CN1898011B - 渗透膜蒸馏设备和方法 - Google Patents
渗透膜蒸馏设备和方法 Download PDFInfo
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- CN1898011B CN1898011B CN2005800014200A CN200580001420A CN1898011B CN 1898011 B CN1898011 B CN 1898011B CN 2005800014200 A CN2005800014200 A CN 2005800014200A CN 200580001420 A CN200580001420 A CN 200580001420A CN 1898011 B CN1898011 B CN 1898011B
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- 238000000034 method Methods 0.000 title claims abstract description 126
- 239000012528 membrane Substances 0.000 title claims abstract description 66
- 238000004821 distillation Methods 0.000 title abstract description 12
- 230000003204 osmotic effect Effects 0.000 title abstract description 4
- 239000000243 solution Substances 0.000 claims abstract description 195
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 170
- 230000008569 process Effects 0.000 claims abstract description 62
- 239000000126 substance Substances 0.000 claims abstract description 34
- 238000010790 dilution Methods 0.000 claims abstract description 26
- 239000012895 dilution Substances 0.000 claims abstract description 26
- 230000002209 hydrophobic effect Effects 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 14
- 239000007864 aqueous solution Substances 0.000 claims abstract description 10
- 229910010272 inorganic material Inorganic materials 0.000 claims abstract description 8
- 150000002484 inorganic compounds Chemical class 0.000 claims abstract description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 105
- 239000003513 alkali Substances 0.000 claims description 52
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 48
- 239000002699 waste material Substances 0.000 claims description 48
- 239000012266 salt solution Substances 0.000 claims description 41
- 150000004820 halides Chemical class 0.000 claims description 37
- 229910001507 metal halide Inorganic materials 0.000 claims description 31
- 150000005309 metal halides Chemical class 0.000 claims description 31
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 29
- 239000011780 sodium chloride Substances 0.000 claims description 25
- 239000007789 gas Substances 0.000 claims description 21
- 229910052736 halogen Inorganic materials 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 19
- 150000002367 halogens Chemical class 0.000 claims description 18
- 239000012141 concentrate Substances 0.000 claims description 17
- 239000000460 chlorine Substances 0.000 claims description 15
- 238000002360 preparation method Methods 0.000 claims description 15
- 238000005868 electrolysis reaction Methods 0.000 claims description 14
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 13
- 229910052801 chlorine Inorganic materials 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 7
- 230000005540 biological transmission Effects 0.000 claims description 7
- 238000006298 dechlorination reaction Methods 0.000 claims description 7
- 230000006872 improvement Effects 0.000 claims description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 5
- 238000013461 design Methods 0.000 claims description 5
- 229910052717 sulfur Inorganic materials 0.000 claims description 5
- 239000011593 sulfur Substances 0.000 claims description 5
- 229910001508 alkali metal halide Inorganic materials 0.000 claims description 4
- 150000008045 alkali metal halides Chemical class 0.000 claims description 4
- 239000007844 bleaching agent Substances 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 230000001737 promoting effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 2
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- 230000002708 enhancing effect Effects 0.000 abstract 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 55
- 239000012267 brine Substances 0.000 description 54
- 239000003795 chemical substances by application Substances 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 14
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- 229920002981 polyvinylidene fluoride Polymers 0.000 description 4
- 239000011148 porous material Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 229920000544 Gore-Tex Polymers 0.000 description 3
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- 239000011734 sodium Substances 0.000 description 3
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- 102100022463 Alpha-1-acid glycoprotein 1 Human genes 0.000 description 2
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- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 2
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- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- WURBVZBTWMNKQT-UHFFFAOYSA-N 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-1-yl)butan-2-one Chemical compound C1=NC=NN1C(C(=O)C(C)(C)C)OC1=CC=C(Cl)C=C1 WURBVZBTWMNKQT-UHFFFAOYSA-N 0.000 description 1
- FEKJRSSKHNBSFT-UHFFFAOYSA-N 2-fluoro-1,3-dioxole Chemical compound FC1OC=CO1 FEKJRSSKHNBSFT-UHFFFAOYSA-N 0.000 description 1
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 description 1
- 229920003934 Aciplex® Polymers 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229920001780 ECTFE Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
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- 229920003935 Flemion® Polymers 0.000 description 1
- 240000004859 Gamochaeta purpurea Species 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 229910019093 NaOCl Inorganic materials 0.000 description 1
- 229920000557 Nafion® Polymers 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
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- 238000005341 cation exchange Methods 0.000 description 1
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- 239000012024 dehydrating agents Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 description 1
- 229910000396 dipotassium phosphate Inorganic materials 0.000 description 1
- 235000019797 dipotassium phosphate Nutrition 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
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- 235000019674 grape juice Nutrition 0.000 description 1
- 239000012510 hollow fiber Substances 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
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- 238000005342 ion exchange Methods 0.000 description 1
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- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- MJGFBOZCAJSGQW-UHFFFAOYSA-N mercury sodium Chemical compound [Na].[Hg] MJGFBOZCAJSGQW-UHFFFAOYSA-N 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
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- 229910052698 phosphorus Inorganic materials 0.000 description 1
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- 229920002492 poly(sulfone) Polymers 0.000 description 1
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- 239000013535 sea water Substances 0.000 description 1
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- 230000035945 sensitivity Effects 0.000 description 1
- 229910001023 sodium amalgam Inorganic materials 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
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- RYCLIXPGLDDLTM-UHFFFAOYSA-J tetrapotassium;phosphonato phosphate Chemical compound [K+].[K+].[K+].[K+].[O-]P([O-])(=O)OP([O-])([O-])=O RYCLIXPGLDDLTM-UHFFFAOYSA-J 0.000 description 1
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- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/364—Membrane distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/88—Concentration of sulfuric acid
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
Description
温度,℃ | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
22 | 0.42 |
35 | 0.80 |
45 | 1.00 |
55 | 1.25 |
65 | 1.50 |
壳侧流动,ml/sec | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
6.6 | 2.25 |
8.5 | 2.90 |
10.0 | 3.30 |
温度,℃ | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
50 | 1.24 |
60 | 3.82 |
70 | 5.56 |
初始废盐水浓度,重量% | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
18.9 | 4.79 |
20.8 | 3.85 |
22.9 | 3.77 |
初始接收剂(NaOH)浓度,重量% | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
27.75 | 3.90 |
28.38 | 4.10 |
29.15 | 4.40 |
30.25 | 4.60 |
NaOH溶液线速度,cm/sec | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
2.4 | 3.16 |
14.4 | 5.56 |
H<sub>2</sub>O蒸汽压力差,Bar | H<sub>2</sub>O传递速率,kg/m<sup>2</sup>hr |
0.104 | 4.0 |
0.130 | 4.9 |
0.151 | 6.0 |
Claims (31)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA2,469,769 | 2004-06-04 | ||
CA002469769A CA2469769A1 (en) | 2004-06-04 | 2004-06-04 | Apparatus and method for spent alkali metal halide solution concentration using osmotic membrane distillation |
PCT/CA2005/000741 WO2005118114A1 (en) | 2004-06-04 | 2005-05-13 | Apparatus and method for osmotic membrane distillation |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009101755135A Division CN101653697B (zh) | 2004-06-04 | 2005-05-13 | 渗透膜蒸馏设备和方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1898011A CN1898011A (zh) | 2007-01-17 |
CN1898011B true CN1898011B (zh) | 2010-12-08 |
Family
ID=35446539
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2005800014200A Expired - Fee Related CN1898011B (zh) | 2004-06-04 | 2005-05-13 | 渗透膜蒸馏设备和方法 |
CN2009101755135A Expired - Fee Related CN101653697B (zh) | 2004-06-04 | 2005-05-13 | 渗透膜蒸馏设备和方法 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009101755135A Expired - Fee Related CN101653697B (zh) | 2004-06-04 | 2005-05-13 | 渗透膜蒸馏设备和方法 |
Country Status (9)
Country | Link |
---|---|
US (2) | US7361276B2 (zh) |
EP (1) | EP1753522B1 (zh) |
JP (1) | JP4996925B2 (zh) |
CN (2) | CN1898011B (zh) |
AU (1) | AU2005249612B2 (zh) |
CA (2) | CA2469769A1 (zh) |
ES (1) | ES2424152T3 (zh) |
WO (1) | WO2005118114A1 (zh) |
ZA (1) | ZA200601419B (zh) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7892321B2 (en) * | 2006-02-01 | 2011-02-22 | Intelligent Energy, Inc. | Integrated heated prevaporation module |
