive capable of improving substrate quantification of reconstituted tobacco leaves and preparation method and application thereof |
| CN111264901A (en) * | 2020-02-10 | 2020-06-12 | 天津科技大学 | Novel method for mixing and pulping raw materials in production process of tobacco sheets by papermaking method |
| CN111345495A (en) * | 2020-03-10 | 2020-06-30 | 普维思信(深圳)科技有限公司 | Method for producing high-strength homogenized tobacco material by thick pulp papermaking method |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1135940C (en) * | 2002-03-29 | 2004-01-28 | 云南瑞升科技有限公司 | Tobacco-swelling biological additive and its prepn. and application |
| CN1248604C (en) * | 2004-06-25 | 2006-04-05 | 云南瑞升科技有限公司 | Immobilized biological additive and its preparation method and uses |
-
2006
- 2006-10-23 CN CNB2006100487380A patent/CN100534337C/en active Active
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018278B (en) * | 2010-11-24 | 2013-04-03 | 华宝食用香精香料（上海）有限公司 | Method of reducing protein content in cut tobacco by enzymatic treatment |
| CN102018278A (en) * | 2010-11-24 | 2011-04-20 | 华宝食用香精香料（上海）有限公司 | Method of reducing protein content in cut tobacco by enzymatic treatment |
| CN102860581B (en) * | 2012-09-07 | 2014-07-30 | 苏州昆蓝生物科技有限公司 | Method for processing tobacco stems by combining nano materials with a bio-enzyme technology |
| CN102860581A (en) * | 2012-09-07 | 2013-01-09 | 苏州昆蓝生物科技有限公司 | Method for processing tobacco stems by combining nano materials with a bio-enzyme technology |
| CN103315377B (en) * | 2013-06-25 | 2016-01-20 | 浙江中烟工业有限责任公司 | A kind of preparation method of papermaking-method reconstituted tobaccos extract |
| CN103315377A (en) * | 2013-06-25 | 2013-09-25 | 浙江中烟工业有限责任公司 | Method of preparing extracting solution of papermaking reconstituted tobacco |
| CN103494326A (en) * | 2013-10-21 | 2014-01-08 | 李祥麟 | Biological enzyme mixture impurity-removing and tobacco-alcoholization method |
| CN104041933A (en) * | 2014-06-05 | 2014-09-17 | 川渝中烟工业有限责任公司 | Method for processing reconstituted tobaccos through homogeneous and isogenous paper-making process |
| CN104489909A (en) * | 2014-11-20 | 2015-04-08 | 湖北中烟工业有限责任公司 | Method for improving tobacco stem extraction ratio |
| CN104489909B (en) * | 2014-11-20 | 2016-02-03 | 湖北中烟工业有限责任公司 | Improve the method for offal recovery rate |
| CN105029669A (en) * | 2015-08-11 | 2015-11-11 | 广西中烟工业有限责任公司 | Additive capable of improving substrate quantification of reconstituted tobacco leaves and preparation method and application thereof |
| CN111264901A (en) * | 2020-02-10 | 2020-06-12 | 天津科技大学 | Novel method for mixing and pulping raw materials in production process of tobacco sheets by papermaking method |
| CN111345495A (en) * | 2020-03-10 | 2020-06-30 | 普维思信(深圳)科技有限公司 | Method for producing high-strength homogenized tobacco material by thick pulp papermaking method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100534337C (en) | 2009-09-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1947606A (en) | Additives for modifying reproduced tobacco leaves, prepn. method and use thereof | |
| CN102119784B (en) | Spice extractum prepared by waste tobacco leaf, preparation method thereof and application thereof | |
| Xu et al. | Influence of fungal fermentation on the development of volatile compounds in the Puer tea manufacturing process | |
| CN102217780B (en) | Concrete flavouring for tobacco and preparation method and application thereof | |
| CN102524942B (en) | Method for reducing content of lignin in peduncle shred of tobacco | |
| CN1759768A (en) | Method for preparing reconstituted tobacco leaves through paper making method | |
| CN102250812A (en) | Bacillus subtilis preparation for tobacco stem treatment | |
| CN103251125A (en) | Method of manufacturing reconstituted tobacco through high-quality functional paper-making process | |
| Sharma et al. | Biodegradation of paddy straw obtained from different geographic locations by means of Phlebia spp. for animal feed | |
| Doria et al. | Evaluation of lignocellulolytic activities of ten fungal species able to degrade poplar wood | |
| CN104957758A (en) | Method for improving sensory quality of tobacco reconstituted through papermaking method | |
| CN105286078A (en) | Method for papermaking method reconstituted tobacco by replacing wood pulp fibers through cotton stalk bark fibers | |
| CN1600183A (en) | Technique for preparing tobacco sheet through paper making method | |
| CN107418736A (en) | A kind of preparation method of tobacco aromaticss | |
| CN107467707B (en) | Method for improving quality of tobacco sheets by papermaking method by adopting aromatized composite microbial preparation | |
| CN105199847A (en) | Preparing method and application of tobacco favor enhancer | |
| CN101427846A (en) | Method for improving efficiency of slice raw material abstraction and quality of slice flue gas with complex enzyme | |
| CN115644494B (en) | Preparation method and application of mixed tobacco recombinant essence | |
| CN102726823B (en) | A kind of method reducing tobacco sheets by paper making method extract pectic substance content | |
| CN113403878B (en) | Preparation method of tobacco fragrant cigarette paper with moisture retention function | |
| CN1135940C (en) | Tobacco-swelling biological additive and its prepn. and application | |
| CN103251126A (en) | Method for preparing microorganism derived spice component for improving cigarette quality | |
| CN1948453A (en) | Method of screening laccase endogenic bateria from Chinese sumac and preparing laccase through solid state fermentation | |
| CN106473229B (en) | Method for manufacturing filter stick additive by using fermented tobacco leaf residues and application of filter stick additive | |
| CN106834131B (en) | Fungus for degrading pectin and xylan in tobacco stems and application of fungus |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |