CN1923066A - Composite additive for raising cigarette smoke moisture and its use - Google Patents
Composite additive for raising cigarette smoke moisture and its use Download PDFInfo
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- CN1923066A CN1923066A CN 200610048649 CN200610048649A CN1923066A CN 1923066 A CN1923066 A CN 1923066A CN 200610048649 CN200610048649 CN 200610048649 CN 200610048649 A CN200610048649 A CN 200610048649A CN 1923066 A CN1923066 A CN 1923066A
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- compound additive
- cigarette
- cigarette smoke
- moisture
- tobacco
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 108
- 239000000654 additive Substances 0.000 title claims abstract description 66
- 230000000996 additive effect Effects 0.000 title claims abstract description 64
- 239000000779 smoke Substances 0.000 title claims abstract description 27
- 239000002131 composite material Substances 0.000 title claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- 150000007524 organic acids Chemical class 0.000 claims abstract description 9
- 229920000642 polymer Polymers 0.000 claims abstract description 8
- 150000004040 pyrrolidinones Chemical class 0.000 claims abstract description 8
- 241000208125 Nicotiana Species 0.000 claims description 74
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 74
- 150000001875 compounds Chemical class 0.000 claims description 59
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 44
- 239000003546 flue gas Substances 0.000 claims description 44
- 239000000796 flavoring agent Substances 0.000 claims description 21
- 235000013355 food flavoring agent Nutrition 0.000 claims description 15
- XIRNKXNNONJFQO-UHFFFAOYSA-N ethyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC XIRNKXNNONJFQO-UHFFFAOYSA-N 0.000 claims description 12
- 150000002576 ketones Chemical class 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- BQENDLAVTKRQMS-SBBGFIFASA-L Carbenoxolone sodium Chemical compound [Na+].[Na+].C([C@H]1C2=CC(=O)[C@H]34)[C@@](C)(C([O-])=O)CC[C@]1(C)CC[C@@]2(C)[C@]4(C)CC[C@@H]1[C@]3(C)CC[C@H](OC(=O)CCC([O-])=O)C1(C)C BQENDLAVTKRQMS-SBBGFIFASA-L 0.000 claims description 7
- 229960002252 carbenoxolone sodium Drugs 0.000 claims description 7
- 239000007859 condensation product Substances 0.000 claims description 7
- 235000011449 Rosa Nutrition 0.000 claims description 6
- 229940067592 ethyl palmitate Drugs 0.000 claims description 6
- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims description 5
- 229940101029 dipotassium glycyrrhizinate Drugs 0.000 claims description 5
- 235000019505 tobacco product Nutrition 0.000 claims description 5
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 4
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 4
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 4
- 239000001540 sodium lactate Substances 0.000 claims description 4
- 229940005581 sodium lactate Drugs 0.000 claims description 4
- 235000011088 sodium lactate Nutrition 0.000 claims description 4
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- 235000007688 Lycopersicon esculentum Nutrition 0.000 claims description 2
- 240000003768 Solanum lycopersicum Species 0.000 claims description 2
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims description 2
- 229940075495 isopropyl palmitate Drugs 0.000 claims description 2
- 239000004310 lactic acid Substances 0.000 claims description 2
- 235000014655 lactic acid Nutrition 0.000 claims description 2
- 229960000448 lactic acid Drugs 0.000 claims description 2
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 2
- QGKLPGKXAVVPOJ-UHFFFAOYSA-N pyrrolidin-3-one Chemical class O=C1CCNC1 QGKLPGKXAVVPOJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000000470 constituent Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 21
- 238000013019 agitation Methods 0.000 description 16
- 230000008569 process Effects 0.000 description 12
- 238000005516 engineering process Methods 0.000 description 11
- 230000000391 smoking effect Effects 0.000 description 11
- 238000002156 mixing Methods 0.000 description 10
- 239000003205 fragrance Substances 0.000 description 9
- 239000011285 coke tar Substances 0.000 description 8
- 239000004615 ingredient Substances 0.000 description 8
- 238000005303 weighing Methods 0.000 description 7
- 235000019634 flavors Nutrition 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 230000009467 reduction Effects 0.000 description 5
- 239000000523 sample Substances 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 239000013068 control sample Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000011269 tar Substances 0.000 description 4
- 239000011218 binary composite Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 238000009738 saturating Methods 0.000 description 3
- 210000000697 sensory organ Anatomy 0.000 description 3
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 2
- 229920006221 acetate fiber Polymers 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 238000004868 gas analysis Methods 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229960002715 nicotine Drugs 0.000 description 2
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 2
- 238000003359 percent control normalization Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to a composite additive for increasing water content in cigarette smoke and uses thereof, wherein the composite additive comprises the constituents of organic acid and derivative 0-60%, condensate or polymer of ethylene alcohol 10-90%, pyrrolidone compounds 0-30%, gourmet powder 0.1-5%, and deionized water 0-40%.
Description
Technical field
The present invention relates to a kind of compound additive and application thereof that improves cigarette smoke moisture.
Background technology
Along with the pay attention to day by day of society to smoking and health problem, the harmful components that reduce in the cigarette smoke become one of focus of people's concern.At present, the harmful components that reduce in the cigarette smoke generally are to realize by the releasing content of coke tar that reduces cigarette.But cigarette is a kind of special consumer goods, is to enjoy its flue gas by burning and sucking, and along with the reduction of tar content in cigarette, must cause a large amount of losses of fragrance, has a strong impact on the style and the sucking quality of cigarette.Particularly for low-coke tar cigarette, fragrance is thin, and flue gas is dry, stimulates to increase, and problems such as throat's comfortableness reduction have restricted the development of low-coke tar cigarette.Therefore, how to keep the comfortableness of fragrance, reduction stimulation and the raising throat of cigarette to become the tobacco business problem demanding prompt solution.
Cause flue gas dry, stimulate to increase, the reason of problems such as throat's comfortableness reduction is very complicated, and result of study shows that main flume moisture is an important factors that influence these problems, its content how much will directly influence the aesthetic quality of cigarette.Low-coke tar cigarette is owing to use filter tip ventilation dilution technology in a large number, and main flume moisture is generally on the low side, causes flue gas dry, stimulates to increase, and comfortableness reduces.
In view of the importance of flue gas moisture,, become the important topic of domestic and international research to how to regulate and improve cigarette mainstream flue gas moisture.Many in recent years scientific workers to how manage, keep by production technology and outer doping and improve the moisture that cigarette props up, and moisture is studied inhaling the aspects such as influence of distinguishing the flavor of.Xiao Wen equality people studies with the relation of inhaling flavor cigarette Zhi Shuifen, and the variation of having inquired into moisture in cut tobacco is to inhaling the Changing Pattern that influences of flavor.The cigarette smoking result as can be seen, moisture in cut tobacco is influential to inhaling flavor.This influence is irregular normal distribution, along with the rising of cigarette quality, and the trend that the oriented little moisture direction of normal distribution moves.Cigarette Zhi Shuifen changes not obvious to the influence of flue gas moisture.Chinese patent 98113287.1 discloses a kind of novel humectant, effectively keeps the moisture of pipe tobacco.But these research work only limit to the moisture in the pipe tobacco, and yet there are no report for the research, particularly flue gas moisture of cigarette smoke moisture aspect and cigarette aesthetic quality's relation and technical method how to regulate and control to improve flue gas moisture.
Along with the development of low-coke tar cigarette and the increase of the market share, develop a kind of material and the technology that can effectively regulate and improve cigarette mainstream flue gas moisture, increase the flue gas wettability, reducing stimulates, and improves throat's comfortableness, seems very urgent and necessary.
Summary of the invention
The purpose of this invention is to provide a kind of compound additive and application thereof that improves cigarette smoke moisture.This cigarette compound additive by effective adjusting and raising cigarette mainstream flue gas moisture, keeps the style of cigarette constant, increases the flue gas wettability, and reducing stimulates, and improves throat's comfortableness.
The object of the present invention is achieved like this:
A kind of compound additive that improves cigarette smoke moisture mainly is grouped into by following one-tenth: organic acid and derivative thereof (1), the condensation product of ethylene glycol or polymer (2), pyrrolidones (3), essence and flavoring agent (4), deionized water (5).Wherein the percentage by weight of each component is:
(1) organic acid and derivative thereof: 0-60% (weight)
(2) condensation product of ethylene glycol or polymer: 10-90% (weight)
(3) pyrrolidones: 0-30% (weight)
(4) essence and flavoring agent: 0.1-5% (weight)
(5) deionized water: 0-40% (weight).
Organic acid of the present invention and derivative thereof (1) mainly comprise any or any two or more mixture in the compounds such as Carbenoxolone Sodium, dipotassium glycyrrhizinate, ammonium glycyrrhetate, lactic acid, sodium lactate, ethyl palmitate, isopropyl palmitate.Wherein be preferably Carbenoxolone Sodium and ethyl palmitate.
Compound additive of the present invention is characterized in that: the condensation product of described ethylene glycol or polymer (2) comprise any or any two or more mixture in polyethylene glycol, diglycol, the triethylene-glycol.
Pyrrolidones of the present invention (3) comprises one or both mixtures in polyvinylpyrrolidone, the 2-Pyrrolidone.
Compound additive of the present invention, the component of described essence and flavoring agent and the percentage by weight of each component are: tobacco extract 0.1-2% (weight), flue-cured tobacco ketone 0.005-0.05% (weight), 1% Rosa Damascana 0.005-0.05% (weight), malt extract 0.005-0.05% (weight), tomato extract 0.1-2% (weight).Wherein said tobacco extract is the extract of a kind of or any two or more tobacco leaf, offal or fragment in flue-cured tobacco, burley tobaccos, suncured tabacco and the Turkish tobaccos.
Compound additive of the present invention is applicable to various types of tobaccos and tobacco product thereof, is specially adapted to low-coke tar cigarette, also can add to make composite tip stick in the cigarette filter.
Thinking of the present invention: domestic and international research shows that the moisture of pipe tobacco can suitably be adjusted by artificial control and production technology, but the moisture of adjusting pipe tobacco can't produce important effect to flue gas moisture.The flue gas moisture size is relevant with source, kind and the place of production of pipe tobacco.Moisture in the pipe tobacco exists with three kinds of forms according to the difference of combination: free water, adsorbed water and water of constitution.And wherein have only water of constitution the most stable, because of it combines with some composition in the tobacco leaf, be the part of molecular structure.Equilibrium water conten behind tobacco shreds drying is mainly water of constitution, is the main source of flue gas moisture.
Most moisture that cigarette produces in the process of burning and sucking enter into side-stream smoke because of diffusion, only there is a part seldom to enter main flume, the particularly application of high air permeability cigarette paper and filter tip aeration technology, strengthened the diffusion of flue gas, cause the low-coke tar cigarette flue gas moisture less, flue gas is dry, and throat's comfortableness reduces, and sucking quality descends.In view of the moisture of pipe tobacco can't produce material impact to flue gas moisture, therefore in cigarette process, change process conditions, to add measures such as humectant not obvious to the effect that improves main flume moisture.Have only and improve in the pipe tobacco, perhaps change the transmittance process of moisture in flue gas, moisture is shifted as far as possible enter in the main flume, reduce water transport in side-stream smoke, could effectively improve the main flume moisture of cigarette in conjunction with the content of water.New additive agent just is being based on this principle development.
In addition, along with the reduction of tar content in cigarette, cause the change of cigarette style and the loss of cigarette perfume (or spice).Simultaneously, owing to added chemical addition agent, bring bad influence also can for the cigarette organoleptic quality, the present invention adds essence and flavoring agent (as tobacco extract, malt extract etc.) in prescription for this reason, remedy the loss of cigarette perfume (or spice), cover assorted gas, increase the saturating property sent out of flue gas.Remedy the deficiency of low-coke tar cigarette like this, kept the original style of cigarette and jealous, improved the saturating property sent out and the wettability of flue gas.
The preparation method of compound additive of the present invention:
1, the preparation of said tobacco extract in the compound additive of the present invention
Raw material is mainly a kind of or two or more arbitrarily in flue-cured tobacco, burley tobaccos, the Turkish tobaccos, and they can be tobacco leaf, offal or tobacco fragment.Raw tobacco material solvent heating and refluxing extraction, solvent are benzinum, second alcohol and water.Extract after filtration, vacuum and low temperature concentrates, and obtains tobacco extract.If further refining, can utilize technical finesses such as molecular clock, supercritical fluid extraction, the tobacco extract that obtains making with extra care.
2, the preparation of additive
Organic acid and derivative (1) thereof and pyrrolidones (3) are joined in the deionized water, add thermal agitation, temperature 30-80 ℃, make its all dissolving be scattered in the water; Join then in the condensation product or polymer (2) of ethylene glycol, add an amount of essence and flavoring agent again, add thermal agitation, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed gets final product, this compound additive is a kind of light yellow transparency liquid to rufous.
The application of compound additive of the present invention:
Additive of the present invention is of wide application, and is applicable to various types of tobaccos and tobacco product thereof, comprises flue-cured tobacco, burley tobaccos, suncured tabacco and Turkish tobaccos, and tobacco product such as expanded cut tobacco, expanded cut stem, reconstituted tobacoo.Its using method is: after in the reinforced process of cigarette processing technology compound additive and feed liquid being mixed, be sprayed directly on tobacco leaf and the pipe tobacco.Cigarette process routinely rolls into cigarette and props up through throwing, perfuming, cigarette technology.
The consumption of compound additive determines that according to cigarette smoke moisture general consumption is the 0.1%-10% of pipe tobacco weight, and preferable amount is 0.5%-2%.
Compound additive of the present invention also can be used as additives of filter tip and is used for filter tip, additive is scattered in the plasticizer, the acetate fibres that is sprayed onto shredding is intrafascicular, then the wire-beam forming of compound additive will have been added, the acetate fiber section of will feeding in raw material at last and acetate fiber section are compound, make the fine mouth rod of the compound vinegar of binary.The length ratio is 1: 1-2.
The addition of compound additive in filter tip is that 1mg-50mg/ props up, and preferred addition scope is that 2mg-30mg/ props up.
Compound additive of the present invention can add to by the 0.5%-10% of pipe tobacco weight in the cigarette of any brand, cigarette behind the adding additive is compared cigarette mainstream flue gas moisture to be increased with former brand cigarette, and whole style of cigarette and suction flavor are constant, flue gas is soft, increase the flue gas wettability, reducing stimulates, and improves throat's comfortableness.
The main flume analysis of cigarette sample:
Standard by the industry standard YC/T29-1996 of the People's Republic of China (PRC) is prepared smoking machine sample and smoking cigarette; Adopt GB/T5606.5-1996, YC/T29～30-1996, YC/T156～157-2001 standard, TPM, moisture, nicotine, tar and the CO content of detection cigarette smoke.
The aesthetic quality of cigarette sample smokes panel test:
Regulate and the atmospheric environment of testing by National Standard GB/T16447-1996 tobacco and tobacco product " regulate the cigarette sample moisture content, carry out the cigarette aesthetic quality by the panel of expert of smokeing panel test by the regulation of " specification requirement of GB5606.4-1996 cigarette sense organ " and smoke panel test.
Selected three different formulations leaf groups, added 2% compound additive respectively and experimentize, flue gas analysis testing result and smoking result see Table 1 and table 2.From analyzing data as can be seen: additive applies to the leaf group of different formulations all to the effect of being significantly increased of cigarette mainstream flue gas moisture.Compare with control sample, the main flume moisture of cigarette can improve 17.4%-26.7%.Smoking result in the table 2 shows that compound additive adds the soft flue gas of energy in the cigarette to, increases moist feeling, reduces excitant, obviously reduces throat and does thorn, the aesthetic quality who improves cigarette.
Table 1 compound additive is applied to different leaf group cigarette smoke analysis results
| Cigarette brand | Addition (%) | TPM (mg/ props up) | Flue gas moisture (mg/ props up) | Raising rate (%) | Nicotine amount (mg/ props up) | Tar content (mg/ props up) | CO (mg/ props up) |
| 1 2 3 | 2 0 2 0 2 0 | 13.6 12.5 20.5 19.3 17.5 16.8 | 1.9 1.5 3.6 3.0 2.7 2.3 | 26.7％ 20.0％ 17.4％ | 1.0 1.0 1.4 1.4 1.2 1.3 | 10.7 10.0 15.5 14.9 13.6 13.2 | 10.5 10.0 15.6 15.2 12.1 12.0 |
Table 2 cigarette smoke moisture improves the influence to the cigarette aesthetic quality
| The sample title | Describe | Moisture (mg) | The raising rate | The aesthetic quality |
| 1 2 3 | Control sample 2% control sample 2% control sample 2% | 1.5 1.9 3.0 3.6 2.3 2.7 | 26.7％ 20.0％ 17.4％ | Fragrance is soft, and is elegant, the perfume quantity foot, and harmony stimulates obviously, and pleasant impression is still comfortable.Fragrance is light slightly, and cigarette is fragrant fine and smooth soft, and humorous mixing up stimulates for a short time, and damp property is good, does not have the gas of obviously mixing, and pleasant impression is comfortable.Fragrance is plentiful, and is soft, stimulates obviously, and lingual surface has pricking method, do not have assorted gas, and pleasant impression is still clean.Fragrance is mellow and full, and is soft, stimulate little, sweet sense well, little have assorted gas, pleasant impression is clean.Give off a strong fragrance, saturating, it is heavy that thorn is done by throat, stimulates greatly, do not have assorted gas, and pleasant impression is still comfortable.Fragrance is soft, and concentration is light slightly, stimulates for a short time, and overall comfort is good, and sweet sense does not have assorted gas well, and pleasant impression is comfortable. |
Characteristics of the present invention are: (1) sufficient raw, technology is simple, and is easy to make, with low cost.(2) applied range can add in tobacco leaf and pipe tobacco, can add in the filter stick tow, also can add in reconstituted tobacoo.(3) adding technology is simple, need not change existing cigarette producing process.(4) can regulate and improve cigarette main flume moisture, keep the style of cigarette constant, increase the flue gas wettability, reducing stimulates, and improves throat's comfortableness.Thereby can satisfy smoker's psychological need, can alleviate the harm of smoking again human body.Improve core competence of enterprises, for enterprise brings considerable benefit.
The specific embodiment
By specific embodiment given below, can further be well understood to the present invention.But they are not limitation of the invention.
Embodiment 1
Take by weighing the 5g dipotassium glycyrrhizinate, be added in the 18.99g deionized water, add thermal agitation, between temperature 30-80 ℃, it is all dissolved be scattered in the water; Add the 75g diglycol then, add an amount of essence and flavoring agent (wherein tobacco extract 1.0g, flue-cured tobacco ketone 5mg, 1% Rosa Damascana 1mg, malt extract 4mg), add thermal agitation again, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive A.
Embodiment 2
According to the identical compound method of embodiment 1, take by weighing the 10g Carbenoxolone Sodium, be added in the 29.84g deionized water, add thermal agitation, between temperature 30-80 ℃, make its all dissolving be scattered in the water; Add the 60g triethylene-glycol then, add an amount of essence and flavoring agent (wherein tobacco extract 150mg, flue-cured tobacco ketone 3mg, 1% Rosa Damascana 1mg, malt extract 6mg), add thermal agitation again, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive B.
