CN107418736A - A kind of preparation method of tobacco aromaticss - Google Patents
A kind of preparation method of tobacco aromaticss Download PDFInfo
- Publication number
- CN107418736A CN107418736A CN201710472187.9A CN201710472187A CN107418736A CN 107418736 A CN107418736 A CN 107418736A CN 201710472187 A CN201710472187 A CN 201710472187A CN 107418736 A CN107418736 A CN 107418736A
- Authority
- CN
- China
- Prior art keywords
- blueberry
- cigarette
- preparation
- tobacco aromaticss
- glucosidase
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses a kind of preparation method of tobacco aromaticss, comprise the following steps：（1）Fresh blueberry is taken, is squeezed the juice；（2）Prepare immobilization beta glucuroide；（3）Blueberry juice adds immobilization beta glucoside ferment treatment；（4）Infiltrating and vaporizing membrane is enriched with blueberry aroma substance, obtains a kind of tobacco aromaticss.Cigarette blueberry essence prepared by the present invention, there is this perfume of the blueberry of feature, there is preferable cigarette effect.Blueberry extract is added in cigarette, with increase cigarette flavor amount, improve flue gas mass, cigarette feature berry note is obvious, and reducing stimulates, and covers miscellaneous gas, soft fine and smooth flue gas, oral cavity comfort level improves, and increase cigarette returns the effect such as sweet tea sense, is better than traditional blueberry extract in increase cigarette feature note and the positive effect in terms of improving cigarette taste.
Description
Technical field
The present invention relates to technical field of tobacco, more particularly to a kind of preparation method of tobacco aromaticss.
Background technology
Essence spice for cigarette is one of most important core technology of cigarette product, is the pass that cigarette product style and features are formed
Key.Essence and flavoring agent can be played in cigarette modification or the defects of cover tobacco leaf, improve tobacco aroma and it is jealous, improve tobacco
Physical property, the harmful components for reducing cigarette, the effect of the unique taste of cigarette and style is assigned, and product product can be realized
Matter differentiation, stable cigarette smoking quality, has a major impact for the style and quality responses of cigarette.
Fruity type spices is one of conventional spices kind of cigarette, and Fruity type spices has in cigarette to be set off by contrast and highlight volume
The characteristics of cigarette fruity note, it can effectively lift cigarette quality.It is a kind of conventional using blueberry as blueberry extract prepared by raw material
Natural perfume for cigarette, in terms of lifting cigarette flavor quality have it is preferable the effect of, especially setting off by contrast and highlight cigarette slurry
There are important, but the blueberry extract blueberry of conventional method preparation this fragrance unobvious, especially in terms of fruity rhythm
In process of production aroma substance loss it is more serious, therefore, research can be enriched with blueberry fragrance preparation technology have it is important
Meaning.
The content of the invention
It is an object of the invention to provide one kind cigarette blueberry essence is prepared using enzyme immobilization technology and infiltration evaporation membrane technology
The method of oil.This method is practical, and the blueberry essence cigarette effect of preparation is good.
To reach above-mentioned purpose, the concrete technical scheme that the present invention uses is as follows：
A kind of preparation method of tobacco aromaticss, comprises the following steps：（1）Fresh blueberry is taken, cleans and squeezes the juice, collects juice；（2）System
Standby immobilized β-glucosidase：Prepare the % of 6%-10 containing mass percent polyvinyl alcohol and mass percent 1%-3% marine alga
The mixed solution of sour sodium, into mixed solution add mass fraction be 1%-2% beta-glucosidase, then with FeCl3Solution
Mixing carries out cross-linking reaction, obtains PVA.SA-Fe gel balls, dries standby；（3）Immobilization beta-glucosidase is added in blueberry juice
Ferment treatment, the g/L of immobilized β-glucosidase solid dosage 2-5；（4）Infiltrating and vaporizing membrane is enriched with blueberry aroma substance：Blueberry
Juice heats rear feeding, produces steam through infiltrating and vaporizing membrane, condensation is collected, and obtains blueberry essence.
