CN1917757B - 包含聚合物粘着剂的种子处理用配制剂 - Google Patents
包含聚合物粘着剂的种子处理用配制剂 Download PDFInfo
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- CN1917757B CN1917757B CN2005800050442A CN200580005044A CN1917757B CN 1917757 B CN1917757 B CN 1917757B CN 2005800050442 A CN2005800050442 A CN 2005800050442A CN 200580005044 A CN200580005044 A CN 200580005044A CN 1917757 B CN1917757 B CN 1917757B
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- methyl
- acrylate
- seed
- acrylamide
- acid
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- FZXISNSWEXTPMF-UHFFFAOYSA-N terbutylazine Chemical compound CCNC1=NC(Cl)=NC(NC(C)(C)C)=N1 FZXISNSWEXTPMF-UHFFFAOYSA-N 0.000 description 1
- 229940063650 terramycin Drugs 0.000 description 1
- IWVCMVBTMGNXQD-UHFFFAOYSA-N terramycin dehydrate Natural products C1=CC=C2C(O)(C)C3C(O)C4C(N(C)C)C(O)=C(C(N)=O)C(=O)C4(O)C(O)=C3C(=O)C2=C1O IWVCMVBTMGNXQD-UHFFFAOYSA-N 0.000 description 1
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- UBCKGWBNUIFUST-YHYXMXQVSA-N tetrachlorvinphos Chemical compound COP(=O)(OC)O\C(=C/Cl)C1=CC(Cl)=C(Cl)C=C1Cl UBCKGWBNUIFUST-YHYXMXQVSA-N 0.000 description 1
- LITQZINTSYBKIU-UHFFFAOYSA-F tetracopper;hexahydroxide;sulfate Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Cu+2].[Cu+2].[Cu+2].[Cu+2].[O-]S([O-])(=O)=O LITQZINTSYBKIU-UHFFFAOYSA-F 0.000 description 1
- 125000003831 tetrazolyl group Chemical group 0.000 description 1
- NWWZPOKUUAIXIW-FLIBITNWSA-N thiamethoxam Chemical compound [O-][N+](=O)\N=C/1N(C)COCN\1CC1=CN=C(Cl)S1 NWWZPOKUUAIXIW-FLIBITNWSA-N 0.000 description 1
- 125000000437 thiazol-2-yl group Chemical group [H]C1=C([H])N=C(*)S1 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
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- DNVLJEWNNDHELH-UHFFFAOYSA-N thiocyclam Chemical compound CN(C)C1CSSSC1 DNVLJEWNNDHELH-UHFFFAOYSA-N 0.000 description 1
- BAKXBZPQTXCKRR-UHFFFAOYSA-N thiodicarb Chemical compound CSC(C)=NOC(=O)NSNC(=O)ON=C(C)SC BAKXBZPQTXCKRR-UHFFFAOYSA-N 0.000 description 1
- 229960002447 thiram Drugs 0.000 description 1
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 description 1
- 235000010215 titanium dioxide Nutrition 0.000 description 1
- OBZIQQJJIKNWNO-UHFFFAOYSA-N tolclofos-methyl Chemical compound COP(=S)(OC)OC1=C(Cl)C=C(C)C=C1Cl OBZIQQJJIKNWNO-UHFFFAOYSA-N 0.000 description 1
- WPALTCMYPARVNV-UHFFFAOYSA-N tolfenpyrad Chemical compound CCC1=NN(C)C(C(=O)NCC=2C=CC(OC=3C=CC(C)=CC=3)=CC=2)=C1Cl WPALTCMYPARVNV-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- NKNFWVNSBIXGLL-UHFFFAOYSA-N triazamate Chemical compound CCOC(=O)CSC1=NC(C(C)(C)C)=NN1C(=O)N(C)C NKNFWVNSBIXGLL-UHFFFAOYSA-N 0.000 description 1
- FFSJPOPLSWBGQY-UHFFFAOYSA-N triazol-4-one Chemical compound O=C1C=NN=N1 FFSJPOPLSWBGQY-UHFFFAOYSA-N 0.000 description 1
- BQZXUHDXIARLEO-UHFFFAOYSA-N tribenuron Chemical compound COC1=NC(C)=NC(N(C)C(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(O)=O)=N1 BQZXUHDXIARLEO-UHFFFAOYSA-N 0.000 description 1
- YMXOXAPKZDWXLY-QWRGUYRKSA-N tribenuron methyl Chemical group COC(=O)[C@H]1CCCC[C@@H]1S(=O)(=O)NC(=O)N(C)C1=NC(C)=NC(OC)=N1 YMXOXAPKZDWXLY-QWRGUYRKSA-N 0.000 description 1
- ONCZDRURRATYFI-TVJDWZFNSA-N trifloxystrobin Chemical compound CO\N=C(\C(=O)OC)C1=CC=CC=C1CO\N=C(/C)C1=CC=CC(C(F)(F)F)=C1 ONCZDRURRATYFI-TVJDWZFNSA-N 0.000 description 1
- HSMVPDGQOIQYSR-KGENOOAVSA-N triflumizole Chemical compound C1=CN=CN1C(/COCCC)=N/C1=CC=C(Cl)C=C1C(F)(F)F HSMVPDGQOIQYSR-KGENOOAVSA-N 0.000 description 1
- XAIPTRIXGHTTNT-UHFFFAOYSA-N triflumuron Chemical compound C1=CC(OC(F)(F)F)=CC=C1NC(=O)NC(=O)C1=CC=CC=C1Cl XAIPTRIXGHTTNT-UHFFFAOYSA-N 0.000 description 1
- AKTQJCBOGPBERP-UHFFFAOYSA-N triflusulfuron Chemical compound FC(F)(F)COC1=NC(N(C)C)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2C)C(O)=O)=N1 AKTQJCBOGPBERP-UHFFFAOYSA-N 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- KVEQCVKVIFQSGC-UHFFFAOYSA-N tritosulfuron Chemical compound FC(F)(F)C1=NC(OC)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(F)(F)F)=N1 KVEQCVKVIFQSGC-UHFFFAOYSA-N 0.000 description 1
- JARYYMUOCXVXNK-CSLFJTBJSA-N validamycin A Chemical compound N([C@H]1C[C@@H]([C@H]([C@H](O)[C@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)CO)[C@H]1C=C(CO)[C@@H](O)[C@H](O)[C@H]1O JARYYMUOCXVXNK-CSLFJTBJSA-N 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 150000004669 very long chain fatty acids Chemical class 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 239000004552 water soluble powder Substances 0.000 description 1
- 239000005943 zeta-Cypermethrin Substances 0.000 description 1
- AMHNZOICSMBGDH-UHFFFAOYSA-L zineb Chemical compound [Zn+2].[S-]C(=S)NCCNC([S-])=S AMHNZOICSMBGDH-UHFFFAOYSA-L 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/24—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients to enhance the sticking of the active ingredients
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
- A01N25/10—Macromolecular compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/50—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids the nitrogen atom being doubly bound to the carbon skeleton
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/52—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing groups, e.g. carboxylic acid amidines
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- A—HUMAN NECESSITIES
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
- A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
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Abstract
本发明涉及一种种子处理配制剂,其包含(a)至少一种农药;和(b)含羧基的聚合物或共聚物,选自玻璃化转变温度为-40℃至5℃的丁苯橡胶胶乳聚合物、特定的丙烯酸酯共聚物和特定的乙烯/乙酸乙烯酯共聚物;含有该配制剂的种子,一种在播种前处理种子的方法,一种抵抗不希望的植物生长和/或昆虫和/或真菌的方法。
Description
本发明包括一种种子处理配制剂,其包含:
(a)至少一种农药;和
(b)含羧基的聚合物或共聚物,选自玻璃化转变温度为-40℃至5℃的丁苯橡胶胶乳聚合物、丙烯酸酯共聚物和乙烯/乙酸乙烯酯共聚物,其中
(i)丙烯酸酯共聚物由如下单体组成:
(a’)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)选自下列的单体:(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯,以及(甲基)丙烯酰胺,例如二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺;和
(c’)选自下列的单体:丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、甲基丙烯酸2-羟乙酯、甲基丙烯酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;和
(d’)选自苯乙烯和苯乙烯衍生物的单体,例如苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯、对甲氧基苯乙烯;
且该丙烯酸酯共聚物得玻璃化转变温度为-40℃至5℃,或者如果其具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃;和
(ii)乙烯/乙酸乙烯酯聚合物由乙酸乙烯酯、乙烯和丙烯酸组成且玻璃化转变温度为-25℃至-5℃。
种子处理是保护种子免受有害物(真菌和昆虫)侵害且适合如下作物种子的有希望的方法:玉米(甜玉米和野玉米(field corn))、大豆、小麦、大麦、燕麦、稻、棉花、向日葵、苜蓿、高粱、油菜籽、甜菜、芸苔属、西红柿、豆、胡萝卜、烟草以及花籽如三色堇、凤仙花属植物、矮牵牛和老鹳草,如由Japan Plant Protection Association(第133-139页,“PesticideApplication Technology”,1998)所述。
农民面对的问题之一是用于种子处理的农药快速释放于土壤中或水中。尤其是在稻种处理中(如在种子浸渍方法中),农药释放是一个很大的问题,因为一方面是环境安全,另一方面是失去了农药抵抗土壤滋生真菌和昆虫的保护。
WO 01/78507公开了一种用于非浸渍法的稻种处理配制剂,将聚乙酸乙烯酯、聚乙烯醇、聚乙烯吡咯烷酮和聚氨酯混合物作为用于种子处理配制剂的聚合物。
WO 02/080675公开了种子处理配制剂并公开了大量适用于种子处理配制剂的不具有共同化学特征的聚合物。