Embodiment 3
According to the identical compound method of embodiment 1, take by weighing the 10g dipotassium glycyrrhizinate, the 10g sodium lactate is added in the 29.79g deionized water, adds thermal agitation, between temperature 30-80 ℃, make its all dissolving be scattered in the water; Add an amount of essence and flavoring agent (wherein tobacco extract 200mg, flue-cured tobacco ketone 5mg, Rosa Damascana 1mg, malt extract 5mg), add thermal agitation again, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive C.
Embodiment 4
According to the identical compound method of embodiment 1, take by weighing the 30g dipotassium glycyrrhizinate, the 10g sodium lactate is added in the 29.79g deionized water, adds thermal agitation, between temperature 30-80 ℃, make its all dissolving be scattered in the water; Add an amount of essence and flavoring agent (wherein tobacco extract 200mg, flue-cured tobacco ketone 5mg, malt extract 5mg), add thermal agitation again, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive D.
Embodiment 5
According to the identical compound method of embodiment 1, take by weighing the 10g Carbenoxolone Sodium, be added in the 29.84g deionized water, add thermal agitation, between temperature 30-80 ℃, make its all dissolving be scattered in the water; Add the 30g triethylene-glycol then, add an amount of essence and flavoring agent (wherein tobacco extract 150mg, flue-cured tobacco ketone 3mg, 1% Rosa Damascana 1mg, malt extract 6mg), add thermal agitation again, temperature 20-60 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive E.
Embodiment 6
According to the identical compound method of embodiment 1, take by weighing the 5g Carbenoxolone Sodium, the 5g polyvinylpyrrolidone is added in the 39.95g ethanol, adds thermal agitation; Add the 10g polyethylene glycol then, the 20g ethyl palmitate adds an amount of essence and flavoring agent (wherein tobacco extract 50mg, flue-cured tobacco ketone 3mg), adds thermal agitation, temperature 30-40 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive F.
Embodiment 7
According to the identical compound method of embodiment 1, taking by weighing the 5g polyvinylpyrrolidone is added in the 49.95g ethanol, add thermal agitation, add the 10g polyethylene glycol then, the 40g ethyl palmitate adds an amount of essence and flavoring agent (wherein tobacco extract 50mg, flue-cured tobacco ketone 3mg), adds thermal agitation, temperature 30-40 ℃, the blending ingredients dissolving is uniformly dispersed promptly obtains compound additive G.
Embodiment 8～14
The common application process of compound additive of the present invention in cigarette is: get the compound additive A-E solution 1-5kg (pressing the 1-5% of pipe tobacco weight) for preparing, evenly spray application on the 100kg tobacco leaf with high pressure nozzle, the process of spraying is to return in the reinforced process at Ye Zuchao to carry out, cigarette process routinely rolls into cigarette and props up through throwing, perfuming, wraparound technology then.On same production line, roll the contrast cigarette by identical cigarette process and prop up.Carry out the cigarette mainstream flue gas analysis and the cigarette aesthetic quality smokes panel test, concrete outcome is listed in the table 3.
As seen from Table 3, compare with the contrast cigarette that does not contain compound additive by the cigarette that contains compound additive of the present invention that embodiment 8～14 obtains, cigarette mainstream flue gas moisture all is significantly increased, the raising rate has a certain distance, from 11.6% to 28.5% according to the kind of additive and consumption different.Aesthetic quality's smoking result shows the adding compound additive, and original style of cigarette is distinguished the flavor of with suction not to be influenced, the soft flue gas of energy, and raising flue gas exquisiteness, increase flue gas wettability reduces stimulation, improves throat's comfortableness.Obviously improve the aesthetic quality of cigarette.
