CN1943547A - Chinese medicine tooth paste containing camellia flower extract - Google Patents
Chinese medicine tooth paste containing camellia flower extract Download PDFInfo
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- CN1943547A CN1943547A CN 200610122575 CN200610122575A CN1943547A CN 1943547 A CN1943547 A CN 1943547A CN 200610122575 CN200610122575 CN 200610122575 CN 200610122575 A CN200610122575 A CN 200610122575A CN 1943547 A CN1943547 A CN 1943547A
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- chinese medicinal
- toothpaste
- flos camelliae
- camelliae japonicae
- supercritical extraction
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Abstract
A Chinese medicine toothpaste containing extracts from camellia , said toothpaste comprising paste and active component of supercritical extracting from camellia , thereof said active components of extraction make up 0.5%-10% of the total amount of toothpaste, the remainder of said toothpaste is base material of paste. Because active crystal substance applying into the paste by adopting supercritical isolation technique of CO2 extraction d by said invention, leading to defects resolved from traditional extraction technique and obtaining slight white and active crystals of camellia with definite ingredient.
Description
Technical field
The present invention relates to a kind of articles for daily use, particularly relate to a kind of Chinese medicinal toothpaste that contains the Chinese herbal medicine extract composition.
Background technology
At present, Chinese medicinal toothpaste kind daily on the market is a lot, it mainly is to add corresponding Chinese medicine ingredients to form Chinese medicinal toothpaste in the lotion of toothpaste substrate of forming toothpaste, it is used for multipotency and suppresses the oral cavity noxious bacteria, anti-inflammatory analgesic, anti-this desensitization, caries prevention, the control gingivitis, periodontitis, periodontals such as dental hemorrhage.And traditional lotion of toothpaste substrate mainly includes wetting agent, binding agent, abrasive, essence and glucide and appropriate amount of deionized water, and wherein wetting agent adopts glycerol or sorbitol or propylene glycol or Polyethylene Glycol or its combination; Binding agent adopts sodium carboxymethyl cellulose or carboxyethyl cellulose or carrageenan or HANSHENGJIAO or its combination; Abrasive adopts calcium carbonate or calcium hydrogen phosphate or silicon dioxide or its combination.At this moment, the percentage ratio of described each ingredients constitute toothpaste total composition weight is: wetting agent 15%～28%, binding agent 1%～3%, foaming agent 1.5%～3.0%, abrasive 38%～50%, essence 1%～1.8%, glucide 0.1%～0.4%, surplus are deionized water.Flos Camelliae Japonicae active matter composition has excellent clearing away heat to stop bleeding function, the disease treatments such as inside and outside section of medical science have been widely used in, therefore utilize the drug effect of Flos Camelliae Japonicae active matter composition to be applied to the oral cavity health nursing field and have positive effect, carry or ethanol is carried crystallization process and the extracting method of traditional Flos Camelliae Japonicae active matter composition is a water, these two kinds of methods all need to carry out the high temperature high cooking.Not only make the extraction ratio of Flos Camelliae Japonicae active matter composition low, and the color and luster of extract is darker.Owing to the steam temperature height, extraction time is long simultaneously, some thermal sensitivity active ingredient decomposition easily, oxidation or hydrolysis in the Flos Camelliae Japonicae, and in addition, concentration process can make the extractum color burn behind the decocting in water.So the Flos Camelliae Japonicae extract effective component content that these traditional extracting method make is not high, impurity is too many, and the color is too dark, the composition complexity.Not only influence the outward appearance of product when making an addition to it in toothpaste, and the active ingredient of Flos Camelliae Japonicae can't be fully utilized also, recipe design is subjected to certain restriction.On formulation of toothpaste, select opaque resin and cover its ugly color, also will solve the addition of Flos Camelliae Japonicae extract and the problem of stability, increased toothpaste simultaneously again and produced aftertreatment technology, improved production cost, energy consumption greatly except needs.Obviously, add in the toothpaste for these Flos Camelliae Japonicae active matters that extract with traditional method for making, as desire to make the maximization useful effect of toothpaste performance medicine must strengthen addition, such toothpaste color is inevitable very dark, influences the mastic outward appearance; If want to keep the pure white preferably color of toothpaste, then the amount of medicated premix can not be too big, so often can not guarantee drug effect, so addition (drug effect) and mastic outward appearance and stability are contradiction.
Summary of the invention
The objective of the invention is existence, provide a kind of supercritical CO at the problems referred to above
2The Flos Camelliae Japonicae active matter crystalline solid that extraction and separation technology extracts is applied in the toothpaste, make the not only pure white exquisiteness of outward appearance of made toothpaste, need not to add opaque resin, and because of the Flos Camelliae Japonicae active matter crystalline solid purity height of supercritical extraction, both made Chinese medicinal toothpaste use effect can be fully guaranteed the Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract that made things convenient for recipe design again, improves the quality of products.
The objective of the invention is to be achieved through the following technical solutions:
A kind of Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract, comprise lotion of toothpaste substrate and supercritical extraction Flos Camelliae Japonicae active compound, the percentage ratio that wherein said supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and the surplus of described Chinese medicinal toothpaste is a lotion of toothpaste substrate.
Wherein above-mentioned supercritical extraction Flos Camelliae Japonicae active compound comprises supercritical extraction Flos Camelliae Japonicae active matter crystalline solid, the supercritical extraction paeonol, tranamic acid, the percentage ratio that this moment, described supercritical extraction paeonol accounted for above-mentioned Chinese medicinal toothpaste gross weight is 0%～2%, the percentage ratio that described tranamic acid accounts for above-mentioned Chinese medicinal toothpaste gross weight is 0%～1%, the percentage ratio that described supercritical extraction Flos Camelliae Japonicae active compound crystalline solid accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and described supercritical extraction paeonol, tranamic acid, the percentage ratio that supercritical extraction Flos Camelliae Japonicae active matter crystalline solid three sum accounts for the Chinese medicinal toothpaste gross weight is no more than 10%.
Above-mentioned lotion of toothpaste substrate comprises that accounting for the Chinese medicinal toothpaste total weight percent is following constituent:
Wetting agent 15%～28% binding agent 1%～3%
Foaming agent 1.5%～3.0% abrasivus 38%～50%
Essence 1.0%～1.8% glucide 0.1%～0.4%
Surplus is a deionized water.
The present invention is owing to adopt supercritical CO
2The Flos Camelliae Japonicae active matter crystalline solid that extraction and separation technology extracts is applied in the toothpaste, because supercritical CO
2Extraction and separation technology, it is low to have temperature, without solvent, can separate to greatest extent and the characteristics of the composition of remaining valid, and is described as green isolation technics.Therefore the present invention is used for supercritical carbon dioxide extraction method the extraction of Flos Camelliae Japonicae dexterously, solved the defective of traditional Flos Camelliae Japonicae extractive technique well, obtained the white and clear and definite Flos Camelliae Japonicae active matter crystalline solid of composition of lighter color, this Flos Camelliae Japonicae active matter crystalline solid purity height of while, appearance color is shallow white, so it is suitable as the medicated premix of toothpaste very much.And the made toothpaste this moment pure white exquisiteness of outward appearance not only, need not to make toner, and, the effective dose of Chinese medicinal toothpaste of the present invention was guaranteed because of Flos Camelliae Japonicae active matter crystalline solid purity height, guarantee that fully it uses effect good, has made things convenient for recipe design again and has improved the quality of products.Thereby make the present invention can obtain Flos Camelliae Japonicae active matter content height, color is pure white, the clearing away heat to stop bleeding effect is good Chinese medicine health-care toothpaste very reliably.
Describe realization of the present invention in detail below in conjunction with embodiment:
The specific embodiment
The Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract of the present invention comprises lotion of toothpaste substrate and supercritical extraction Flos Camelliae Japonicae active compound, the percentage ratio that wherein said supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and the surplus of described Chinese medicinal toothpaste is a lotion of toothpaste substrate.This moment, described lotion of toothpaste substrate adopted traditional lotion of toothpaste substrate, and it includes wetting agent, binding agent, abrasive, essence and glucide and appropriate amount of deionized water, and wherein wetting agent adopts glycerol or sorbitol or propylene glycol or Polyethylene Glycol or its combination; Binding agent adopts sodium carboxymethyl cellulose or carboxyethyl cellulose or carrageenan or HANSHENGJIAO or its combination; Abrasive adopts calcium carbonate or calcium hydrogen phosphate or silicon dioxide or its combination.At this moment, the percentage ratio of described each ingredients constitute toothpaste total composition weight is: wetting agent 15%～28%, binding agent 1%～3%, foaming agent 1.5%～3.0%, abrasive 38%～50%, essence 1%～1.8%, glucide 0.1%～0.4%, surplus are deionized water.The preferred values of the percentage ratio of each ingredients constitute toothpaste total composition weight is wetting agent 17%～25%, binding agent 1.5%～2.0%, foaming agent 1.6%～2.8%, abrasive 42%～49%, essence 1.0%～1.5%, glucide 0.1%～0.3% in the wherein above-mentioned lotion of toothpaste substrate, and surplus is a deionized water.And the optimum of the percentage