Preferably, the FeCl3Concentration of polymer solution is 5 g/L, pH value 2.
Preferably, the mixed solution of the polyvinyl alcohol, sodium alginate and beta-glucosidase instills FeCl3Solution is carried out
Cross-linking reaction, reaction time 9-15h.
Preferably, the PVA.SA-Fe gel balls add distilled water by cross-linking reaction product through a large amount of distilled water flushings
Middle desalination 2-4 h are obtained.
Preferably, the condition of the immobilized β-glucosidase processing blueberry juice is：PH value 4-6,30-40 DEG C of temperature,
Time 10-30 h.
Preferably, the infiltrating and vaporizing membrane is PEI infiltrating and vaporizing membranes.
Preferably, 50-80 DEG C of the feeding temperature of the infiltration evaporation processing, charging rate 20-100 mL/min.
Preferably, the infiltrating and vaporizing membrane per-meate side vacuum is 20-50 Pa.
Preferably, the steam condensing mode cools down for liquid nitrogen.
Beneficial effects of the present invention：Blueberry juice is handled using immobilized β-glucosidase, discharges the fragrance in blueberry juice
Composition, and be enriched with the aroma substance in blueberry using vaporization infiltration membrane technology, prepare a kind of fragrant with blueberry feature
The blueberry essence of gas, the Aromatic Matter Contents height of the essential oil, aroma of pure, cigarette application effect are preferable.Blueberry extract is added
It is added in cigarette, there is increase cigarette flavor amount, improve flue gas mass, assign cigarette feature berry note, reducing stimulates, and covers
Miscellaneous gas, soft fine and smooth flue gas, oral cavity comfort level improve, and increase cigarette returns the effect such as sweet tea sense, lift blueberry extract of knowing clearly and are rolling up
Adaptability in cigarette.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
（1）A certain amount of fresh blueberry is taken, cleans, squeezes the juice, collects juice；
（2）The immobilization of beta-glucosidase：Prepare the marine alga of polyvinyl alcohol and mass percent 1% containing mass percent 6%
The mixed solution of sour sodium, then adds the beta-glucosidase that mass fraction is 1% into mixed solution, and matter is instilled with syringe
Amount concentration is 5 g/L, the FeCl that pH value is 23It is crosslinked 9 hours in solution, with a large amount of distilled water flushings, adds in distilled water and take off
The h of salt 2, finally gives PVA.SA-Fe gel balls, dries standby；
（3）Using step（2）The immobilized β-glucosidase processing blueberry juice of preparation, immobilized β-glucosidase solid are used
Measure 2 g/L, the pH value 4 of ferment treatment, 30 DEG C of ferment treatment temperature, enzyme processing time 10h；
（4）From PEI infiltrating and vaporizing membranes, step（3）Blueberry juice is 50 DEG C in heating-up temperature after processing, charging rate 20
ML/min, liquid nitrogen cooling, under conditions of aroma substance collects the Pa of pressure 20, infiltration processing is vaporized, and collect fragrance thing
Matter, obtain a kind of tobacco aromaticss.
Embodiment 2
（1）A certain amount of fresh blueberry is taken, cleans, squeezes the juice, collects juice；
（2）The immobilization of beta-glucosidase：Prepare the polyvinyl alcohol of the % containing mass percent 8 and the % of mass percent 2 sea
The mixed solution of mosanom, the beta-glucosidase that mass fraction is 1% is then added into mixed solution, is instilled with syringe
It is crosslinked 12 hours in the FeCl3 solution that mass concentration is 5g/L, pH value is 2, with a large amount of distilled water flushings, adds in distilled water
The h of desalination 2, finally gives PVA.SA-Fe gel balls, dries standby；
（3）Using step（2）The immobilized β-glucosidase processing blueberry juice of preparation, immobilized β-glucosidase solid are used
Measure 2 g/L, the pH value 5 of ferment treatment, 35 DEG C of ferment treatment temperature, enzyme processing time 15h；
（4）From PEI infiltrating and vaporizing membranes, step（3）Blueberry juice is 60 DEG C in heating-up temperature after processing, charging rate 40mL/
Min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 30Pa, infiltration processing is vaporized, and collects aroma substance, obtained
A kind of tobacco aromaticss.