Embodiment 15
The consumption that the compound additive F that embodiment 6 is prepared props up with 5mg/ adds in the filter rod, preparation binary composite filter tip.After this filter rod was applied to cigarette, cigarette mainstream flue gas moisture propped up from 1.6mg/ and is increased to 1.9mg/ and props up, and improves 18.8%.Aesthetic quality's smoking result shows that this additive keeps the style of cigarette constant, increases the flue gas wettability, and reducing stimulates, and improves throat's comfortableness.Improve cigarette sense organ suction quality.
Embodiment 16
The consumption that the compound additive F that embodiment 6 is prepared props up with 10mg/ adds in the filter rod, preparation binary composite filter tip.After this filter rod was applied to cigarette, cigarette mainstream flue gas moisture propped up from 1.7mg/ and is increased to 2.2mg/ and props up, and improves 29.4%.Aesthetic quality's smoking result shows that this additive keeps the style of cigarette constant, increases the flue gas wettability, and reducing stimulates, and improves throat's comfortableness.Improve cigarette sense organ suction quality.
Embodiment 17
The consumption that the compound additive G that embodiment 7 is prepared props up with 20mg/ adds in the filter rod, preparation binary composite filter tip.After this filter rod was applied to cigarette, cigarette mainstream flue gas moisture propped up from 1.6mg/ and is increased to 2.3mg/ and props up, and improves 43.7%.Aesthetic quality's smoking result shows that this additive keeps the style of cigarette constant, increases the flue gas wettability, and reducing stimulates, and improves throat's comfortableness.
Table 3 compound additive improves the effect of cigarette smoke moisture
| Embodiment | Additive types | Consumption (weight %) | Flue gas moisture raising rate (%) | Range of application |
| Embodiment 8 | A | 0.5 | 11.6 | Pipe tobacco |
| Embodiment 9 | A | 1.0 | 18.2 | Pipe tobacco |
| Embodiment 10 | A | 2.0 | 28.5 | Pipe tobacco |
| Embodiment 11 | B | 1.0 | 17.8 | Pipe tobacco |
| Embodiment 12 | C | 1.0 | 21.0 | Pipe tobacco |
| Embodiment 13 | D | 2.0 | 23.1 | Pipe tobacco |
| Embodiment 14 | E | 2.0 | 25.3 | Pipe tobacco |
| Embodiment 15 | F | 18.8 | Filter tip | |
| Embodiment 16 | F | 29.4 | Filter tip | |
| Embodiment 17 | G | 43.7 | Filter tip |
Claims (10)
1, a kind of compound additive that improves cigarette smoke moisture, it is characterized in that described compound additive mainly is grouped into by following one-tenth: the condensation product of organic acid and derivative thereof (1), ethylene glycol or polymer (2), pyrrolidones (3), essence and flavoring agent (4), deionized water (5), wherein the percentage by weight of each component is:
(1) organic acid and derivative thereof: 0-60%
(2) condensation product of ethylene glycol or polymer: 10-90%
(3) pyrrolidones: 0-30%
(4) essence and flavoring agent: 0.1-5%
(5) deionized water: 0-40%.
2, the compound additive of raising cigarette smoke moisture as claimed in claim 1 is characterized in that: described organic acid and derivative thereof (1) mainly comprise any or any two or more mixture in the compounds such as Carbenoxolone Sodium, dipotassium glycyrrhizinate, ammonium glycyrrhetate, lactic acid, sodium lactate, ethyl palmitate, isopropyl palmitate.
3, the compound additive of raising cigarette smoke moisture as claimed in claim 2 is characterized in that: described organic acid and derivative thereof are preferably Carbenoxolone Sodium and ethyl palmitate.
4, the compound additive of raising cigarette smoke moisture as claimed in claim 1 is characterized in that: the condensation product of described ethylene glycol or polymer (2) comprise any or any two or more mixture in polyethylene glycol, diglycol, the triethylene-glycol.
5, the compound additive of raising cigarette smoke moisture as claimed in claim 1 is characterized in that: described pyrrolidones (3) comprises one or both mixtures in polyvinylpyrrolidone, the 2-Pyrrolidone.