所有上述配制剂均显示农药释放至环境中。
因此,本发明的目的是提供一种种子处理配制剂,该配制剂优选在种子浸渍和/或萌发(prime)过程中使农药保持在种子上并防止农药明显释放到环境中(水或土壤)。
在本发明中,该目的通过提供一种包含如下组分的种子处理配制剂实现:
(a)至少一种农药;和
(b)含羧基的聚合物或共聚物,其选自玻璃化转变温度为-40℃至5℃的丁苯橡胶胶乳聚合物、丙烯酸酯共聚物和乙烯/乙酸乙烯酯共聚物,其中
(i)丙烯酸酯共聚物由如下单体组成:
(a’)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)选自下列的单体:(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯,以及(甲基)丙烯酰胺,例如二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺;和
(c’)选自下列的单体:丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、甲基丙烯酸2-羟乙酯、甲基丙烯酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;和
(d’)选自苯乙烯和苯乙烯衍生物的单体,例如苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯、对甲氧基苯乙烯;
且该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃;或者如果其具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃;和
(ii)乙烯/乙酸乙烯酯聚合物由乙酸乙烯酯、乙烯和丙烯酸组成且玻璃化转变温度为-25℃至-5℃。
在优选实施方案中,羧基含量r至少为0.05-20重量%,优选0.05-5重量%,更优选0.1-3重量%。
本发明的丙烯酸酯共聚物为包含下列单体的那些:
(a)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)选自下列的单体:(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯,以及(甲基)丙烯酰胺,例如二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺;和
(c)选自下列的单体:丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、甲基丙烯酸2-羟乙酯、甲基丙烯酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;和
(d)选自苯乙烯和苯乙烯衍生物的单体,例如苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯、对甲氧基苯乙烯。
优选的丙烯酸酯共聚物为包含下列单体的那些:
(a)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(c)丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、丙烯酸2-羟丙酯或甲基丙烯酸2-羟丙酯;和
(d)苯乙烯。
更优选的为包含下列单体的那些丙烯酸酯共聚物:
(a)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d)苯乙烯。
最优选的为具有如下组成的那些丙烯酸酯共聚物:
(a)0.2-6重量%的丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)50-99.8重量%的甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d)0-50重量%的苯乙烯。
在特别优选的实施方案中,丙烯酸酯共聚物具有核壳结构。这些丙烯酸酯共聚物可以通过已知技术,例如通过逐步乳液聚合技术而制备。
在第一步中,核聚合物用丙烯酸酯共聚物的单体(参见上述定义)通过乳液聚合法制备。在第二步中,将丙烯酸酯共聚物的单体(参见上述定义)在分散的在第一步中制备的核聚合物存在下聚合而产生壳结构(例如参见可由http://www2.warwick.ac.uk/fac/sci/chemistry/cim/research/haddleton/posters/gordon03charlie.pdf得到的Wagner等人,Polymer Chemistry&Technology,Publication of Unversity of Warwick,Center for Interfacesand Materials)。
上述不具有核壳结构的丙烯酸酯共聚物的玻璃化转变温度为-40℃至15℃,优选-30℃至10℃,更优选-30℃至5℃,最优选-25℃至-5℃。
具有核壳结构的丙烯酸酯共聚物的内核的玻璃化转变温度(Tg)为-60℃至5℃,优选-40℃至0℃,更优选-30℃至-5℃。
具有核壳结构的丙烯酸酯共聚物的外壳的Tg为20-150℃,优选80-130℃。
本发明的乙烯/乙酸乙烯酯聚合物主要由乙烯和乙酸乙烯酯组成,也可以包含丙烯酸。本发明的乙烯/乙酸乙烯酯聚合物的玻璃化转变温度为-25℃至-5℃。
最优选具有10-40重量%乙烯和60-90重量%乙酸乙烯酯和0-4重量%丙烯酸的那些乙烯/乙酸乙烯酯共聚物。
上述乙酸乙烯酯共聚物也可部分水解成相应的乙烯醇。
本发明丁苯橡胶胶乳聚合物包含:
(1)(烷基)丙烯酸和(烷基)丙烯酸酯衍生物如:
a)(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯、(甲基)丙烯酸2-羟乙酯、(甲基)丙烯酸2-羟丙酯,
b)氟化的(甲基)丙烯酸烷基酯,例如(甲基)丙烯酸氟化烷基酯;(甲基)丙烯酸三氟乙基酯、(甲基)丙烯酸五氟丙基酯、(甲基)丙烯酸七氟丁基酯,
c)硅氧烷基化合物,例如(甲基)丙烯酸三甲基硅氧烷基二甲代甲硅基丙酯、(甲基)丙烯酸三(三甲基硅氧烷基)甲硅基丙酯、二(甲基)丙烯酰丙基·二甲代甲硅烷基醚,
d)含氨基的(甲基)丙烯酸酯,例如(甲基)丙烯酸二甲氨基甲酯、(甲基)丙烯酸二甲氨基乙酯、(甲基)丙烯酸二甲氨基丙酯、(甲基)丙烯酸二乙氨基甲酯、(甲基)丙烯酸二乙氨基丙酯,
e)烷撑二醇的单或二(甲基)丙烯酸酯,例如乙二醇、1,2-丙二醇、1,3-丙二醇、1,6-己二醇的单或二(甲基)丙烯酸酯,
f)(甲基)丙烯酸烷氧基烷基酯,例如(甲基)丙烯酸2-甲氧基乙酯、(甲基)丙烯酸2-乙氧基乙酯、(甲基)丙烯酸3-乙氧基丙酯,
g)(甲基)丙烯酸芳氧基烷基酯,例如(甲基)丙烯酸2-苯氧基乙酯、(甲基)丙烯酸2-苯氧基丙酯、(甲基)丙烯酸3-苯氧基丙酯,
h)低聚(甲基)丙烯酸酯,例如多元醇如甘油、1,2,4-丁三醇、季戊四醇、三羟甲基链烷(C1-C3)、四羟甲基链烷(C1-C3)的二(甲基)丙烯酸酯、三(甲基)丙烯酸酯或四(甲基)丙烯酸酯,
i)(甲基)丙烯酸羟基烷基酯,例如(甲基)丙烯酸2-羟乙酯、(甲基)丙烯酸2-羟丙酯、(甲基)丙烯酸3-羟丙酯,
j)由下式(I)代表的环酯的开环缩合(甲基)丙烯酸酯:
CH2=CR4-COO-(CmH2mCOO)t-R5 …(I)
其中
R4为C1-C5烷基,R5为氢或C1-C10烷基或苯基,m和t为1-10的整数;
如CH2=CH-COO-C3H6COO-H、CH2=C(CH3)-COO-C3H6COO-H、CH2=CH-COO-C4H8COO-H、CH2=C(CH3)-COO-C4H8COO-H、CH2=CH-COO-C5H10COO-H、CH2=C(CH3)-COO-C5H10COO-H、CH2=CH-COO-C3H6COO-CH3、CH2=C(CH3)-COO-C3H6COO-CH3、CH2=CH-COO-C4H8COO-CH3、CH2=C(CH3)-COO-C4H8COO-CH3、CH2=CH-COO-C5H10COO-CH3、CH2=C(CH3)-COO-C5H10COO-CH3、CH2=CH-COO-C5H10COO-C2H5、CH2=C(CH3)-COO-C5H10COO-C2H5、CH2=CH-COO-C5H10COO-C4H9、CH2=C(CH3)-COO-C5H10COO-C4H9、CH2=CH-COO-C5H10COO-C8H17、CH2=C(CH3)-COO-C5H10COO-C8H17、CH2=CH-COO-(C3H6COO)2-H、CH2=C(CH3)-COO-(C3H6COO)2-H、CH2=CH-COO-(C4H8COO)2-H、CH2=C(CH3)-COO-(C4H8COO)2-H、CH2=CH-COO-(C5H10COO)2-H、CH2=C(CH3)-COO-(C5H10COO)2-H、CH2=CH-COO-(C3H6COO)2-C2H5、CH2=C(CH3)-COO-(C3H6COO)2-C2H5、CH2=CH-COO-(C4H8COO)2-C2H5、CH2=C(CH3)-COO-(C4H8COO)2-C2H5、CH2=CH-COO-(C5H10COO)2-C2H5、CH2=C(CH3)-COO-(C5H10COO)2-C2H5、CH2=CH-COO-(C5H10COO)3-C2H5、CH2=C(CH3)-COO-(C5H10COO)3-C2H5、CH2=CH-COO-(C5H10COO)4-C2H5、CH2=C(CH3)-COO-(C5H10COO)4-C2H5、CH2=CH-COO-(C5H10COO)5-C2H5、CH2=C(CH3)-COO-(C5H10COO)5-C2H5、CH2=CH-COO-(C5H10COO)2-C8H17、CH2=C(CH3)-COO-(C5H10COO)2-C8H17;
和/或
(2)(甲基)丙烯酰胺,例如二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺,以及(甲基)丙烯酰胺的衍生物如N-甲基丙烯酰胺、N-羟甲基丙烯酰胺、N-羟甲基甲基丙烯酰胺;
和/或
(3)丙烯酸氰基(烷基)酯如(甲基)丙烯酸氰烷基酯;(甲基)丙烯酸氰基乙酯、(甲基)丙烯酸氰基丙酯;
和/或
(4)丙烯腈类如丙烯腈、甲基丙烯腈;
和/或
(5)不饱和一元羧酸酯,例如巴豆酸甲酯、巴豆酸乙酯、肉桂酸甲酯、肉桂酸乙酯;
如/或
(6)不饱和羧酸的羟基烷基酯,例如巴豆酸2-羟乙酯、巴豆酸2-羟丙酯、肉桂酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;
和/或
(7)不饱和(一元)羧酸,例如巴豆酸、肉桂酸、马来酸、衣康酸;
和/或
(8)不饱和多元羧酸及其酸酐、单酯或二酯,例如马来酸、富马酸、衣康酸、柠康酸,以及上述酸的酸酐;
和/或
(9)乙烯基酯,例如乙酸乙烯酯、氯乙酸乙烯酯、丙酸乙烯酯,
和/或
(10)C4-C12链二烯,例如1,3-丁二烯、2-甲基-1,3-丁二烯(=异戊二烯)、2,3-二甲基-1,3-丁二烯、1,3-戊二烯、2-甲基-1,3-戊二烯、1,3-己二烯、4,5-二乙基-1,3-辛二烯、3-丁基-1,3-辛二烯;
和/或
(11)乙烯基吡啶如2-乙烯基吡啶、4-乙烯基吡啶;
和/或
(12)苯乙烯和苯乙烯衍生物,例如苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯、对甲氧基苯乙烯。
丁苯橡胶胶乳共聚物的玻璃化转变温度为-40℃至15℃,优选-30℃至10℃,更优选-30℃至5℃,最优选-25℃至-5℃。
优选如上定义的丙烯酸酯共聚物和乙烯/乙酸乙烯酯共聚物。如上定义的丙烯酸酯共聚物是最优选的。
聚合物、共聚物的玻璃化转变温度由差示扫描量热计(DSC)测定。将所有试样在110℃下干燥1小时以消除水/溶剂对共聚物Tg的影响。DSC试样尺寸为约10-15mg。通常在N2气氛下,从-100℃至100℃以20℃/min进行测量。Tg由转变区的中间点测得。
所有上述聚合物和共聚物在下文中称为“粘着剂”。
本发明包括粘着剂在制备种子处理配制剂中的用途。
农药为至少一种杀真菌剂或至少一种杀虫剂或者由杀真菌剂和至少一种杀虫剂组成的混合物;或为至少一种除草剂和/或安全剂或者包含除草剂和/或安全剂和至少一种选自杀真菌剂和杀虫剂的农药的混合物。优选活性成分为至少一种杀真菌剂或至少一种杀虫剂或由至少一种杀真菌剂和至少一种杀虫剂组成的混合物。
术语安全剂具有如下含义:已知在某些情况下通过联合施用特定作用的除草剂和有机活性化合物可获得较好的作物相容性,其中一些有机活性化合物本身具有除草活性。在这些情况下,活性化合物作为解毒剂和拮抗剂,由于它们事实上可减少或甚至防止作物受到损害,在本文中它们也称为安全剂。
杀真菌剂选自:
·酰基丙氨酸类,如苯霜灵(benalaxyl)、呋氨丙灵(furalaxyl)、甲霜灵(metalaxyl)、甲呋酰胺(ofurace)、噁霜灵(oxadixyl),
·胺衍生物,如aldimorph、多果定(dodine)、吗菌灵(dodemorph)、丁苯吗啉(fenpropimorph)、苯锈啶(fenpropidin)、双胍盐(guazatine)、双胍辛醋酸盐(iminoctadine)、螺噁茂胺(spiroxamin)或克啉菌(tridemorph),
·苯胺基嘧啶类,如二甲嘧菌胺(pyrimethanil)、嘧菌胺(mepanipyrim)或cyrodinyl,
·抗菌素,如放线菌酮(cycloheximid)、灰黄霉素(griseofulvin)、春雷霉素(kasugamycin)、多马霉素(natamycin)、多氧霉素(polyoxin)或链霉素(streptomycin)、有效霉素(validamycin A),
·唑类,如双苯三唑醇(bitertanol)、糠菌唑(bromnconazole)、氰霜唑(cyazofamide)、环唑醇(cyproconazole)、噁醚唑(difenoconazole)、烯唑醇(dinitroconazole)、氧唑菌(epoxiconazole)、氯唑灵(etridazole)、腈苯唑(fenbuconazole)、喹唑菌酮(fluquinconazole)、氟硅唑(flusilazole)、粉唑醇(flutriafol)、麦穗宁(fuberidazole)、己唑醇(hexaconazole)、土菌消(hymexazole)、烯菌灵(imazalil)、酰胺唑(imibenconazole)、环戊唑菌(metconazole)、腈菌唑(myclobutanil)、戊菌唑(penconazole)、perfurazoate、丙环唑(propiconazole)、丙氯灵(prochloraz)、丙硫菌唑(prothioconazole)、硅氟唑(simeconazole)、戊唑醇(tebuconazole)、氟醚唑(tetraconazole)、涕必灵(thiabendazole)、三唑酮(triadimefon)、唑菌醇(triadimenol)、氟菌唑(triflumizol)、戊叉唑菌(triticonazole),5-氯-7-(4-甲基哌啶-1-基)-6-(2,4,6-三氟苯基)-[1,2,4]三唑并[1,5-a]嘧啶、2-丁氧基-6-碘-3-丙基苯并吡喃-4-酮、3-(3-溴-6-氟-2-甲基吲哚-1-磺酰基)-[1,2,4]三唑-1-磺酸二甲酰胺,
·二羧酰亚胺类,如异丙定(iprodion)、甲菌利(myclozolin)、杀菌利(procymidon)、烯菌酮(vinclozolin),
·二硫代氨基甲酸盐类,如福美铁(ferbam)、代森钠(nabam)、代森锰(maneb)、代森锰锌(mancozeb)、威百亩(metam)、代森联(metiram)、甲基代森锌(propineb)、福代锌(polycarbamate)、福美双(thiram)、福美锌(ziram)、代森锌(zineb),
·杂环化合物,如敌菌灵(anilazine)、苯菌灵(benomyl)、啶酰菌胺(boscalid)、多菌灵(carbendazim)、萎锈灵(carboxin)、氧化萎锈灵(oxycarboxin)、氰霜唑(cyazofamid)、棉隆(dazomet)、二噻农(dithianon)、乙菌定(ethirimol)、甲菌定(dimethirimol)、噁唑酮菌(famoxadon)、咪唑菌酮(fenamidon)、异嘧菌醇(fenarimol)、麦穗宁(fuberidazole)、氟酰胺(flutolanil)、呋吡唑灵(furametpyr)、稻瘟灵(isoprothiolane)、丙氧灭绣胺(mepronil)、氟苯嘧啶醇(nuarimol)、异噻菌酮(octhilinone)、噻菌灵(probenazole)、丙氧喹啉(proquinazid)、啶斑肟(pyrifenox)、咯喹酮(pyroquilon)、喹氧灵(quinoxyfen)、硅噻菌胺(silthiofam)、涕必灵、溴氟唑菌(thifluzamid)、甲基托布津(thiophanate-methyl)、噻酰菌胺(tiadinil)、三环唑(tricyclazole)、嗪氨灵(triforine)、3-[5-(4-氯苯基)-2,3-二甲基异噁唑烷-3-基]吡啶、磺嘧菌灵(bupirimate),
·铜杀真菌剂,如波尔多液(Bordeaux混合物)、醋酸铜、氢氧化铜、王铜、碱式硫酸铜,
·硝基苯基衍生物,如乐杀螨(binapacryl)、敌螨普(dinocap)、敌螨通(dinobuton)、异丙消(nitrophthalisopropyl),
·苯基吡咯类,如拌种咯(fenpiclonil)或氟噁菌(fludioxonil),
·硫,
·有机金属化合物,如三苯基锡盐,
·有机磷化合物,如克瘟散(edifenphos)、克瘟散(Edifenphos)、异稻瘟净(Iprobenfos)、定菌磷(Pyrazophos)、甲基立枯磷(tolclofos-methyl)、藻菌磷(fosetyl)、藻菌磷(fosetyl-aluminum)、亚磷酸,
·其它杀真菌剂,如噻二唑素(acibenzolar-S-methyl)、苯噻菌胺(benthiavalicarb)、氯环丙酰胺(carpropamid)、百菌清(chlorothalonil)、环氟菌胺(cyflufenamid)、清菌脲(cymoxanil)、棉隆(dazomet)、哒菌清(diclomezin)、双氯氰菌胺(diclocymet)、乙霉威(diethofencarb)、噻唑菌胺(ethaboxam)、环酰菌胺(fenhexamid)、薯瘟锡(fentin-acetate)、氰菌胺(fenoxanil)、嘧菌腙(ferimzone)、氟啶胺(fluazinam)、藻菌磷(fosetyl)、藻菌磷(fosetyl-aluminum)、异丙菌胺(iprovalicarb)、六氯苯(hexachlorobenzene)、苯菌酮(metrafenon)、戊菌隆(pencycuron)、百维灵(propamocarb)、四氯苯酞(phthalide)、甲基立枯磷、五氯硝基苯(quintozene)、苯酰菌胺(zoxamid)、稻瘟灵、probenfos、苯酰菌胺(zoxamide)、氟吡菌胺(Fluopicolide)(Picobenzamid);氯环丙酰胺、双炔酰菌胺(Mandipropamid)、N-(2-{4-[3-(4-氯苯基)-丙-2-炔氧基]-3-甲氧基苯基}乙基)-2-甲磺酰氨基-3-甲基丁酰胺、N-(2-{4-[3-(4-氯苯基)-丙-2-炔氧基]-3-甲氧基苯基}乙基)-2-乙磺酰氨基-3-甲基丁酰胺;呋吡唑灵(furametpyr)、溴氟唑菌(thifluzamide)、吡噻菌胺(penthiopyrad)、环酰菌胺、3,4-二氯异噻唑-5-甲酸(2-氰基苯基)酰胺、flubenthiavalicarb、3-(4-氯苯基)-3-(2-异丙氧基羰基氨基-3-甲基丁酰氨基)丙酸甲酯、{2-氯-5-[1-(6-甲基吡啶-2-基甲氧基亚氨基)乙基]苄基}氨基甲酸甲酯、{2-氯-5-[1-(3-甲基苄氧基亚氨基)乙基]苄基}氨基甲酸甲酯、磺菌胺(flusulfamide)、四氯苯酞、六氯苯、下式酰胺:
其中
X为CHF2或CH3;和
R1、R2互相独立地为卤素、甲基或卤代甲基;
·嗜球果伞素类,如腈嘧菌酯(azoxystrobin)、醚菌胺(dimoxystrobin)、烯肟菌酯(enestroburin)、氟嘧菌酯(fluoxastrobin)、亚胺菌(kresoxim-methyl)、叉氨苯酰胺(metominostrobin)、肟醚菌胺(orysastrobin)、啶氧菌酯(picoxystrobin)、唑菌胺酯(pyraclostrobin)或肟菌酯(trifloxystrobin),
·次磺酸衍生物,如敌菌丹(captafol)、克菌丹(captan)、抑菌灵(dichlofluanid)、灭菌丹(folpet)、对甲抑菌灵(tolylfluanid),
·肉桂酰胺及类似化合物,如烯酰吗啉(dimethomorph)、氟联苯菌(flumetover)或氟吗啉(flumorph),
·酰胺杀真菌剂,如cyclofenamid或(Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺;
优选苯菌灵、甲基托布津、涕必灵、环戊唑醇(ipconazole)、氟菌唑、稻瘟酯(pefurazoate)、喹菌酮(oxolinic acid)、氟噁菌、福美双、氢氧化铜、王铜、克菌丹、春雷霉素、肟醚菌胺、丙氧灭绣胺、氟酰胺、甲基立枯磷、土霉素(oxytetracycline)、双胍辛醋酸盐、氧唑菌、喹唑菌酮、环戊唑菌、丙氯灵、戊叉唑菌、戊唑醇、噻菌灵、咯喹酮、噻二唑素、氯环丙酰胺、双氯氰菌胺、氰菌胺、腈嘧菌酯、醚菌胺、氟嘧菌酯、亚胺菌、叉氨苯酰胺、肟醚菌胺、啶氧菌酯、唑菌胺酯或肟菌酯、三环唑、噻酰菌胺、稻瘟灵、异稻瘟净;
更优选苯菌灵、甲基托布津、涕必灵、环戊唑醇、氟菌唑、丙氯灵、稻瘟酯、喹菌酮、氟噁菌、福美双、氢氧化铜、王铜、克菌丹、春雷霉素、肟醚菌胺、噻菌灵、咯喹酮、噻二唑素、氯环丙酰胺、双氯氰菌胺、噻酰菌胺、三环唑;
最优选肟醚菌胺。
杀虫剂选自:
有机磷酸酯类:高灭磷(Acephate)、谷硫磷(Azinphos-methyl)、毒死蜱(Chlorpyrifos)、毒虫畏(Chlorfenvinphos)、二嗪农(Diazinon)、敌敌畏(Dichlorvos)、甲基毒虫畏(dimethylvinphos)、杀抗松(dioxabenzofos)、百治磷(Dicrotophos)、乐果(Dimethoate)、乙拌磷(Disulfoton)、乙硫磷(Ethion)、苯硫磷(EPN)、杀螟松(Fenitrothion)、倍硫磷(Fenthion)、异噁唑磷(Isoxathion)、马拉硫磷(Malathion)、甲胺磷(Methamidophos)、杀扑磷(Methidathion)、甲基一六零五(Methyl-parathion)、速灭磷(Mevinphos)、久效磷(Monocrotophos)、砜吸磷(Oxydemeton-methyl)、对氧磷(Paraoxon)、一六零五(Parathion)、稻丰散(Phenthoate)、伏杀磷(Phosalone)、亚胺硫磷(Phosmet)、磷胺(Phosphamidon)、甲拌磷(Phorate)、辛硫磷(Phoxim)、虫螨磷(Pirimiphos-methyl)、丙溴磷(Profenofos)、丙硫磷(Prothiofos)、乙基虫螨磷(pirimiphos-ethyl)、吡唑硫磷(pyraclofos)、打杀磷(pyridaphenthion)、乙丙硫磷(Sulprophos)、三唑磷(Triazophos)、敌百虫(Trichlorfon);杀虫畏(tetrachlorvinphos)、蚜灭多(vamidothion);
氨基甲酸酯类:棉铃威(Alanycarb)、丙硫克百威(Benfuracarb)、噁虫威(Bendiocarb)、甲萘威(Carbaryl)、丁苯威(BPMC)、虫螨威(carbofuran)、丁硫克百威(Carbosulfan)、双氧威(Fenoxycarb)、呋线威(Furathiocarb)、噁二唑虫(Indoxacarb)、灭虫威(Methiocarb)、灭多虫(Methomyl)、甲氨叉威(Oxamyl)、抗蚜威(Pirimicarb)、残杀威(Propoxur)、硫双威(Thiodicarb)、唑蚜威(Triazamate);
拟除虫菊酯类:氟氯菊酯(Bifenthrin)、氟氯氰菊酯(Cyfluthrin)、乙氰菊酯(cycloprothrin)、氯氰菊酯(Cypermethrin)、溴氰菊酯(Deltamethrin)、高氰戊菊酯(esfenvalerate)、醚菊酯(ethofenprox)、甲氰菊酯(fenpropathrin)、杀灭菊酯(fenvalerate)、(RS)氯氟氰菊酯(cyhalothrin)、氯氟氰菊酯(lambda-cyhalothrin)、氯菊酯(permethrin)、灭虫硅醚(silafluofen)、氟胺氰菊酯(tau-fluvalinate)、七氟菊酯(tefluthrin)、四溴菊酯(tralomethrin)、甲体氯氰菊酯(alpha-cypermethrin)、己体氯氰菊酯(zeta-cypermethrin)、氯菊酯(permethrin);
新烟碱类(Neonicotinoids):吡虫清(Acetamiprid)、噻虫胺(Clothianidin)、呋虫胺(Dinotefuran)、氟啶虫酰胺(Flonicamid)、吡虫啉(Imidacloprid)、硝胺烯啶(Nitenpyram)、噻虫嗪(Thiamethoxam)、噻虫啉(Thiacloprid);
节肢动物生长调节剂:a)几丁质合成抑制剂:苯甲酰脲类:定虫隆(chlorfluazuron)、氟脲杀(diflubenzuron)、氟螨脲(flucycloxuron)、氟虫脲(flufenoxuron)、氟铃脲(hexaflumuron)、氟丙氧脲(lufenuron)、双苯氟脲(novaluron)、伏虫隆(teflubenzuron)、杀虫隆(triflumuron);噻嗪酮(buprofezin)、噁茂醚(diofenolan)、噻螨酮(hexythiazox)、特苯噁唑(etoxazole)、四螨嗪(clofentazine);b)蜕皮激素拮抗剂:特丁苯酰肼(halofenozide)、甲氧苯酰肼(methoxyfenozide)、双苯酰肼(tebufenozide);c)保幼激素类似物:蚊蝇醚(pyriproxyfen)、蒙五一五(methoprene)、双氧威(fenoxycarb);d)类脂生物合成抑制剂:螺螨酯(spirodiclofen);各种杀虫剂:齐墩螨素(abamectin)、灭螨醌(acequinocyl)、虫螨脒(amitraz)、艾扎丁(azadirachtin)、杀虫磺(bensultap)、联苯肼酯(bifenazate)、杀螟丹(cartap)、杀虫磺(bensultap)、氟唑虫清(chlorfenapyr)、杀虫脒(chlordimeform)、灭蝇胺(cyromazine)、杀螨硫隆(diafenthiuron)、噁茂醚(diofenolan)、甲氨基阿维菌素苯甲酸盐(emamectin benzoate)、硫丹(endosulfan)、ethiprole、喹螨醚(fenazaquin)、锐劲特(Fipronil)、伐虫脒(formetanate)、伐虫脒盐酸盐(formetanate hydrochloride)、林丹(gamma-HCH)、灭蚁腙(hydramethylnon)、噁二唑虫(indoxacarb)、异丙威(isoprocarb)、速灭威(metolcarb)、硝胺烯啶、哒螨酮(pyridaben)、拒嗪酮(pymetrozine)、艾克敌105(spinosad)、硫、吡螨胺(tebufenpyrad)、硫环杀(thiocyclam)、二甲威(XMC)、灭杀威(xylylcarb)、啶虫丙醚(Pyridalyl)、啶虫丙醚、氟啶虫酰胺、Fluacypyrim、米尔螨素(Milbemectin)、螺甲螨酯(Spiromesifen)、吡氟硫磷(Flupyrazofos)、NC 512、唑虫酰胺(Tolfenpyrad)、Flubendiamide、双三氟虫脲(Bistrifluron)、Benclothiaz、Pyrafluprole、Pyriprole、Amidoflumet、Flufenerim、Cyflumetofen、灭螨醌(Acequinocyl)、Lepimectin、Profluthrin、四氟甲醚菊酯(Dimefluthrin)、Amidrazone、Metaflumizone、N-乙基-2,2-二氯-1-甲基环丙烷甲酰胺-2-(2,6-二氯-α,α,α-三氟对甲苯基)腙、
下式的特窗酸:
下式的氨基异噻唑:
其中
R为-CH2OCH3或H,和
R’为-CF2CF2CF3、
下式的邻氨基苯甲酰胺:
下式的杀虫活性化合物:
优选选自高灭磷、毒死蜱、毒虫畏、马拉硫磷、丙硫克百威、噁虫威、虫螨威、丁硫克百威、呋线威、灭虫威、硫双威;氟氯菊酯、七氟菊酯、甲体氯氰菊酯、氯菊酯、吡虫清、噻虫胺、呋虫胺、Ethiprole、锐劲特、林丹、吡虫啉、艾克敌105、噻虫嗪和噻虫啉、杀螟丹、杀虫磺、硫环杀、硝胺烯啶、噻嗪酮、拒嗪酮、杀螟松、二嗪农、丁苯威、倍硫磷、氟啶虫酰胺;
更优选锐劲特、丙硫克百威、噁虫威、丁硫克百威、呋线威、氯菊酯、吡虫清、噻虫胺、呋虫胺、Ethiprole、Imidacroprid、艾克敌105、噻虫嗪、噻虫啉、甲氨基阿维菌素苯甲酸盐;
最优选锐劲特。
除草剂选自:
b1)类脂生物合成抑制剂,例如炔禾灵(chlorazifop)、炔草酯(clodinafop)、氯丁草(clofop)、氰氟草酯(cyhalofop)、氯甲草(diclofop)、噁唑禾草灵(fenoxaprop)、高噁唑禾草灵(fenoxaprop-p)、噻唑禾草灵(fenthiaprop)、吡氟禾草灵(fluazifop)、精吡氟禾草灵(fluazifop-P)、吡氟氯禾灵(haloxyfop)、精吡氟氯禾灵(haloxyfop-P)、恶草醚(isoxapyrifop)、噁唑酰草胺(metamifop)、喔草酯(propaquizafop)、喹禾灵(quizalofop)、精喹禾灵(quizalofop-P)、三氟苯氧丙酸(trifop)、枯杀达(alloxydim)、丁氧环酮(butroxydim)、烯草酮(clethodim)、环己烯草酮(cloproxydim)、噻草酮(cycloxydim)、环苯草酮(profoxydim)、稀禾定(sethoxydim)、醌肟草(tepraloxydim)、肟草酮(tralkoxydim)、苏达灭(butylate)、草灭特(cycloate)、燕麦敌(diauate)、哌草丹(dimepiperate)、扑草灭(EPTC)、禾草畏(esprocarb)、抑草威(ethiolate)、氮草(isopolinate)、甲硫苯威(methiobencarb)、草达灭(molinate)、坪草丹(orbencarb)、克草猛(pebulate)、苄草丹(prosulfocarb)、草克死(sulfallate)、杀草丹(thiobencarb)、丁草威(tiocarbazil)、野麦畏(triallate)、灭草猛(vernolate)、呋草黄(benfuresate)、乙呋草黄(ethofumesate)和地散磷(bensulide);
b2)ALS抑制剂,例如磺氨黄隆(amidosulfuron)、四唑黄隆(azimsulfuron)、苄嘧黄隆(bensulfuron)、氯嘧黄隆(chlorimuron)、绿黄隆(chlorsulfuron)、醚黄隆(cinosulfuron)、环丙黄隆(cyclosulfamuron)、胺苯黄隆(ethametsulfuron)、乙氧嘧黄隆(ethoxysulfuron)、啶嘧黄隆(flazasulfuron)、氟啶黄隆(flupyrsulfuron)、甲酰胺黄隆(foramsulfuron)、吡氯黄隆(halosulfuron)、啶咪黄隆(imazosulfuron)、碘黄隆(iodosulfuron)、甲基二黄隆(mesosulfuron)、甲黄隆(metsulfuron)、烟黄隆(nicosulfuron)、环丙氧黄隆(oxasulfuron)、氟嘧黄隆(primisulfuron)、氟丙黄隆(prosulfuron)、吡嘧黄隆(pyrazosulfuron)、玉嘧黄隆(rimsulfuron)、嘧黄隆(sulfometuron)、乙黄黄隆(sulfosulfuron)、噻黄隆(thifensulfuron)、醚苯黄隆(triasulfuron)、苯黄隆(tribenuron)、三氟啶黄隆(trifloxysulfuron)、氟胺黄隆(triflusulfuron)、三氟甲黄隆(tritosulfuron)、咪草酯(imazamethabenz)、咪草啶酸(imazamox)、甲基咪草烟(imazapic)、灭草烟(imazapyr)、灭草喹(imazaquin)、咪草烟(imazethapyr)、唑嘧磺胺盐(cloransulam)、唑嘧磺胺(diclosulam)、双氟磺草胺(florasulam)、氟唑啶草(flumetsulam)、metosulfam、五氟磺草胺(penoxsulam)、双嘧苯甲酸(bispyribac)、肟啶草(pyriminobac)、丙苯磺隆(propoxycarbazone)、氟酮黄隆(flucarbazone)、嘧苯草肟(pyribenzoxim)、环酯草醚(pyriftalid)和嘧硫苯甲酸(pyrithiobac);
b3)光合作用抑制剂,例如莠去通(atraton)、莠去津(atrazine)、莠灭净(ametryne)、叠氮津(aziprotryn)、草净津(cyanazine)、硫草净津(cyanatryn)、可乐津(chlorazine)、环草津(cyprazine)、敌草净(desmetryne)、戊草津(dimethametryne)、杀草净(dipropetryn)、草止津(eglinazine)、草怕津(ipazine)、麦苏百津(mesoprazine)、醚草通(methometon)、盖草津(methoprotryne)、环氰津(procyazine)、丙草止津(proglinazine)、扑灭通(prometon)、扑草净(prometryne)、扑灭津(propazine)、另丁津(sebuthylazine)、密草通(secbumeton)、西玛津(simazine)、西玛通(simeton)、西草净(simetryne)、甲氧去草净(terbumeton)、特丁津(terbuthylazine)、去草净(terbutryne)、草达津(trietazine)、特津酮(ametridione)、特草嗪酮(amibuzin)、六嗪同(hexazinone)、嗪丁草(isomethiozin)、苯嗪草(metamitron)、赛克津(metribuzin)、除草定(bromacil)、异草定(isocil)、环草定(lenacil)、特草定(terbacil)、溴杀草敏(brompyrazon)、杀草敏(chloridazon)、敌米达松(dimidazon)、异苯敌草(desmedipham)、敌克草(phenisopham)、苯敌草(phenmedipham)、乙苯敌草(phenmedipham-ethyl)、噻草隆(benzthiazuron)、丁噻隆(buthiuron)、噻二唑隆(ethidimuron)、异恶隆(isouron)、噻唑隆(methabenzthiazuron)、绿谷隆(monolinuron)、丁唑隆(tebuthiuron)、赛唑隆(thiazafluron)、疏草隆(anisuron)、播土隆(buturon)、氯溴隆(chlorbromuron)、乙氧苯隆(chloreturon)、绿麦隆(chlorotoluron)、枯草隆(chloroxuron)、枯莠隆(difenoxuron)、丁噁隆(dimefuron)、敌草隆(diuron)、非草隆(fenuron)、伏草隆(fluometuron)、氟苯隆(fluothiuron)、异丙隆(isoproturon)、利谷隆(linuron)、灭草恒(methiuron)、色满隆(metobenzuron)、秀谷隆(metobromuron)、甲氧隆(metoxuron)、绿谷隆(monolinuron)、灭草隆(monuron)、草不隆(neburon)、对伏隆(parafluron)、稀草隆(phenobenzuron)、环草隆(siduron)、氟氧隆(tetrafluron)、赛二唑素(thidiazuron)、莎草快(cyperquat)、二乙除草双(diethamquat)、苯敌快(difenzoquat)、敌草快阳离子(diquat)、伐草快(morfamquat)、对草快(paraquat)、糠草腈(bromobonil)、溴苯腈(bromoxynil)、羟敌草腈(chloroxynil)、碘草腈(iodobonil)、碘苯腈(ioxynil)、氨唑草酮(amicarbazone)、杀草全(bromofenoxim)、三氟噁嗪(flumezin)、灭草定(methazole)、噻草平(bentazone)、敌稗(propanil)、蔬草灭(pentanochlor)、达草止(pyridate)和6-氯-3-苯基-4-哒嗪醇(pyridafol);
b4)原卟啉原IX氧化酶抑制剂,例如氟锁草醚(aeifluorfen)、治草醚(bifenox)、氯硝醚(chlomethoxyfen)、草枯醚(chlornitrofen)、氯氟草醚(ethoxyfen)、消草醚(fluorodifen)、乙羧氟草醚(fluoroglycofen)、氯草醚(fluoronitrofen)、氟黄胺草醚(fomesafen)、氟呋草醚(furyloxyfen)、氟硝磺酰胺(halosafen)、乳氟禾草灵(lactofen)、除草醚(nitrofen)、硝氟草醚(nitrofluorfen)、氟硝草醚(oxyfluorfen)、异丙吡草酯(fluazolate)、氟唑草酯(pyraflufen)、吲哚酮草酯(cinidon-ethyl)、酰亚胺苯氧乙酸(flumiclorac)、氟噁嗪酮(flumioxazin)、炔草胺(flumipropyn)、达草氟(fluthiacet)、噻二唑胺(thidiazimin)、恶草灵(oxadiazon)、炔丙噁唑草(oxadiargyl)、唑啶炔草(azafenidin)、氟酮唑草(carfentrazone)、磺胺草唑(sulfentrazone)、戊噁唑草(pentoxazone)、双苯嘧草酮(benzfendizone)、氟丙嘧草酯(butafenacil)、双唑草腈(pyraclonil)、氟唑草胺(profluazol)、氟哒嗪草酯(flufenpyr)、flupropacil、吡氯草胺(nipyraclofen)和乙胺草醚(etnipromid);
b5)增白剂除草剂,例如氟哒草(metflurazon)、达草灭(norflurazon)、氟苯啶草(flufenican)、吡氟草胺(diflufenican)、氟吡酰草胺(picolinafen)、氟丁酰草胺(beflubutamid)、氟草同(fluridone)、氟咯草酮(flurochloridone)、呋草酮(flurtamone)、硝磺酮(mesotrione)、磺草酮(sulcotrione)、氯草酮(isoxachlortole)、异噁氟草(isoxaflutole)、吡草酮(benzofenap)、吡唑特(pyrazolynate)、苄草唑(pyrazoxyfen)、苯并双环酮(benzobicyclon)、杀草强(amitrole)、异恶草酮(clomazone)、苯草醚(aclonifen)、4-(3-三氟甲基苯氧基)-2-(4-三氟甲基苯基)嘧啶,以及式II的3-杂环基取代的苯甲酰衍生物(参见WO 96/26202、WO 97/41116、WO 97/41117和WO 97/41118):
其中变量R8至R13如下定义:
R8、R10为氢、卤素、C1-C6烷基、C1-C6卤代烷基、C1-C6烷氧基、C1-C6卤代烷氧基、C1-C6烷硫基、C1-C6烷基亚磺酰基或C1-C6烷基磺酰基;
R9为选自下列的杂环基:噻唑-2-基、噻唑-4-基、噻唑-5-基、异噁唑-3-基、异噁唑-4-基、异噁唑-5-基、4,5-二氢异噁唑-3-基、4,5-二氢异噁唑-4-基和4,5-二氢异噁唑-5-基,其中所述9个基团可以为未取代或被单取代或多取代,例如由卤素、C1-C4烷基、C1-C4烷氧基、C1-C4卤代烷基、C1-C4卤代烷氧基或C1-C4烷硫基单取代、二取代、三取代或四取代;
R11为氢、卤素或C1-C6烷基;
R12为C1-C6烷基;
R13为氢或C1-C6烷基;
b6)EPSP合成酶抑制剂如草甘膦(glyphosate);
b7)谷氨酰胺合成酶抑制剂如草铵膦(glufosinate)和双丙氨酰膦(bilanaphos);
b8)DHP合成酶抑制剂如黄草灵(asulam);
b9)有丝分裂抑制剂,例如氟草胺(benfluralin)、地乐胺(butralin)、敌乐胺(dinitramine)、丁氟消草(ethalfluralin)、氟消草(fluchloralin)、异乐灵(isopropalin)、氟烯硝草(methalpropalin)、磺乐灵(nitralin)、黄草消(oryzalin)、胺硝草(pendimethalin)、氨基丙氟灵(prodiamine)、卡乐施(profluralin)、氟乐灵(trifluralin)、甲基胺草磷(amiprofos-methyl)、草胺磷(butamifos)、氟硫草定(dithiopyr)、噻氟啶草(thiazopyr)、拿草特(propyzamide)、丙戊草胺(tebutam)、敌草索(chlorthal)、长杀草(carbetamide)、氯草灵(chlorbufam)、氯苯胺灵(chlorpropham)和苯胺灵(propham);
b10)VLCFA抑制剂,例如乙草胺(acetochlor)、甲草胺(alachlor)、丁草胺(butachlor)、丁烯草胺(butenachlor)、敌草乐(delachlor)、安塔(diethatyl)、克草胺(dimethachlor)、噻吩草胺(dimethenamid)、精噻吩草胺(dimethenamid-P)、吡草胺(metazachlor)、异丙甲草胺(metolachlor)、S-异丙甲草胺(S-metolachlor)、丙草胺(pretilachlor)、扑草胺(propachlor)、异丙草胺(propisochlor)、广草胺(prynachlor)、猛杀草(terbuchlor)、噻醚草胺(thenylchlor)、二甲苯草胺(xylachlor)、草毒死(allidochlor)、草立死(CDEA)、磺唑草(epronaz)、草乃敌(diphenamid)、草萘胺(napropamide)、萘丙胺(naproanilide)、烯草胺(pethoxamid)、氟噻草胺(flufenacet)、苯噻草胺(mefenacet)、四唑草胺(fentrazamide)、莎稗磷(anilofos)、哌草磷(piperophos)、唑草胺(cafenstrole)、茚草酮(indanofan)和灭草环(tridiphane);
b11)纤维素生物合成抑制剂,例如敌草腈(dichlobenil)、草克乐(chlorthiamid)、异恶草胺(isoxaben)和胺草唑(flupoxam);
b12)去偶(decoupler)除草剂,例如消草酯(dinofenate)、硝丙酚(dinoprop)、戊硝酚(dinosam)、地乐酚(dinoseb)、dinoterb(地乐消酚)、二硝甲酚(DNOC)、硝草酚(etinofen)和丁硝酚(medinoterb);
b13)植物生长素除草剂,例如稗草胺(clomeprop)、2,4-滴(2,4-D)、2,4,5-涕(2,4,5-T)、2甲4氯(MCPA)、酚硫杀(MCPA thioethyl)、2,4-滴丙酸(dichlorprop)、高2,4-滴丙酸(dichlorprop-P)、2甲4氯丙酸(mecoprop)、高2甲4氯丙酸盐(mecoprop-P)、2,4-滴丁酸(2,4-DB)、2甲4氯丁酸(MCPB)、草灭平(chloramben)、麦草畏(dicamba)、草芽平(2,3,6-TBA)、杀草畏(tricamba)、二氯喹啉酸(quinclorac)、喹草酸(quinmerac)、二氯皮考啉酸(clopyralid)、氟草烟(fluroxypyr)、毒莠定(picloram)、定草酯(triclopyr)和草除灵(benazolin);
b14)植物生长素输送抑制剂,例如抑草生(naptalam)、二氟吡隆(diflufenzopyr);
b15)新燕灵(benzoylprop)、氟燕灵(flamprop)、强氟燕灵(flamprop-M)、溴丁酰草胺(bromobutide)、氯甲丹(chlorflurenol)、环庚草醚(cinmethylin)、甲基杀草隆(methyldymron)、乙苯酰草(etobenzanid)、膦铵素(fosamine)、威百亩(metam)、稗草畏(pyributicarb)、氯噁嗪草(oxaziclomefone)、棉隆(dazomet)、苯氧丙胺津(triaziflam)和溴甲烷(methyl bromide)。
优选苏达灭、燕麦敌、甲硫苯威、草达灭、苄草丹、杀草丹、野麦畏、乙呋草黄、环丙黄隆、碘黄隆、甲基二黄隆、甲黄隆、氟丙黄隆、醚苯黄隆、咪草啶酸、甲基咪草烟、灭草烟、灭草喹、咪草烟、唑草磺胺(metosulam)、莠去津、莠灭净、草净津、特丁津、去草净、苯嗪草、赛克津、环草定、杀草敏、绿麦隆、丁噁隆、敌草隆、伏草隆、异丙隆、利谷隆、绿谷隆、草不隆、敌稗、磺胺草唑、吡氟草胺、氟吡酰草胺、氟咯草酮、呋草酮、硝磺酮、异噁氟草、异恶草酮、草甘膦、草铵膦、黄草灵、氟草胺、地乐胺、丁氟消草、胺硝草、氟乐灵、拿草特、长杀草、乙草胺、甲草胺、丁草胺、噻吩草胺、精噻吩草胺、吡草胺、异丙甲草胺、S-异丙甲草胺、丙草胺、扑草胺、草萘胺、氟噻草胺、苯噻草胺、灭草环、异恶草胺和胺草唑、麦草畏、二氯喹啉酸、喹草酸、毒莠定、环庚草醚、威百亩和棉隆。
安全剂选自:
解草酮(benoxacor)、喹氧乙酸(cloquintocet)、抑害腈(cyometrinil)、抑害胺(dichlormid)、dicyclonon、dietholate、解草唑(fenchlorazole)、解草啶(fenclorim)、解草安(flurazole)、肟草安(fluxofenim)、解草呋(furilazole)、isoxadifen、吡咯二酸(mefenpyr)、mephenate、萘二甲酸酐、2,2,5-三甲基-3-(二氯乙酰基)-1,3-噁唑烷(R-29148)、4-(二氯乙酰基)-1-氧杂-4-氮杂螺[4.5]癸烷(AD-67;MON 4660)和解草腈(oxabetrinil)。
此外,配制剂任选包含配制助剂,例如:
(a)表面活性剂如烷基苯磺酸盐、聚氧乙烯脂肪醇醚、木素磺酸盐、烷基萘磺酸盐、萘磺酸盐-甲醛缩合物、烷基萘磺酸盐-甲醛缩合物、苯酚磺酸/甲醛缩聚物的钠盐、聚氧乙烯烷基醚、聚氧乙烯烷基醚硫酸盐、聚氧乙烯烷基醚磷酸盐、聚氧乙烯烷基苯基醚、聚氧乙烯烷基苯基醚硫酸盐、聚氧乙烯烷基芳基醚硫酸盐、聚氧乙烯烷基芳基醚磷酸盐、聚氧乙烯烷基芳基苯基醚、聚氧乙烯苯乙烯基苯基醚硫酸盐、聚氧乙烯苯乙烯基苯基醚、聚氧乙烯烷基酯、聚乙二醇单甲醚、聚氧乙烯脱水山梨糖醇烷基化物、聚(聚氧乙烯苯乙烯基苯基醚)、聚亚氧烷基二醇、聚羧酸酯、苯酚磺酸盐、烷基磺酸盐、磺基琥珀酸二烷基酯、烷基醚硫酸盐、乙炔二醇(Acetylene glycols)及其混合物,其中优选聚氧乙烯苯乙烯基苯基醚硫酸盐和苯酚磺酸/甲醛缩聚物的钠盐的混合物;
(b)溶剂,例如水、芳族溶剂(如Solvesso产品、二甲苯)、石蜡(如矿物油馏分)、醇类(如甲醇、丁醇、戊醇、苄醇)、酮类(如环己酮、γ-丁内酯)、吡咯烷酮(NMP、NOP)、DMSO、乙酸酯(乙二醇二乙酸酯)、二醇、脂肪酸二甲基酰胺、脂肪酸及脂肪酸酯。原则上还可以使用溶剂混合物;优选的溶剂是水;
(c)载体(对于固体配制剂)/填料或媒介物(对于液体配制剂),例如磨碎的天然矿物(如高岭土、粘土、滑石、白垩)、磨碎的合成矿物(如高度分散的硅石、硅酸盐)或如上述(b)中所列的溶剂;
(d)增稠剂(或悬浮剂),例如羧甲基纤维素钠、甲基纤维素、乙基纤维素、聚乙烯醇、海藻酸钠、聚丙烯酸钠、黄原胶、文莱胶(Welan gum)、阿拉伯树胶、蒙脱土、木素磺酸盐、羟甲基纤维素、糊精、淀粉及其混合物;
(e)防冻剂,例如甘油、乙二醇、丙二醇,优选丙二醇;
(f)消泡剂,例如硅油、矿物油、脂肪酸酯;
(g)生物杀伤剂,例如苯甲酸钠、1,2-苯并异噻唑啉-3-酮、2-甲基-4-异噻唑啉-3-酮、5-氯-2-甲基-4-异噻唑啉-3-酮、山梨酸钾、对羟基苯甲酸盐。优选的生物杀伤剂为1,2-苯并异噻唑啉-3-酮和2-甲基-4-异噻唑啉-3-酮。
任选地,配制剂中也可以包括颜料。适合种子处理配制剂的颜料或染料为颜料蓝15:4、颜料蓝15:3、颜料蓝15:2、颜料蓝15:1、颜料蓝80、颜料黄1、颜料黄13、颜料红112、颜料红48:2、颜料红48:1、颜料红57:1、颜料红53:1、颜料橙43、颜料橙34、颜料橙5、颜料绿36、颜料绿7、颜料白6、颜料棕25、碱性紫10、碱性紫49、酸性红51、酸性红52、酸性红14、酸性蓝9、酸性黄23、碱性红10、碱性红108。
常规的种子处理配制剂例如包括可流动的浓缩物FS、溶液LS、干处理用粉末DS、淤浆处理用水分散性粉末WS、水溶性粉末SS以及乳液ES和EC。更优选以FS配制剂在播种之前施用于种子上,或者直接施用于种子上或者在催芽之后施用。
在种子处理配制剂中,粘着剂的量基于固体含量为0.1-15重量%,优选0.5-12重量%,最优选1.0-8重量%。
农药和配制助剂的量随着配制剂类型的变化而变化。对于相应的配制剂,熟练技术人员熟悉必需量的确定。
例如,用于种子处理如稻的FS配制剂通常包含:0.5-80%农药;0.5-20%表面活性剂(a);0.1-5%增稠剂(d);5-20%防冻剂(e);0.1-2%消泡剂(f);0%-75%填料/媒介物(c);和0.01-1%生物杀伤剂(g);以及0-20%颜料和/或染料。然后可以向该配制剂中加入如前所述的量的粘着剂。
相应配制剂的制备对本领域熟练技术人员是已知的(例如参见评论US3,060,084、EP-A 707 445(对于液体浓缩物),Browning,“Agglomeration”,Chemical Engineering,1967年12月4号,147-48,Perry’s ChemicalEngineer’s Handbook,第4版,McGraw-Hill,纽约,1963,第8-57页以及随后各页。WO 91/13546、US 4,172,714、US 4,144,050、US 3,920,442、US 5,180,587、US 5,232,701、US 5,208,030、GB 2,095,558、US 3,299,566,Klingman,Weed Control as a Science,John Wiley and Sons,Inc.,NewYork,1961,Hance等人,Weed Control Handbook,第8版,BlackwellScientific Publications,Oxford,1989和Mollet,H.,Grubemann,A.,Formulation technology,Wiley VCH Verlag GmbH,Weinheim(德国),2001,2.D.A.Knowles,Chemistry and Technology of AgrochemicalFormulations,Kluwer Academic Publishers,Dordrecht,1998(ISBN0-7514-0443-8)。
粘着剂可以在上面定义的溶剂中的乳液、分散体或溶液的形式使用。
在本发明一个实施方案中,种子处理配制剂可以基于粘着剂、农药和任选的配制助剂而制备。
在本发明另一实施方案中,配制剂可以在第一步中基于农药和任选的上述配制助剂而制备。或者,可以使用市售配制剂。在第二步中,将粘着剂加入所制备的包含至少一种农药和配制助剂的配制剂中,或加入市售配制剂中。该方法不仅适合固体配制剂(该固体配制剂在第一步中分散于水中,然后在其中加入粘着剂),也适合液体配制剂(该液体配制剂在第一步中分散/稀释于水中,然后在其中加入粘着剂)。
在另一实施方案中,将包含配制助剂和至少一种农药的配制剂(或市售配制剂)与粘着剂溶液一起或依次施用于种子。
所有上述种子处理配制剂的实施方案以下称为“本发明配制剂”。
本发明配制剂可用于处理如选自下列的作物种子:大田作物种子如玉米(甜玉米和野玉米)、硬粒小麦、大豆、小麦、大麦、燕麦、黑麦、黑小麦、稻、棉花、向日葵、土豆、牧草、苜蓿、草、草坪、高粱、油菜籽、芸苔属和甜菜,蔬菜作物种子如西红柿、莴苣、卷心莴苣、胡椒、黄瓜、南瓜、甜瓜、豆、豌豆、韭菜、大蒜、洋葱、甘蓝、胡萝卜,块茎如甘蔗,特殊作物种子如烟草,以及观赏植物种子如三色堇、凤仙花属植物、矮牵牛和老鹳草,优选可在种子萌发过程中用种子处理配制剂处理的种子,例如蔬菜作物种子,特殊作物种子如烟草以及观赏植物种子;甜菜、玉米和稻;最优选稻。
本发明进一步包括用本发明配制剂处理的种子,其中种子优选选自大田作物种子如玉米(甜玉米和野玉米)、硬粒小麦、大豆、小麦、大麦、燕麦、黑麦、黑小麦、稻、棉花、向日葵、土豆、牧草、苜蓿、草、草坪、高粱、油菜籽、芸苔属和甜菜,蔬菜作物种子如西红柿、莴苣、卷心莴苣、胡椒、黄瓜、南瓜、甜瓜、豆、豌豆、韭菜、大蒜、洋葱、甘蓝、胡萝卜,块茎如甘蔗,特殊作物种子如烟草,以及观赏植物种子如三色堇、凤仙花属植物、矮牵牛和老鹳草,优选可在种子萌发过程中用种子处理配制剂处理的种子,例如蔬菜作物种子,特殊作物种子如烟草以及观赏植物种子,甜菜,玉米和稻;最优选稻。
种子可以是去壳的、未去壳的或部分去壳的,优选去壳的。
本发明还包括用本发明配制剂处理的种子。
本发明进一步包括一种用本发明配制剂在播种前处理种子的方法,包括下列步骤:
a)将本发明配制剂施用于溶剂中;和
b)将在步骤a)中得到的混合物施用于种子。
在优选实施方案中,溶剂为水。如上所述,也可将配制剂(如市售配制剂)和粘着剂分别施用于种子,这是指将任选在溶剂如水中稀释的配制剂和粘着剂一起或依次施用于种子。
在本发明另一优选实施方案中,种子可用本发明配制剂和/或不含粘着剂的配制剂(如包含一种、两种或更多种农药的市售配制剂)处理。
例如,可将种子如下处理:
a)用不含粘着剂的配制剂处理,由此产生含有不含粘着剂的配制剂的第一层;然后用本发明配制剂处理,由此产生含有粘着剂的第二层;或
b)首先用本发明配制剂处理种子,由此产生含粘着剂的第一层;然后用配制剂(如包含一种、两种或更多种农药的市售配制剂)处理,由此产生含有不含粘着剂的配制剂的第二层;或
c)数层本发明配制剂,其中
(1)将包含一种、两种或更多种农药的第一种本发明配制剂施用于种子,由此产生含有配制剂的第一层;然后
(2)将包含一种、两种或更多种农药的第二种本发明配制剂施用于种子,其中该配制剂在农药方面不同于第一种配制剂(步骤1),由此产生含有第二种配制剂的第二层(步骤2);
任选地,可以施用第三种配制剂,所述第三种配制剂不同于上述涂覆的种子(a)、(b)或(c)的步骤(1)和(2)的第一和第二种配制剂,产生第三层。
在优选实施方案中,用本发明配制剂处理种子的方法主要有四种,即浸没或浸渍、涂覆、种子干处理和种子喷雾处理(例如参见评论Japan PlantProtection Association(第133-139页“Pesticide Application Technology”,1998;ASGROW Reports:Seed treatments:Trends and Opportunities,2002):
1.浸没最常用于稻种。根据该方法,清洁种子并装入袋中,然后将其浸入与种子体积相当的化学溶液中,其中化学溶液通常通过稀释配制剂如FS、LS、DS、WS、SS和ES而得到。然后将种子干燥。
2.涂覆最常用于稻、蔬菜、土豆、球根。根据该方法,将种子清洁,然后用稀释的配制剂(如在水中的0.5%WP配制剂)通过使用旋转罐式混合器涂覆约3分钟,然后可逆旋转。然后将种子干燥。
3.对于种子干处理,将略微稀释的配制剂在混合器中用水稀释(如在混合器中一起加入WP和2%的水),然后加入种子、培育。
4.种子喷雾处理是一种通常用于处理大量稻种的方法。为此将通过稀释配制剂(如FS、LS、DS、WS、SS和ES)而得到的溶液在自动测量并从进料斗中进料的喷雾室中连续喷雾于种子上,然后在干燥室中在升高温度下(如40℃)干燥。
在本发明特别优选的实施方案中,可将种子在种子萌发过程中用本发明配制剂处理(参见评论:ASGROW Reports:Seed treatments:Trends andOpportunities,2002;Khan等人:International Journal of AgriculturalBotany,2003;SeedQuest@seedquest.com.)。这种方法通常包括下列步骤:
-使种子在受控条件下吸水(hydrate),然后使种子在受控条件下发芽;
-用本发明配制剂处理种子;
其中取决于相应方法,可首先使种子吸水,在第二步中用本发明配制剂处理种子,或者,可首先用本发明配制剂处理种子,然后使种子吸水。对于稻种处理,优选首先用本发明配制剂处理种子,然后使种子吸水。
可用本发明配制如上所述处理种子。
种子萌发过程或“预播种吸水处理”是一种改进种子发芽特性的种子改进方法。萌发通过使种子部分吸水并在所限定的湿度、温度和通风条件下保持规定的时间而实现。对于该过程,将种子用精确控制的条件处理,使大多数发芽的活动发生,但防止种子真正发芽。该过程包括使用通常的自然条件,控制这些条件从而操纵种子中的活动。种子萌发通常可如下进行:
(1)湿润,
(2)吸水萌发,
(3)渗透萌发,
(4)交替吸水-脱水。
在这种情况下,使种子吸水并调至所需代谢活动。这触发了重要的预发芽生理步骤,例如膜修复、DNA和RNA合成和修复、不成熟胚的发育、胚覆盖组织的变更、休眠块的破坏或移除以及一般预发芽新陈代谢的改进。在萌发过程结束时,将种子再干燥至其储存的湿度水平以促进良好的储存。据了解,一旦建立真正发芽的框架并将种子干燥至稳定的湿度水平,在田地中种植种子将通过与土壤或栽培介质中的水分接触而激活最后的发芽过程。
在萌发中得到的并没有在随后的种子再干燥中失去。在萌发过程之后,因为如下原因使种子在生理上更接近于发芽(参见评论ASGROWReports:Seed treatments:Trends and Opportunities,2002;Khan等人:International Journal of Agricultural Botany,2003):
(1)缩短了在田地中的发芽时间,
(2)克服了休眠影响,
(3)在较恶劣的田地条件下,引入了良好的发芽,
(4)更快的田地出苗,
(5)更快的作物生长,
(6)种子消毒。
术语“预播种吸水处理”或萌发包括:
a)非受控(如浸渍法,其中水可自由得到且不受环境限制)水吸收,和
b)受控水吸收(如调节种子水分含量,防止发芽完成的方法)。
两种技术可用于非受控性水吸收:
(1)用溶液萌发或浸渍;和/或
(2)用固体颗粒体系萌发或浸渍。
三种技术可用于受控性水吸收(参见评论ASGROW Reports:Seedtreatments:Trends and Opportunities,2002;Khan等人:InternationalJournal of Agricultural Botany,2003;Seed Quest@seedquest.com):
(1)用溶液萌发;
(2)用固体颗粒体系萌发;和/或
(3)通过受控的吸水萌发。
在特别优选的实施方案中,将用本发明配制剂处理的种子用于稻的非受控性种子萌发或浸渍过程(N.Slaton和R Cartwright:Water-Seeded Rice.in:Rice Production Handbook,University of Arkansas Publication,Arkansas,美国)。
在种子萌发过程中,尤其在用本发明配制剂处理的稻种的非受控性种子萌发过程中,可获得高达120天的延长的对抗植物病原性真菌和昆虫的种子保护,这优于育苗箱处理。
本发明进一步包括一种防治不希望的植物生长和/或抵抗植物病原性昆虫和/或植物病原性真菌的方法,包括将本发明配制剂在播种前施用于种子。优选地,本发明进一步包括一种抵抗土壤昆虫和/或真菌的方法,包括将本发明配制剂在播种前施用于种子。种子可用本发明配制剂如上所述处理。
术语植物病原性真菌包括,但并不局限于:
蔬菜、水果和稻上的链格孢(Alternaria)属,
禾谷类、稻和草坪中的平脐蠕孢(Bipolaris)属和内脐蠕孢(Drechslera)属,
禾谷类中的禾白粉菌(Blumeria graminis)(白粉病),
草莓、蔬菜、观赏植物和葡萄藤上的灰葡萄孢(Botrytis cinerea)(灰霉病),
葫芦科植物上的二孢白粉菌(Erysiphe cichoracearum)和单丝壳(Sphaerotheca fuliginea),
各种植物上的镰孢霉(Fusarium)属和轮枝孢(Verticillium)属,
禾谷类、香蕉和花生上的球腔菌(Mycosphaerella)属,
大豆上的Phakopsara pachyrhizi和Phakopsara meibomiae,
土豆和西红柿上的致病疫霉(Phytophthora infestans),
葡萄藤上的葡萄生单轴霉(Plasmopara viticola),
苹果上的苹果白粉病菌(Podosphaera leucotricha),
小麦和大麦上的小麦基腐病菌(Pseudocercosporella herpotrichoides),
啤酒花和黄瓜上的假霜霉(Pseudoperonospora)属,
禾谷类上的柄锈菌(Puccinia)属,
稻上的稻瘟病菌(Pyricularia oryzae)、宫部旋孢腔菌(Cochliobolusmiyabeanus)和笹木伏革菌(Corticium sasaki)(立枯丝核菌(Rhizoctoniasolani))、半裸镰孢(Fusarium semitectum)(和/或串珠镰孢(moniliforme))、蠕虫(Helminth.)属、稻尾孢(Cercospora oryzae)、宫部旋孢腔菌、稻帚梗柱孢(Sarocladium oryzae)、长管帚梗柱孢(S attenuatum)、稻叶黑粉菌(Entyloma oryzae)、稻恶苗病菌(Gibberella fujikuroi)(恶苗病(bakanae))、革兰氏染色配合物(Grainstaining complex)(各种病原体)和/或腐霉属(Pythium),
棉花、稻和草坪上的丝核菌(Rhizoctonia)属,
小麦上的小麦壳针孢(Septoria tritici)和颖枯壳多孢(Stagonosporanodorum),
葡萄藤上的葡萄钩丝壳(Uncinula necator),
禾谷类和甘蔗上的黑粉菌(Ustilago)属,以及
苹果和梨上的黑星菌(Venturia)属(黑星病);
优选下列属:
稻上的链格孢属、稻瘟病菌、宫部旋孢腔菌和笹木伏革菌(立枯丝核菌)、半裸镰孢(和/或串珠镰孢)、蠕虫(Helminth.)属、稻尾孢、宫部旋孢腔菌、稻帚梗柱孢、长管帚梗柱孢、稻叶黑粉菌、稻恶苗病菌(恶苗病)、革兰氏染色配合物(各种病原体)和/或腐霉属。
术语病原性昆虫包括,但并不局限于此:
来自鳞翅目的昆虫(鳞翅目(Lepidoptera)),例如小地老虎(Agrotisypsilon)、黄地老虎(Agrotis segetum)、木棉虫(Alabama argillacea)、黎豆夜蛾(Anticarsia gemmatalis)、Argyresthia conjugella、叉纹夜蛾(Autographa gamma)、树尺蠖(Bupalus piniarius)、Cacoecia murinana、Capua reticulana、Cheimatobia brumata、云杉色卷蛾(Choristoneurafumiferana)、Choristoneura occidentalis、二化螟(Cirphis unipuncta)、苹果小卷蛾(Cydia pomonella)、松毛虫(Dendrolimus pini)、Diaphanianitidalis、西南玉米杆草螟(Diatraea grandiosella)、埃及钻夜蛾(Eariasinsulana)、南美玉米苗斑螟(Elasmopalpus lignosellus)、女贞细卷蛾(Eupoecilia ambiguella)、Evetria bouliana、Feltia subterranea、蜡螟(Galleria mellonella)、李小食心虫(Grapholitha funebrana)、梨小食心虫(Grapholitha molesta)、棉铃虫(Heliothis armigera)、烟芽夜蛾(Heliothisvirescens)、玉米穗虫(Heliothis zea)、菜螟(Hellula undalis)、Hiberniadefoliaria、美国白蛾(Hyphantria cunea)、苹果巢蛾(Hyponomeutamalinellus)、番茄虫蛾(Keiferia lycopersicella)、Lambdina fiscellaria、甜菜夜蛾(Laphygma exigua)、咖啡潜叶蛾(Leucoptera coffeella)、旋纹潜蛾(Leucoptera scitella)、Lithocolletis blancardella、葡萄浆果小卷蛾(Lobesiabotrana)、甜菜网螟(Loxostege sticticalis)、舞毒蛾(Lymantria dispar)、模毒蛾(Lymantria monacha)、桃潜蛾(Lyonetia clerkella)、黄褐天幕毛虫(Malacosoma neustria)、甘蓝夜蛾(Mamestra brassicae)、黄杉毒蛾(Orgyiapseudotsugata)、玉米螟(Ostrinia nubilalis)、小眼夜蛾(Panolis flammea)、棉花红铃虫(Pectinophora gossypiella)、疆夜蛾(Peridroma saucia)、圆掌舟蛾(Phalera bucephala)、马铃薯麦蛾(Phthorimaea operculella)、柑桔潜叶蛾(Phyllocnistis citrella)、欧洲粉蝶(Pieris brassicae)、苜蓿绿夜蛾(Plathypena scabra)、菜蛾(Plutella xylostella)、大豆夜蛾(Pseudoplusiaincludens)、Rhyacionia frustrana、Scrobipalpula absoluta、麦蛾(Sitotrogacerealella)、葡萄卷叶蛾(Sparganothis pilleriana)、草地夜蛾(Spodopterafrugiperda)、海灰翅夜蛾(Spodoptera littoralis)、斜纹夜蛾(Spodopteralitura)、Thaumatopoea pityocampa、绿色橡木飞蛾(Tortrix viridana)、粉纹夜蛾(Trichoplusia ni)和Zeiraphera canadensis;
甲虫(鞘翅目(Coleoptera)),例如梨窄吉丁(Agrilus sinuatus)、直条叩头虫(Agriotes lineatus)、暗色叩头虫(Agriotes obscurus)、Amphimallussolstitialis、Anisandrus dispar、墨西哥棉铃象(Anthonomus grandis)、苹花象(Anthonomus pomorum)、甜菜隐食甲(Atomaria linearis)、纵坑切梢小蠹(Blastophagus piniperda)、Blitophaga undata、蚕豆象(Bruchusrufimanus)、豌豆象(Bruchus pisorum)、欧洲兵豆象(Bruchus lentis)、苹卷象(Byctiscus betulae)、甜菜大龟甲(Cassida nebulosa)、Cerotomatrifurcata、白菜籽龟象(Ceuthorrhynchus assimilis)、芫菁龟象(Ceuthorrhynchus napi)、甜菜胫跳甲(Chaetocnema tibialis)、Conoderusvespertinus、石刁柏负泥虫(Crioceris asparagi)、Diabrotica longicornis、Diabrotica 12-punctata、玉米根叶甲(Diabrotica virgifera)、墨西哥豆瓢虫(Epilachna varivestis)、烟草跳甲(Epitrix hirtipennis)、棉灰蒙象变种(Eutinobothrus brasiliensis)、欧洲松树皮象(Hylobius abietis)、埃及苜蓿叶象(Hypera brunneipennis)、紫苜蓿叶象(Hypera postica)、云杉八齿小蠹(Ipstypographus)、烟草负泥虫(Lema bilineata)、黑角负泥虫(Lemamelanopus)、马铃薯叶甲(Leptinotarsa decemlineata)、Limoniuscalifornicus、稻水象甲(Lissorhoptrus oryzophilus)、Melanotus communis、油菜露尾甲(Meligethes aeneus)、大栗鳃金龟(Melolontha hippocastani)、五月鳃金龟(Melolontha melolontha)、水稻负泥虫(Oulema oryzae)、葡萄黑耳喙象(Ortiorrhynchus sulcatus)、草莓根象甲(Otiorrhynchus ovatus)、辣根猿叶甲(Phaedon cochleariae)、Phyllotreta chrysocephala、食叶鳃金龟属(Phyllophaga sp.)、庭园发丽金龟(Phyllopertha horticola)、大豆淡足跳甲(Phyllotreta nemorum)、黄曲条菜跳甲(Phyllotreta striolata)、日本金龟子(Popillia japonica)、豌豆叶象(Sitona lineatus)和谷象(Sitophilusgranaria);
双翅目昆虫(双翅目(Diptera)),例如埃及伊蚊(Aedes aegypti)、剌扰伊蚊(Aedes vexans)、墨西哥果蝇(Anastrepha ludens)、五斑按蚊(Anophelesmaculipennis)、地中海实蝇(Ceratitis capitata)、蛆症金蝇(Chrysomyabezziana)、Chrysomya hominivorax、Chrysomya macellaria、高粱瘿蚊(Contarinia sorghicola)、Cordylobia anthropophaga、尖音库蚊(Culexpipiens)、瓜蝇(Dacus cucurbitae)、油橄榄实蝇(Dacus oleae)、油菜叶瘿蚊(Dasineura brassicae)、小毛厕蝇(Fannia canicularis)、马蝇(Gasterophilusintestinalis)、刺舌蝇(Glossina morsitans)、Haematobia irritans、Haplodiplosis equestris、花生田灰地种蝇(Hylemyia platura)、纹皮蝇(Hypoderma lineata)、蔬菜斑潜蝇(Liriomyza sativae)、美国潜叶蝇(Liriomyza trifolii)、Lucilia caprina、铜绿蝇(Lucilia cuprina)、丝光绿蝇(Lucilia sericata)、Lycoria pectoralis、麦瘿蚊(Mayetiola destructor)、家蝇(Musca domestica)、厩腐蝇(Muscina stabulans)、羊狂蝇(Oestrus ovis)、欧洲麦秆蝇(Oscinella frit)、天仙子泉蝇(Pegomya hysocyami)、Phorbiaantiqua、萝卜蝇(Phorbia brassicae)、Phorbia coarctata、樱桃实蝇(Rhagoletis cerasi)、苹果实蝇(Rhagoletis pomonella)、Tabanus bovinus、Tipula oleracea和欧洲大蚊(Tipula paludosa);
蓟马(缨翅目(Thysanoptera)),例如烟褐蓟马(Frankliniella fusca)、苜蓿花蓟马(Frankliniella occidentalis)、东方花蓟马(Frankliniella tritici)、桔硬蓟马(Scirtothrips citri)、稻蓟马(Thrips oryzae)、棕榈蓟马(Thrips palmi)和烟蓟马(Thrips tabaci);
膜翅目昆虫(膜翅目(Hymenoptera)),例如新疆菜叶蜂(Athalia rosae)、切叶蚁(Atta cephalotes)、Atta sexdens、Atta texana、Hoplocampa minuta、Hoplocampa testudinea、小黄家蚁(Monomorium pharaonis)、热带火蚁(Solenopsis geminate)和红火蚁(Solenopsis invicta);
异翅目昆虫(异翅目(Heteroptera)),例如拟绿蝽(Acrosternum hilare)、玉米长蝽(Blissus leucopterus)、黑斑烟盲蝽(Cyrtopeltis notatus)、棉红蝽(Dysdercus cingulatus)、Dysdercus intermedius、麦扁盾蝽(Eurygasterintegriceps)、Euschistus impictiventris、棉红铃喙缘蝽(Leptoglossusphyllopus)、美洲牧草盲蝽(Lygus lineolaris)、牧草盲蝽(Lygus pratensis)、稻绿蝽(Nezara viridula)、甜菜拟网蝽(Piesma quadrata)、Solubea insularis和Thyanta perditor;
同翅目昆虫(同翅目(Homoptera)),例如Acyrthosiphon onobrychis、落叶松球蚜(Adelges laricis)、Aphidula nasturtii、甜菜蚜(Aphis fabae)、草莓根蚜(Aphis forbesi)、苹果蚜(Aphis pomi)、棉蚜(Aphis gossypii)、北美茶簏子蚜(Aphis grossulariae)、Aphis schneideri、卷叶蚜(Aphis spiraecola)、Aphis sambuci、豌豆蚜(Acyrthosiphon pisum)、马铃薯蚜(Aulacorthumsolani)、Brachycaudus cardui、杏圆尾蚜(Brachycaudus helichrysi)、Brachycaudus persicae、Brachycaudus prunicola、甘蓝蚜(Brevicorynebrassicae)、Capitophorus horni、Cerosipha gossypii、Chaetosiphonfragaefolii、Cryptomyzus ribis、高加索冷杉椎球蚜(Dreyfusianordmannianae)、云杉椎球蚜(Dreyfusia piceae)、居根西圆尾蚜(Dysaphisradicola)、Dysaulacorthum pseudosolani、Dysaphis plantaginea、Dysaphispyri、蚕豆微叶蝉(Empoasea fabae)、桃大尾蚜(Hyalopterus pruni)、Hyperomyzus lactucae、麦长管蚜(Macrosiphum avenae)、大戟长管蚜(Macrosiphum euphorbiae)、蔷薇管蚜(Macrosiphon rosae)、Megouraviciae、巢莱修尾蚜(Melanaphis pyrarius)、麦无网蚜(Metopolophiumdirhodum)、Myzodes persicae、冬葱瘤额蚜(Myzus ascalonicus)、Myzuscerasi、李瘤蚜(Myzus varians)、Nasonovia ribis-nigri、稻飞虱(Nilaparvatalugens)、囊柄瘿绵蚜(Pemphigus bursarius)、蔗飞虱(Perkinsiellasaccharicida)、忽布疣蚜(Phorodon humuli)、苹木虱(Psylla mali)、梨木虱(Psylla piri)、冬葱瘤蛾蚜(Rhopalomyzus ascalonicus)、玉米蚜(Rhopalosiphum maidis)、禾谷溢管蚜(Rhopalosiphum padi)、Rhopalosiphum insertum、Sappaphis mala、Sappaphis mali、麦二叉蚜(Schizaphis graminum)、schizoneura lanuginosa、麦长管蚜(Sitobionavenae)、白粉虱(Trialeurodes vaporariorum)、Toxoptera aurantiiand和葡萄根瘤蚜(Viteus vitifolii);