Embodiment 3
（1）A certain amount of fresh blueberry is taken, cleans, squeezes the juice, collects juice；
（2）The immobilization of beta-glucosidase：Prepare the marine alga of polyvinyl alcohol and the % of mass percent 2 containing mass percent 8%
The mixed solution of sour sodium, the beta-glucosidase that mass fraction is 1.5% is then added into mixed solution, is instilled with syringe
It is crosslinked 12 hours in the FeCl3 solution that mass concentration is 5 g/L, pH value is 2, with a large amount of distilled water flushings, adds distilled water
The middle h of desalination 3, finally gives PVA.SA-Fe gel balls, dries standby；
（3）Using step（2）The immobilized β-glucosidase processing blueberry juice of preparation, immobilized β-glucosidase solid are used
Measure 4 g/L, the pH value 5 of ferment treatment, 35 DEG C of ferment treatment temperature, the h of enzyme processing time 20；
（4）From PEI infiltrating and vaporizing membranes, step（3）Blueberry juice is 65 DEG C in heating-up temperature after processing, and charging rate is 60 mL/
Min, liquid nitrogen cooling, under conditions of aroma substance collects the Pa of pressure 35, infiltration processing is vaporized, and collects aroma substance, obtained
A kind of tobacco aromaticss.
Embodiment 4
（1）A certain amount of fresh blueberry is taken, cleans, squeezes the juice, collects juice；
（2）The immobilization of beta-glucosidase：Prepare the polyvinyl alcohol of the % containing mass percent 10 and the % of mass percent 3 sea
The mixed solution of mosanom, the beta-glucosidase that mass fraction is 2% is then added into mixed solution, is instilled with syringe
It is crosslinked 15 hours in the FeCl3 solution that mass concentration is 5 g/L, pH value is 2, with a large amount of distilled water flushings, adds distilled water
The middle h of desalination 4, finally gives PVA.SA-Fe gel balls, dries standby；
（3）Using step（2）The immobilized β-glucosidase processing blueberry juice of preparation, immobilized β-glucosidase solid are used
Measure 5 g/L, the pH value 6 of ferment treatment, 40 DEG C of ferment treatment temperature, the h of enzyme processing time 30；
（4）From PEI infiltrating and vaporizing membranes, step（3）Blueberry juice is 80 DEG C in heating-up temperature after processing, charging rate 100
ML/min, liquid nitrogen cooling, under conditions of aroma substance collects the Pa of pressure 50, infiltration processing is vaporized, and collect fragrance thing
Matter, obtain a kind of tobacco aromaticss.
The present invention prepares tobacco aromaticss using enzyme immobilization technology and vaporization infiltration technology, with traditional blueberry extract feature
Aromatic Matter Contents are contrasted as indicated with 1, with traditional blueberry extract cigarette sensory effects to such as table 2.
The blueberry essence of table 1 and blueberry extract characteristic perfume material comparative analysis result
The blueberry essence of table 2 and traditional blueberry extract cigarette sensory effects comparing result
To sum up, the blueberry essence that prepared by the present invention is compared with conventional method prepares blueberry extract（Such as table 1）, its 3 Methylbutanoic acid
9 kinds of blueberry characteristic perfumes such as ethyl ester, 3 Methylbutanoic acid methyl esters, methyl 2-methylbutyrate, 1,2- diethyl phthalates, terpineol
The relative amount of material has increase, and characteristic perfume material total content adds 41.71%.Blueberry essence extracts with traditional blueberry
Thing cigarette sensory effects comparing result shows（Such as table 2）, this note of feature blueberry is more obvious, is added in cigarette, has
Increase cigarette flavor amount, improve flue gas mass, cigarette feature berry note is obvious, and reducing stimulates, and covers miscellaneous gas, soft fine and smooth cigarette
Gas, oral cavity comfort level improve, and increase cigarette returns the effect such as sweet tea sense, in terms of increasing cigarette feature note and improving cigarette taste
Positive effect is better than traditional blueberry extract.