ratio of each ingredients constitute toothpaste total composition weight is wetting agent 23%, binding agent 1.7%, foaming agent 2.5%, abrasive 46%, essence 1.4%, glucide 0.23% in the lotion of toothpaste substrate, and surplus is a deionized water.The percentage ratio preferred values that wherein above-mentioned supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 2.5%～5%.The percentage ratio optimum that this moment, supercritical extraction Flos Camelliae Japonicae active compound of the present invention accounted for the Chinese medicinal toothpaste gross weight is 3%.Simultaneously for to make the more remarkable treatment effect of Chinese medicinal toothpaste of the present invention lasting, Flos Camelliae Japonicae active compound in the Chinese medicinal toothpaste of the present invention both can be independent Flos Camelliae Japonicae active matter crystalline solid, also can be and paeonol with clearing away heat to stop bleeding effect, the combination of one or several in the additives such as tranamic acid and Flos Camelliae Japonicae active matter crystalline solid, thereby reach coordinating effect so that its more remarkable effect, this moment, above-mentioned supercritical extraction Flos Camelliae Japonicae active compound comprised supercritical extraction Flos Camelliae Japonicae active matter crystalline solid, the supercritical extraction paeonol, tranamic acid, the percentage ratio that wherein said supercritical extraction paeonol accounts for above-mentioned Chinese medicinal toothpaste gross weight is 0%～2%, the percentage ratio that described tranamic acid accounts for above-mentioned Chinese medicinal toothpaste gross weight is 0%～1%, described supercritical extraction Flos Camelliae Japonicae active compound crystalline solid, the percentage ratio that accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and described supercritical extraction paeonol, tranamic acid, the percentage ratio that supercritical extraction Flos Camelliae Japonicae active matter crystalline solid three sum accounts for the Chinese medicinal toothpaste gross weight is no more than 10%.
This moment interpolation Flos Camelliae Japonicae supercritical CO of the present invention
2The manufacture method of the toothpaste of extraction active matter may further comprise the steps:
(1) binding agent is joined in the wetting agent, stir and form finely dispersed suspension;
(2) glucide is joined in the deionized water, be stirred to dissolving fully;
(3) wetting agent and the described liquor saccharini of step 2 are joined the suspension described in the step 1, stir into transparent rubber cement;
(4) with oil-soluble Flos Camelliae Japonicae supercritical CO
2Extraction active matter crystalline solid is dissolved in the essence;
(5) with abrasive, foaming agent and be dissolved with the Flos Camelliae Japonicae supercritical CO
2The essence of extraction active matter crystalline solid joins in the above-mentioned rubber cement, stirs into paste, obtains lotion of toothpaste again after grinding the degassing, and through aseptic process, is packaged to be the toothpaste finished product.
This moment supercritical CO of the present invention
2The preparation method of extraction Flos Camelliae Japonicae is: the dry thing of a certain amount of Flos Camelliae Japonicae put in the extraction kettle, and to extraction kettle, first extraction-container, second extraction-container, detached dowel, crystallization kettle heats respectively or cool off, when reaching selected temperature, unlatching CO
2Bottle pressurizes to whole device by high-pressure pump, when extraction kettle, first extraction-container, second extraction-container, when detached dowel pressure reaches the pressure that sets respectively, close CO
2Bottle, the beginning cycling extraction adds a certain amount of entrainer simultaneously, and regulates CO
2Flow to a certain amount of, keep constant temperature and pressure.After reaching selected extraction time,, obtain desired supercritical extraction Flos Camelliae Japonicae active matter crystalline solid from the crystallization kettle discharge hole for discharge.
Embodiment 1:
The Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract described in this enforcement includes that to account for the Chinese medicinal toothpaste total weight percent be following constituent: glycerol 10%, and sorbitol 15%, CMC 1%, glucide 0.1%, K
121.5%, calcium carbonate 47%, supercritical extraction Flos Camelliae Japonicae active matter crystalline solid 1.5%, essence 1.0%, surplus is a deionized water.
Embodiment 2:
The Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract described in this enforcement includes that to account for the Chinese medicinal toothpaste total weight percent be following constituent: glycerol 12%, and propylene glycol 16%, sorbitol 10%, CMC 1%, HEC0.2%, glucide 0.2%, K
122.1%, calcium hydrogen phosphate 42%, super critical extraction Flos Camelliae Japonicae active matter crystalline solid 0.5%, supercritical extraction paeonol 0.1% essence 1.3%, deionized water surplus.