白蚁(等翅目(Isoptera)),例如Calotermes flavicollis、Leucotermesflavipes、欧洲散白蚁(Reticulitermes lucifugus)和Termes natalensis;
直翅目昆虫(直翅目(Orthoptera)),例如居屋艾蟋(Acheta domestica)、东方蜚蠊(Blatta orientalis)、德国小蠊(Blattella germanica)、欧洲球螋(Forficula auricularia)、蝼蛄(Gryllotalpa gryllotalpa)、飞蝗(Locustamigratoria)、双纹黑蝗(Melanoplus bivittatus)、红足黑蝗(Melanoplusfemur-rubrum)、墨西哥黑蝗(Melanoplus mexicanus)、迁飞黑蝗(Melanoplus sanguinipes)、石栖黑蝗(Melanoplus spretus)、条纹红蝗(Nomadacris septemfasciata)、美洲蟑螂(Periplaneta americana)、美洲沙漠蝗(Schistocerca americana)、Schistocerca peregrina、Stauronotusmaroccanus和庭疾灶螽(Tachycines asynamorus),
蛛形纲(Arachnoidea),如蜘蛛(蜱螨目(acarina)),例如软蜱科(Argasidae)、硬蜱科(Ixodidae)和疥螨科(Sarcoptidae),如长星形壁虱(Amblyomma americanum)、热带花蜱(Amblyomma variegatum)、波斯锐缘蜱(Argas persicus)、牛壁虱(Boophilus annulatus)、Boophilusdecoloratus、微小牛蜱(Boophilus microplus)、Dermacentor silvarum、Hyalomma truncatum、蓖子硬蜱(Ixodes ricinus)、Ixodes rubicundus、Ornithodorus moubata、Otobius megnini、鸡皮刺螨(Dermanyssusgallinae)、绵羊疥病(Psoroptes ovis)、Rhipicephalus appendiculatus、Rhipicephalus evertsi、人疥螨(Sarcoptes scabiei),瘿螨属(Eriophyidaespp.),如苹果刺锈螨(Aculus schlechtendali)、Phyllocoptrata oleivora和Eriophyes sheldoni;细螨属(Tarsonemidae spp.),如Phytonemus pallidus和侧多食跗线螨(Polyphagotarsonemus latus);细须螨属(Tenuipalpidaespp.),如紫红短须螨(Brevipalpus phoenicis);叶螨属(Tetranychidae spp.),如朱砂叶螨(Tetranychus cinnabarinus)、神泽叶螨(Tetranychus kanzawai)、太平洋叶螨(Tetranychus pacificus)、棉叶螨(Tetranychus telarius)和二点叶螨(Tetranychus urticae),苹果叶螨(Panonychus ulmi)、柑椐叶螨(Panonychus citri)和oligonychus pratensis;
线虫,尤其是植物寄生线虫如根结线虫,北方根结线虫(Meloidogynehapla)、南方根结线虫(Meloidogyne incognita)、爪哇根结线虫(Meloidogynejavanica)和其它根结线虫属(Meloidogyne);形成胞囊的线虫,马铃薯金线虫(Globodera rostochiensis)和其它球胞囊(Globodera)属;禾谷胞囊线虫(Heterodera avenae)、大豆胞囊线虫(Heterodera glycines)、甜菜胞囊线虫(Heterodera schachtii)、三叶草胞囊线虫(Heterodera trifolii)和其它胞囊线虫(Heterodera)属;种子肿瘿线虫,粒线虫(Anguina)属;茎叶线虫,滑刃线虫(Aphelenchoides)属;刺线虫,杂草刺线虫(Belonolaimus longicaudatus)和其它针刺线虫属(Belonolaimus);松线虫,松材线虫(Bursaphelenchusxylophilus)和其它伞滑刃线虫属(Bursaphelenchus);环形线虫,环纹线虫属(Criconema)、小环线虫属(Criconemella)、轮线虫属(Criconemoides)、中环线虫属(Mesocriconema);球茎线虫,腐烂茎线虫(Ditylenchusdestructor)、甘薯茎线虫(Ditylenchus dipsaci)和其它茎线虫属(Ditylenchus);锥线虫,锥线虫属(Dolichodorus);螺旋形线虫,Heliocotylenchus multicinctus和其它Helicotylenchus属;鞘线虫和鞘形(sheathoid)线虫,鞘线虫属(Hemicycliophora)和Hemicriconemoides属;Hirshmanniella属;冠线虫,Hoploaimus属;伪根结线虫,珍珠线虫属(Nacobbus);针线虫,Longidorus elongatus和其它长针线虫属(Longidorus);根腐线虫,Pratylenchus neglectus、穿刺根腐线虫(Pratylenchus penetrans)、Pratylenchus curvitatus、Pratylenchus goodeyi和其它根腐线虫属(Pratylenchus);穿孔线虫,香蕉穿孔线虫(Radopholussimilis)和其它穿孔线虫属(Radopholus);肾形线虫,Rotylenchus robustus和其它盘旋线虫属(Rotylenchus);Scutellonema属;残根线虫,Trichodorusprimitivus和其它毛刺线虫属(Trichodorus)、拟毛刺属(Paratrichodorus);阻长线虫,Tylenchorhynchus claytoni、Tylenchorhynchus dubius和其它矮化线虫属(Tylenchorhynchus);柑桔线虫,垫刃线虫属(Tylenchulus);剑线虫,剑线虫属(Xiphinema);以及其它植物寄生线虫;
以及稻病原体,例如稻水象(rice water weevil)(Lissorhoptrusoryzaphilus)、水稻二化螟(rice stem borer)(Chilo suppresalis)、稻纵卷叶螟(rice leaf roller)、稻负泥虫(rice leaf beetle)、稻秆蝇(rice leafminer)(Agromyca oryzae)、叶蝉(浮尘子属(Nephotettix spp.);尤其是小型褐叶蝉、稻绿叶蝉)、飞虱(飞虱科;尤其是白背飞虱(white backedplanthopper)、水稻褐飞虱(brown rice planthopper))、臭蝽;
优选稻病原体,例如稻水象、水稻二化螟、稻纵卷叶螟、稻负泥虫、稻秆蝇(Agromyca oryzae)、叶蝉(浮尘子属;尤其是小型褐叶蝉、稻绿叶蝉)、飞虱(飞虱科;尤其是白背飞虱、水稻褐飞虱)、臭蝽。
防治不希望的植物生长的含义是指破坏杂草。杂草在最广意义上的含义是指所有生长在不希望它们生长的地方的那些植物,例如:
下列属的双子叶杂草:白芥属(Sinapis)、独行菜属(Lepidium)、猪殃殃属(Galium)、繁缕属(Stellaria)、母菊属(Matricaria)、春黄菊属(Anthemis)、牛滕菊属(Galinsoga)、藜属(Chenopodium)、荨麻属(Urtica)、千里光属(Senecio)、苋属(Amaranthus)、马齿苋属(Portulaca)、苍耳属(Xanthium)、旋花属(Convolvulus)、番薯属(Ipomoea)、蓼属(Polygonum)、田菁属(Sesbania)、豚草属(Ambrosia)、蓟属(Cirsium)、飞廉属(Carduus)、苦苣菜属(Sonchus)、茄属(Solanum)、蔊菜属(Rorippa)、节节菜属(Rotala)、母草属(Lindernia)、野芝麻属(Lamium)、婆婆纳属(Veronica)、苘麻属(Abutilon)、Emex、曼陀罗属(Datura)、堇菜属(Viola)、鼬瓣花属(Galeopsis)、罂粟属(Papaver)、矢车菊属(Centaurea)、车轴草属(Trifolium)、毛茛属(Ranunculus)、蒲公英属(Taraxacum)。
下列属的单子叶杂草:稗属(Echinochloa)、狗尾草属(Setaria)、黍属(Panicum)、马唐属(Digitaria)、梯牧草属(Phleum)、早熟禾属(Poa)、羊茅属(Festuca)、椮属(Eleusine)、臂形草属(Brachiaria)、黑麦草属(Lolium)、雀麦属(Bromus)、燕麦属(Avena)、莎草属(Cyperus)、高粱属(Sorghum)、冰草属(Agropyron)、狗牙根属(Cynodon)、雨久花属(Monochoria)、飘拂草属(Fimbristyslis)、慈菇属(Sagittaria)、荸荠属(Eleocharis)、藨草属(Scirpus)、雀稗属(Paspalum)、鸭嘴草属(Ischaemum)、尖瓣花属(Sphenoclea)、龙爪茅属(Dactyloctenium)、剪股颖属(Agrostis)、看麦娘属(Alopecurus)、阿披拉草属(Apera)。
处理种子的农药用量为0.1g-10kg农药/100kg种子,希望1g-5kg农药/100kg种子,更希望1g-2.5kg农药/100kg种子。
下列实施例更详细阐述本发明。
实施例
实施例1
粘着剂的商品名汇集于表1。
表1
粘着剂/水乳液的商品名 | 供应商 | 含量(重量%) | 化学名 |
AcronalYJ2810Dap | BASF | 50 | 具有丙烯酰基、丙烯酸烷基酯、甲基丙烯酸烷基酯的共聚物 |
Polysol OLZ1094 | ShowaHighpolymer | 50 | 丙烯酸烷基酯共聚物 |
Lawnfix 700 | ShowaHighpolymer | 50 | 乙烯/乙酸乙烯酯共聚物 |
Polysol AG-100 | ShowaHighpolymer | 50 | 丙烯酸烷基酯共聚物 |
粘着剂/水乳液的商品名 | 供应商 | 含量(重量%) | 化学名 |
Polysol AT-860 | ShowaHighpolymer | 50 | 丙烯酸烷基酯共聚物 |
A)制备FS配制剂
表2配制剂
编号 | FS配制剂 | 成分 |
1 | 肟醚菌胺FS配制剂(500g肟醚菌胺/L) | FS配制剂包含肟醚菌胺作为农药,苯酚磺酸、尿素和甲醛的缩合物以及POE苯乙烯基苯基醚作为表面活性剂,硅油乳液作为消泡剂,丙二醇作为防冻剂,黄原胶作为增稠剂,1,2-苯并异噻唑啉-3-酮和2-甲基-4-异噻唑啉-3-酮作为生物杀伤剂,以及水作为填料/媒介物 |
2 | 苯菌酮FS配制剂(500g苯菌酮/L) | FS配制剂包含苯菌酮作为农药,甲基萘磺酸、甲醛的聚合物、钠盐和氧化乙烯/氧化丙烯嵌段共聚物作为表面活性剂,硅油乳液作为消泡剂,丙二醇作为防冻剂,黄原胶作为增稠剂,苯并异噻唑啉酮作为生物杀伤剂,以及水作为填料/媒介物 |
3 | (Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺FS配制剂(100g(Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺/L) | FS配制剂包含(Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺作为农药(参见EP-A 1017670),苯酚磺酸、甲醛和尿素的聚合物、钠盐和氧化乙烯/氧化丙烯嵌段共聚物作为表面活性剂,硅油乳液作为消泡剂,丙二醇作为防冻剂,黄原胶作为增稠剂,苯并异噻唑啉酮作为生物杀伤剂,以及水作为填料/媒介物 |
4 | 喹唑菌酮FS配制剂(100g喹唑菌酮/L) | 市售FS配制剂(Jockey) |
编号 | FS配制剂 | 成分 |
5 | 戊叉唑菌FS配制剂(25g戊叉唑菌/L) | 市售FS配制剂(Premis) |
A-1)制备表2的悬浮液浓缩物
将约400ml水引入容器中,加入表2所列量的配制助剂(表面活性剂和消泡剂)和杀真菌剂(肟醚菌胺)并均化混合物。将所得悬浮液借助珠磨式湿磨机研磨并用已经预分散于98ml水中的增稠剂以及生物杀伤剂(参见表2)增稠。用水和防冻剂将悬浮液的体积加至1000ml。
实施例2
A)涂覆稻种
对于涂覆稻种,将具有表2所示组成的3.2ml FS配制剂与表1所列的相应粘着剂溶液搅拌并用5-7ml水稀释,用于100g稻种。将所得含水悬浮液和水滴至在转鼓[TY-NEE Tumbler(A.E.Aubin)]中转动的种子上并培育5-10分钟。然后在室温下,通过空气充分干燥涂覆的种子。
B)测定稻种涂覆的有效性
将5g根据A1)涂覆的种子浸入在室温下(20℃)的1升水中,通过在2天、5天和8天定期萃取,化验在种子上的剩余的活性成分。根据通常的稻种发芽方法,在种子浸渍过程中为了向种子提供氧气,在3天和6天两次将所有水换成新鲜水。表3所示的结果说明用粘着剂涂覆的种子在用水浸渍8天并换水二次之后,种子上的活性成分显示出优异的剩余率(>80%),而不含粘着剂的种子仅显示低剩余率。
表3
配制剂[活性成分] | 粘着剂 | 活性成分量[g]<sup>2)</sup> | 粘着剂量[g]<sup>2</sup> | 剩余活性成分[%] |
肟醚菌胺<sup>1)</sup> | Acronal | 500 | 33 | 92.76 |
肟醚菌胺<sup>1)</sup> | Lawnfix | 500 | 33 | 85.2 |
肟醚菌胺<sup>1)</sup> | Polysol | 500 | 33 | 85.1 |
肟醚菌胺<sup>1)</sup> | 不含 | 500 | 33 | 50.9 |
1)表2FS配制剂
2)g/32kg种子
实施例3
A)涂覆小麦种子
对于涂覆100g小麦种子,用少量水稀释相应的FS配制剂。将FS配制剂和相应的粘着剂乳液滴至在转鼓中转动的种子上并培育15-20分钟。
然后在室温(25℃)下,通过空气干燥涂覆的种子。
B)测定小麦种子涂覆的有效性
如表4所示,用粘着剂涂覆的种子在室温下用水浸渍24小时后,种子上的活性成分显示出优异的剩余率(>80%),而不含粘着剂的种子仅显示低剩余率。
表4
配制剂[活性成分] | 粘着剂 | 活性成分量<sup>1)</sup> | 粘着剂量<sup>1)</sup> | 剩余活性成分[%] |
喹唑菌酮FS配制剂<sup>2)</sup> | 不含 | 150 | - | 27.3 |
喹唑菌酮FS配制剂<sup>2)</sup> | Lawnfix 700 | 150 | 3 | 99.6 |
喹唑菌酮FS配制剂<sup>2)</sup> | AcronalYJ2810Dap | 150 | 3 | 98.9 |
戊叉唑菌FS配制剂<sup>3)</sup> | 不含 | 60 | - | 24.1 |
戊叉唑菌FS配制剂<sup>3)</sup> | Lawnfix 700 | 60 | 3 | 87.2 |