The preferred embodiments of the present invention are the foregoing is only, are not limitation of the present invention, all designs in the present invention
All any modification, equivalent and improvement made in thinking etc., should be included in the scope of the protection.
Claims (9)
1. a kind of preparation method of tobacco aromaticss, it is characterised in that comprise the following steps：
（1）Fresh blueberry is taken, cleans and squeezes the juice, collects juice；
（2）Prepare immobilized β-glucosidase：Prepare the % of 6%-10 containing mass percent polyvinyl alcohol and mass percent
The mixed solution of 1%-3% sodium alginate, the beta-glucosidase that mass fraction is 1%-2% is added into mixed solution, then
With FeCl3Solution mixing carries out cross-linking reaction, obtains PVA.SA-Fe gel balls, dries standby；
（3）Immobilized β-glucosidase processing, the g/L of immobilized β-glucosidase solid dosage 2-5 are added in blueberry juice；
（4）Infiltrating and vaporizing membrane is enriched with blueberry aroma substance：Blueberry juice heats rear feeding, and steam, condensation are produced through infiltrating and vaporizing membrane
Collect, obtain blueberry essence.
2. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The FeCl3Concentration of polymer solution is
5 g/L, pH value 2.
3. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The polyvinyl alcohol, sodium alginate
FeCl is instilled with the mixed solution of beta-glucosidase3Solution carries out cross-linking reaction, reaction time 9-15h.
4. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The PVA.SA-Fe gel balls by
Cross-linking reaction product adds desalination 2-4 h in distilled water and obtained through a large amount of distilled water flushings.
5. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The immobilized β-glucosidase
Processing blueberry juice condition be：PH value 4-6,30-40 DEG C of temperature, time 10-30 h.
6. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The infiltrating and vaporizing membrane oozes for PEI
Vaporization film thoroughly.
7. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The charging of the infiltration evaporation processing
50-80 DEG C of temperature, charging rate 20-100 mL/min.
8. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The infiltrating and vaporizing membrane per-meate side is true
Reciprocal of duty cycle is 20-50 Pa.
9. the preparation method of tobacco aromaticss according to claim 1, it is characterised in that：The steam condensing mode is liquid nitrogen
Cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710472187.9A CN107418736B (en) | 2017-06-21 | 2017-06-21 | Preparation method of tobacco flavor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710472187.9A CN107418736B (en) | 2017-06-21 | 2017-06-21 | Preparation method of tobacco flavor |
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| CN107418736A true CN107418736A (en) | 2017-12-01 |
| CN107418736B CN107418736B (en) | 2020-12-04 |
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| CN201710472187.9A Active CN107418736B (en) | 2017-06-21 | 2017-06-21 | Preparation method of tobacco flavor |
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Cited By (4)
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| CN110693063A (en) * | 2019-11-13 | 2020-01-17 | 湖北中烟工业有限责任公司 | Preparation method of blueberry extract for cigarettes |
| CN113100469A (en) * | 2021-03-15 | 2021-07-13 | 云南中烟工业有限责任公司 | Method for improving aroma of cigarette products by using raspberry glycosides |
| CN113974205A (en) * | 2021-10-26 | 2022-01-28 | 河南中烟工业有限责任公司 | Blueberry essence, blueberry extract, and preparation methods and applications thereof |
| CN114689746A (en) * | 2022-03-25 | 2022-07-01 | 江苏中烟工业有限责任公司 | Method, device, electronic equipment and medium for screening tobacco extract characteristics |
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| CN107418736B (en) | 2020-12-04 |
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