6, the compound additive of raising cigarette smoke moisture as claimed in claim 1, it is characterized in that: the component of described essence and flavoring agent and the percentage by weight of each component are: tobacco extract 0.1-2%, flue-cured tobacco ketone 0.005-0.05%, 1% Rosa Damascana 0.005-0.05%, malt extract 0.005-0.05%, tomato extract 0.1-2%.
7, a kind of application that improves the compound additive of cigarette smoke moisture is characterized in that: applicable to various types of tobaccos and tobacco product thereof, comprise flue-cured tobacco, burley tobaccos, suncured tabacco and Turkish tobaccos, and expanded cut tobacco, expanded cut stem, reconstituted tobacoo.
8, a kind of application that improves the compound additive of cigarette smoke moisture as claimed in claim 7 is characterized in that: its consumption determines that according to cigarette mainstream flue gas moisture general consumption is the 0.1%--10% of pipe tobacco weight.
9, a kind of application that improves the compound additive of cigarette smoke moisture is characterized in that: also can be used as additives of filter tip and be used for filter tip, additive is added to forming composite tip stick in the filter tip.
10, the application of the compound additive of raising cigarette smoke moisture as claimed in claim 9 is characterized in that: the addition of compound additive in filter tip is that 1mg-50mg/ props up, and preferred addition scope is that 2mg-30mg/ props up.
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| CN200610048649A CN100593980C (en) | 2006-08-31 | 2006-08-31 | Composite additive for raising cigarette smoke moisture and its use |
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| CN200610048649A CN100593980C (en) | 2006-08-31 | 2006-08-31 | Composite additive for raising cigarette smoke moisture and its use |
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| CN100593980C CN100593980C (en) | 2010-03-17 |
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| CN103060093A (en) * | 2012-12-28 | 2013-04-24 | 华宝食用香精香料（上海）有限公司 | Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use |
| CN103099310A (en) * | 2013-02-04 | 2013-05-15 | 红云红河烟草(集团)有限责任公司 | Tobacco humectant and application thereof |
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
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Family Cites Families (2)
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| CN87101921A (en) * | 1987-03-10 | 1988-02-24 | 魏太良 | Preparation for medicinal cigarette |
| CN1106807C (en) * | 1998-07-16 | 2003-04-30 | 吕次昌 | Moist-keeping agent for tobacco |
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- 2006-08-31 CN CN200610048649A patent/CN100593980C/en not_active Expired - Fee Related
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| CN103060093A (en) * | 2012-12-28 | 2013-04-24 | 华宝食用香精香料（上海）有限公司 | Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use |
| CN103099310A (en) * | 2013-02-04 | 2013-05-15 | 红云红河烟草(集团)有限责任公司 | Tobacco humectant and application thereof |
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
| CN103504475B (en) * | 2013-10-11 | 2015-06-17 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
| CN103767079A (en) * | 2014-01-21 | 2014-05-07 | 深圳市凯神科技股份有限公司 | Electronic cigarette oil solvent |
| CN106948222A (en) * | 2016-11-21 | 2017-07-14 | 云南中烟工业有限责任公司 | The fragrant cigarette paper of one kind profit, preparation method and the usage |
| CN106948222B (en) * | 2016-11-21 | 2018-05-04 | 云南中烟工业有限责任公司 | The fragrant cigarette paper of one kind profit, preparation method and the usage |
| CN107183783A (en) * | 2017-07-25 | 2017-09-22 | 云南中烟工业有限责任公司 | A kind of high retention efficiency filter for preventing that filter tip heat from collapsing |
| CN113017142A (en) * | 2019-12-24 | 2021-06-25 | 深圳波顿香料有限公司 | Fuming gel, preparation method thereof and low-temperature smoke with gel |
| CN114886154A (en) * | 2022-05-27 | 2022-08-12 | 河南中烟工业有限责任公司 | Additive for improving filter tip ventilated cigarette dry feeling and preparation method thereof |
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