Embodiment 3:
The Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract described in this enforcement includes that to account for the Chinese medicinal toothpaste total weight percent be following constituent: Polyethylene Glycol 10%, sorbitol 15%, CMC1.0%, HANSHENGJIAO 0.3%, glucide 0.3%, K
122.7%, calcium hydrogen phosphate 35%, silica 1 0%, supercritical extraction Flos Camelliae Japonicae active matter crystalline solid 3.0% tranamic acid 0.5% essence 1.5%, surplus is a deionized water.
Embodiment 4:
The Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract described in this enforcement includes that to account for the Chinese medicinal toothpaste total weight percent be following constituent: Polyethylene Glycol 5%, propylene glycol 10%, sorbitol 13%, CMC1.2%, carrageenan 0.4%, glucide 0.4%, K
123%, calcium carbonate 25%, silica 1 5%, supercritical extraction Flos Camelliae Japonicae active matter crystalline solid 5%, supercritical extraction paeonol 0.8% tranamic acid 0.5%, essence 1.8%, surplus is a deionized water.
Claims (5)
1, a kind of Chinese medicinal toothpaste that contains the Flos Camelliae Japonicae extract, it is characterized in that described Chinese medicinal toothpaste comprises lotion of toothpaste substrate and supercritical extraction Flos Camelliae Japonicae active compound, the percentage ratio that wherein said supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and the surplus of described Chinese medicinal toothpaste is a lotion of toothpaste substrate.
2, Chinese medicinal toothpaste according to claim 1 is characterized in that the percentage ratio that above-mentioned supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 2.5%～5%.
3, Chinese medicinal toothpaste according to claim 2 is characterized in that the percentage ratio that above-mentioned supercritical extraction Flos Camelliae Japonicae active compound accounts for the Chinese medicinal toothpaste gross weight is 3%.
4, according to claim 1 or 2 or 3 described Chinese medicinal toothpastes, it is characterized in that above-mentioned supercritical extraction Flos Camelliae Japonicae active compound comprises supercritical extraction Flos Camelliae Japonicae active matter crystalline solid, the supercritical extraction paeonol, tranamic acid, the percentage ratio that wherein said supercritical extraction paeonol accounts for above-mentioned Chinese medicinal toothpaste gross weight is 0%～2%, the percentage ratio that described tranamic acid accounts for above-mentioned Chinese medicinal toothpaste gross weight is 0%～1%, the percentage ratio that described supercritical extraction Flos Camelliae Japonicae active compound crystalline solid accounts for the Chinese medicinal toothpaste gross weight is 0.5%～10%, and described supercritical extraction paeonol, tranamic acid, the percentage ratio that supercritical extraction Flos Camelliae Japonicae active matter crystalline solid three sum accounts for the Chinese medicinal toothpaste gross weight is no more than 10%.
5,, it is characterized in that above-mentioned lotion of toothpaste substrate comprises that accounting for the Chinese medicinal toothpaste total weight percent is following constituent according to claim 1 or 2 or 3 described Chinese medicinal toothpastes:
Wetting agent 15%～28% binding agent 1%～3%
Foaming agent 1.5%～3.0% abrasivus 38%～50%
Essence 1.0%～1.8% glucide 0.1%～0.4%
Surplus is a deionized water
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610122575 CN1943547A (en) | 2006-09-30 | 2006-09-30 | Chinese medicine tooth paste containing camellia flower extract |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200610122575 CN1943547A (en) | 2006-09-30 | 2006-09-30 | Chinese medicine tooth paste containing camellia flower extract |
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| CN1943547A true CN1943547A (en) | 2007-04-11 |
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| CN 200610122575 Pending CN1943547A (en) | 2006-09-30 | 2006-09-30 | Chinese medicine tooth paste containing camellia flower extract |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184515A (en) * | 2017-05-24 | 2017-09-22 | 缪来耿 | A kind of whitening toothpaste and preparation method thereof |
| CN108969413A (en) * | 2017-06-05 | 2018-12-11 | 狮王株式会社 | Composition for oral cavity |
| CN113662898A (en) * | 2021-10-09 | 2021-11-19 | 浙江山茶之都农业开发股份有限公司 | Technology of camellia Chinese herbal medicine toothpaste for preventing and treating oral diseases |
-
2006
- 2006-09-30 CN CN 200610122575 patent/CN1943547A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184515A (en) * | 2017-05-24 | 2017-09-22 | 缪来耿 | A kind of whitening toothpaste and preparation method thereof |
| CN108969413A (en) * | 2017-06-05 | 2018-12-11 | 狮王株式会社 | Composition for oral cavity |
| CN113662898A (en) * | 2021-10-09 | 2021-11-19 | 浙江山茶之都农业开发股份有限公司 | Technology of camellia Chinese herbal medicine toothpaste for preventing and treating oral diseases |
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