戊叉唑菌FS配制剂<sup>3)</sup> | AcronalYJ2810Dap | 60 | 3 | 88.4 |
Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺FS配制剂<sup>4)</sup> | 不含 | 50 | 3 | 29.2 |
Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺FS配制剂<sup>4)</sup> | Lawnfix 700 | 50 | 3 | 84.8 |
Z)-N-[α-(环丙基甲氧基亚氨基)-2,3-二氟-6-(二氟甲氧基)苄基]-2-苯基乙酰胺FS配制剂<sup>4)</sup> | AcronalYJ2810Dap | 50 | 3 | 94.0 |
苯菌酮FS配制剂<sup>5)</sup> | 不含 | 500 | - | 54.1 |
苯菌酮FS配制剂<sup>5)</sup> | Lawnfix 700 | 500 | 3 | 91.7 |
配制剂[活性成分] | 粘着剂 | 活性成分量<sup>1)</sup> | 粘着剂量<sup>1)</sup> | 剩余活性成分[%] |
苯菌酮FS配制剂<sup>5)</sup> | AcronalYJ2810Dap | 500 | 3 | 94.4 |
1)[g]/100kg种子
2)见表2,编号4
3)见表2,编号5
4)见表2,编号3
5)见表2,编号2
实施例4测定种子涂覆的有效性
将根据实施例2A涂覆的稻栽培品种Koshihikari的稻种浸渍在具有标准种子消毒剂(环戊唑醇和氢氧化铜)的溶液中以防治种子本身的病害,然后浸渍在水中直至发芽。在种子消毒之后,在水中浸渍稻种直至发芽的特征在于胚芽刚破出种子外壳。将发芽的种子以所需播种密度在秧苗箱(通常30×60×3cm)中的底土上播种并盖上表土。在播种之后,将秧苗箱在所需温度(通常为25-30℃)下培育直至出苗,出苗的特征为胚芽鞘破出土壤表面。在确定出苗之后,将秧苗箱转移至阳光下,继续秧苗培育至移植。
在田地中,将瘟病侵染(稻瘟病菌)的稻秧苗移植在整块稻田中。对于鞘瘟病,将作为接种的菌丝体撒播在稻田中。
对于数据评估,在标准化(Hashiba method)后计算鞘瘟病的损害指数,这基于在某试样点的侵染植物的数目和病害症状的纵向发展的评价。穗颈瘟(panicle blast)通过计算由带有颈瘟病的穗的数目并分级而测定。
汇集于表5的数据显示用本发明粘着剂涂覆的种子几乎没有受到稻瘟病的影响。
表5
配制剂[活性成分(量<sup>1)</sup>)] | 粘着剂(量<sup>1)</sup>) | 有效性%<sup>2)</sup>叶瘟病<sup>3)</sup> | 有效性%<sup>2)</sup>穗颈瘟<sup>3)</sup> | 有效性%<sup>2)</sup>鞘瘟病<sup>4)</sup> |
[肟醚菌胺(500)] | LAWNFIX(33) | 97 | 84 | 99 |
[肟醚菌胺(500)] | POLYSOL(33) | 97 | 80 | 99 |
未处理<sup>3)</sup> | 0 | 0<sup>5)</sup> | 0<sup>5)</sup> | 0<sup>5)</sup> |
1)g/32kg种子;FS配制剂(参见表2,编号1)
2)防治百分数=(未处理的侵染-处理的侵染)/(未处理的侵染)×100
3)稻瘟病菌
4)笹木伏革菌
5)21.7%侵染.
Claims (13)
1.一种种子处理配制剂,其包含:
(a)至少一种农药;和
(b)丙烯酸酯共聚物,其中丙烯酸酯共聚物由如下单体组成:
(a’)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)选自下列的单体:选自(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯的(甲基)丙烯酸烷基酯,以及选自二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺的(甲基)丙烯酰胺;和
(c’)选自下列的单体:丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、甲基丙烯酸2-羟乙酯、甲基丙烯酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;和
(d’)选自下列的单体:苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯和对甲氧基苯乙烯;
且该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果其具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃;以及
其中所述丙烯酸酯共聚物的量基于固体含量为0.5-15重量%。
2.一种种子处理配制剂,其包含:
(a)至少一种农药;和
(b)丙烯酸酯共聚物,包含:
(a’)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d’)苯乙烯,
其中该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果该丙烯酸酯共聚物具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃,以及
其中所述丙烯酸酯共聚物的量基于固体含量为0.5-15重量%。
3.一种种子处理配制剂,其包含:
(a)至少一种农药;和
(b)丙烯酸酯共聚物,包含:
(a’)0.2-6重量%的丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)50-99.8重量%的甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d’)0-50重量%的苯乙烯,
其中该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果该丙烯酸酯共聚物具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃,
其中组分(a’)、(b’)和(d’)之和为100%;以及
其中所述丙烯酸酯共聚物的量基于固体含量为0.5-15重量%。
4.根据权利要求1-3任一项的种子处理配制剂,其中所述共聚物为具有核/壳结构的丙烯酸酯共聚物。
5.丙烯酸酯共聚物在制备种子处理配制剂中的用途,其中
(i)丙烯酸酯共聚物由如下单体组成:
(a’)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b’)选自下列的单体:选自(甲基)丙烯酸甲酯、(甲基)丙烯酸乙酯、(甲基)丙烯酸正丙酯、(甲基)丙烯酸正丁酯、(甲基)丙烯酸叔丁酯、(甲基)丙烯酸月桂酯、(甲基)丙烯酸环己酯、(甲基)丙烯酸2-乙基己酯、(甲基)丙烯酸硬脂醇酯、(甲基)丙烯酸十二烷酯的(甲基)丙烯酸烷基酯,以及选自二甲基(甲基)丙烯酰胺、二乙基(甲基)丙烯酰胺、异丙基(甲基)丙烯酰胺、(甲基)丙烯酰基吗啉、二甲氨基甲基(甲基)丙烯酰胺、二甲氨基乙基(甲基)丙烯酰胺、二甲氨基丙基(甲基)丙烯酰胺、二乙氨基甲基(甲基)丙烯酰胺、二乙氨基乙基(甲基)丙烯酰胺、二乙氨基丙基(甲基)丙烯酰胺的(甲基)丙烯酰胺;和
(c’)选自下列的单体:丙烯酸2-羟乙酯、丙烯酸2-羟丙酯、甲基丙烯酸2-羟乙酯、甲基丙烯酸2-羟丙酯、(甲基)丙烯酸缩水甘油酯;和
(d’)选自下列的单体:苯乙烯、α-甲基苯乙烯、邻甲基苯乙烯、间甲基苯乙烯、对甲基苯乙烯、对叔丁基苯乙烯、对氯甲基苯乙烯、对苯乙烯磺酸及其钠盐或钾盐、邻甲氧基苯乙烯、间甲氧基苯乙烯和对甲氧基苯乙烯;
且该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果其具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃。
6.包含如下单体的丙烯酸酯共聚物在制备种子处理配制剂中的用途:
(a)丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d)苯乙烯,
其中该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果该丙烯酸酯共聚物具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃。
7.包含如下单体的丙烯酸酯共聚物在制备种子处理配制剂中的用途:
(a)0.2-6重量%的丙烯酸、甲基丙烯酸或衣康酸或者至少两种选自丙烯酸、甲基丙烯酸或衣康酸的单体的组合;和
(b)50-99.8重量%的甲基丙烯酸甲酯、丙烯酸乙酯、丙烯酸正丁酯、甲基丙烯酸环己酯、丙烯酸2-乙基己酯或者(甲基)丙烯酰胺;和
(d)0-50重量%的苯乙烯,
其中该丙烯酸酯共聚物的玻璃化转变温度为-40℃至5℃,或者如果该丙烯酸酯共聚物具有核/壳结构,则内核的玻璃化转变温度为-60℃至5℃且外壳的玻璃化转变温度为20-150℃,
其中组分(a)、(b)和(d)之和为100%。
8.一种在播种前处理种子的方法,包括如下步骤:
a)将根据权利要求1-3中任一项的配制剂施用于溶剂中;和
b)将在步骤a)中得到的混合物施用于种子。
9.根据权利要求8的在播种前处理种子的方法,其中所述种子为稻种。
10.根据权利要求1-3中任一项的配制剂在种子萌发过程中的用途。
11.一种在播种前在种子萌发过程中处理种子的方法,包括如下步骤:
(i)使种子在受控条件下吸水,然后使种子在受控条件下发芽;
(ii)用根据权利要求1-3中任一项的配制剂处理种子;
其中
(a)可首先吸水,在第二步中用根据权利要求1-3中任一项的配制剂处理种子,或者
(b)可首先用根据权利要求1-3中任一项的配制剂处理种子,然后使种子吸水。
12.一种防治不希望的植物生长和/或抵抗植物病原性昆虫和/或植物病原性真菌的方法,包括将根据权利要求1-3中任一项的配制剂在播种前施用于种子。
13.一种防治不希望的植物生长和/或抵抗植物病原性昆虫和/或植物病原性真菌的方法,包括将根据权利要求1-3中任一项的配制剂在播种前施用于稻种。
Applications Claiming Priority (3)
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EP04003391 | 2004-02-16 | ||
EP04003391.2 | 2004-02-16 | ||
PCT/EP2005/001434 WO2005077170A1 (en) | 2004-02-16 | 2005-02-12 | Formulation for seed treatment comprising polymeric stickers |
Publications (2)
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CN1917757A CN1917757A (zh) | 2007-02-21 |
CN1917757B true CN1917757B (zh) | 2010-06-09 |
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CN2005800050442A Expired - Fee Related CN1917757B (zh) | 2004-02-16 | 2005-02-12 | 包含聚合物粘着剂的种子处理用配制剂 |
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US (1) | US20070298965A1 (zh) |
EP (2) | EP2210490A2 (zh) |
JP (1) | JP2007522174A (zh) |
KR (1) | KR20060131896A (zh) |
CN (1) | CN1917757B (zh) |
AR (1) | AR047674A1 (zh) |
AU (1) | AU2005213180A1 (zh) |
BR (1) | BRPI0507624A (zh) |
CA (1) | CA2554314A1 (zh) |
EA (1) | EA200601454A1 (zh) |
IL (1) | IL176927A0 (zh) |
NZ (1) | NZ548948A (zh) |
TW (2) | TW200605782A (zh) |
WO (2) | WO2005077169A1 (zh) |
ZA (1) | ZA200607692B (zh) |
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- 2005-02-12 EP EP05707358A patent/EP1720407A1/en not_active Withdrawn
- 2005-02-12 CN CN2005800050442A patent/CN1917757B/zh not_active Expired - Fee Related
- 2005-02-12 AU AU2005213180A patent/AU2005213180A1/en not_active Abandoned
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EP1078563B1 (en) * | 1999-08-25 | 2005-11-16 | National Starch and Chemical Investment Holding Corporation | Seed coating compositions for low temperature applications |
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EP2210490A2 (en) | 2010-07-28 |
JP2007522174A (ja) | 2007-08-09 |
IL176927A0 (en) | 2006-12-10 |
CA2554314A1 (en) | 2005-08-25 |
US20070298965A1 (en) | 2007-12-27 |
AR047674A1 (es) | 2006-02-01 |
NZ548948A (en) | 2009-09-25 |
CN1917757A (zh) | 2007-02-21 |
TW200605782A (en) | 2006-02-16 |
EP1720407A1 (en) | 2006-11-15 |
BRPI0507624A (pt) | 2007-07-03 |
WO2005077169A1 (en) | 2005-08-25 |
EA200601454A1 (ru) | 2007-02-27 |
TW200538041A (en) | 2005-12-01 |
KR20060131896A (ko) | 2006-12-20 |
WO2005077170A1 (en) | 2005-08-25 |
AU2005213180A1 (en) | 2005-08-25 |
ZA200607692B (en) | 2008-06-25 |
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