GB2452169A (en) * | 2007-02-25 | 2009-02-25 | Puregeneration | Carbon dioxide sequestering fuel synthesis system and use thereof |
US8178059B2 (en) * | 2007-12-05 | 2012-05-15 | Ch2M Hill Engineers, Inc. | Systems and methods for supplying chlorine to and recovering chlorine from a polysilicon plant |
US7871520B2 (en) * | 2007-12-18 | 2011-01-18 | Milton Roy Company | High-temperature membrane distillation |
US7608185B2 (en) * | 2007-12-18 | 2009-10-27 | Hamilton Sundstrand Corporation | Hollow fiber membrane modules for use in distillation systems |
US9039900B2 (en) | 2008-05-09 | 2015-05-26 | New Jersey Institute Of Technology | Membrane distillation apparatus and methods |
JP2012501233A (ja) * | 2008-08-28 | 2012-01-19 | ミクロリン・エルエルシー | 有益薬剤を一定速度で送出するための装置および方法 |
WO2010081077A2 (en) * | 2009-01-09 | 2010-07-15 | Massachusetts Institute Of Technology | Liquid filtration using pressure difference across a hydrophobic membrane |
DE102009017862A1 (de) * | 2009-04-17 | 2010-10-21 | Bayer Materialscience Ag | Verfahren zur Herstellung von Diarylcarbonat |
BRPI1013028A2 (pt) * | 2009-05-18 | 2016-04-05 | Vito N V | membranas de pervaporação de filme fino |
DE102009023940A1 (de) | 2009-06-04 | 2010-12-09 | Bayer Materialscience Ag | Verfahren zur Herstellung von Polycarbonat |
US20110168381A1 (en) * | 2009-12-11 | 2011-07-14 | Hydration Systems, Llc | Osmotic Water Transfer System and Related Processes |
KR101020316B1 (ko) * | 2010-04-28 | 2011-03-08 | 에스티엑스중공업 주식회사 | 막증류 방식을 이용한 정삼투 담수화 장치 |
US20130145748A1 (en) * | 2010-08-24 | 2013-06-13 | Asahi Kasei Chemicals Corporation | Method and Apparatus for Reducing Nitrogen Oxides in Internal Combustion Engine |
US9017530B2 (en) * | 2011-03-23 | 2015-04-28 | Brookhaven Science Associates, Llc | Method and electrochemical cell for synthesis and treatment of metal monolayer electrocatalysts metal, carbon, and oxide nanoparticles ion batch, or in continuous fashion |
EP2822674A4 (en) * | 2012-03-07 | 2015-12-16 | Chemetics Inc | NANO FILTRATION METHOD FOR IMPROVED SOLDER RECOVERY AND SULPHATE ELIMINATION |
CN103114298B (zh) * | 2013-02-20 | 2016-05-11 | 闫晓琦 | 一种膜蒸馏耦合制碱工艺 |
EP3046659B1 (en) * | 2013-09-18 | 2020-05-20 | Chemetics Inc. | Use of a hollow fibre membrane module with improved fluid flow distribution for osmotic membrane distillation |
CN104973658A (zh) * | 2014-04-09 | 2015-10-14 | 中国石油化工股份有限公司 | 一种低浓度磷酸废液的浓缩方法 |
CN107810044B (zh) * | 2015-07-01 | 2021-05-25 | 科思创德国股份有限公司 | 用于浓缩含有氯化钠的液体的渗透蒸馏方法 |
CN108704484A (zh) * | 2018-06-06 | 2018-10-26 | 大连理工大学 | 一种用于多元污染物水溶液的膜接触器分离方法 |
CN111151140B (zh) * | 2020-01-20 | 2021-10-15 | 河北工业大学 | 一种浓缩氯碱阳极淡盐水的方法 |
CN111232927A (zh) * | 2020-03-09 | 2020-06-05 | 广东水清环保科技有限公司 | 一种废酸回收方法与系统 |
DE102022200590A1 (de) * | 2022-01-19 | 2023-07-20 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein | Integrierte Wasseraufbereitung für die Wasserelektrolyse mittels osmotischer Membrandestillation |
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2005
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- 2005-05-13 ES ES05742602T patent/ES2424152T3/es active Active
- 2005-05-13 WO PCT/CA2005/000741 patent/WO2005118114A1/en not_active Application Discontinuation
- 2005-05-13 CN CN2009101755135A patent/CN101653697B/zh not_active Expired - Fee Related
- 2005-05-13 EP EP05742602.5A patent/EP1753522B1/en not_active Not-in-force
- 2005-05-13 CA CA002504848A patent/CA2504848C/en not_active Expired - Fee Related
- 2005-05-13 AU AU2005249612A patent/AU2005249612B2/en not_active Ceased
- 2005-05-13 JP JP2006548060A patent/JP4996925B2/ja not_active Expired - Fee Related
- 2005-06-01 US US11/141,490 patent/US7361276B2/en not_active Expired - Fee Related
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- 2008-03-03 US US12/073,241 patent/US20080173539A1/en not_active Abandoned
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CN85109400A (zh) * | 1984-11-21 | 1987-07-01 | 赛林斯研究有限公司 | 关于利用两种液体之间存在的渗透压差浓缩液体及其相应的设备 |
DE4229061C2 (de) * | 1992-09-01 | 1995-04-20 | Sep Tech Studien | Verfahren zur Rückgewinnung von wäßrigen Prozeßflüssigkeiten aus Oberflächenbehandlungsbädern |
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Also Published As
Publication number | Publication date |
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ZA200601419B (en) | 2007-05-30 |
JP4996925B2 (ja) | 2012-08-08 |
CN101653697B (zh) | 2013-08-14 |
CA2504848C (en) | 2006-08-22 |
CA2469769A1 (en) | 2005-12-04 |
CN101653697A (zh) | 2010-02-24 |
CA2504848A1 (en) | 2005-09-15 |
ES2424152T3 (es) | 2013-09-27 |
EP1753522A4 (en) | 2007-08-15 |
US20050269266A1 (en) | 2005-12-08 |
US20080173539A1 (en) | 2008-07-24 |
JP2007519823A (ja) | 2007-07-19 |
EP1753522A1 (en) | 2007-02-21 |
EP1753522B1 (en) | 2013-05-01 |
AU2005249612B2 (en) | 2007-09-13 |
AU2005249612A1 (en) | 2005-12-15 |
US7361276B2 (en) | 2008-04-22 |
WO2005118114A1 (en) | 2005-12-15 |
CN1898011A (zh) | 2007-01-17 |
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