CN1843383A - Traditional Chinese medicine preparation method - Google Patents
Traditional Chinese medicine preparation method Download PDFInfo
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- CN1843383A CN1843383A CNA2006100131639A CN200610013163A CN1843383A CN 1843383 A CN1843383 A CN 1843383A CN A2006100131639 A CNA2006100131639 A CN A2006100131639A CN 200610013163 A CN200610013163 A CN 200610013163A CN 1843383 A CN1843383 A CN 1843383A
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Abstract
The invention belongs to field of drug preparation, especially relating to field of traditional medicine preparation. It is characterized in that it comprises following steps: preparing spirit or tinctura with single traditional medicine, air-tight storing; mixing said spirit or tinctura with the amount equal to raw traditional medicine according to medical prescription for use, adding some water, boiling to regular amount soup, and getting the product. The effect component of traditional medicine can not only be extracted out completely, but also the comprehensive effect can be maintained for a long time; the product is easier to be accepted by patient after a part of alcohol being volatilized because of boiling.
Description
Technical field
The invention belongs to the drug formulation process field, particularly belong to the method for Chinese medicinal field.
Background technology
The preparation of Chinese medicine just has " department year be equipped with thing " theory from ancient times, promptly by time, place, plantation, gather, the preparation medicine." genuine medicinal materials " that the traditional Chinese medical science is said, its implication refer to gather two aspects of Chinese medicine place and time in fact.What it was emphasized is medical material collection preparation " relation of place, time and quality, drug effect ".Theory comes from " interior will discuss greatly through the most pure virginity ".Why to " take charge of and year be equipped with thing "? " interior warp " gone up and to be said: " non-department year, how also thing fully? " " loose also, matter with and different grade also ".Acquisition time, place that medical material is described are very big to the influence of drug effect.
We know the quality in order to ensure Chinese crude drug, and the collection of most of Chinese crude drug all has relatively-stationary place.As: the reason of " Fructus Citri tangerinae Sheng Huainan then is a Fructus Citri tangerinae, and it then is trifoliate orange that Fructus Citri tangerinae gives birth to Huai Bei "; In every year, gathering medicinal herbs also all has the time of respective fixation.So-called " Herba Artemisiae Scopariae Artemisia in April in March ".The quality of medicinal material of gathering between same every year and every year also is not quite similar.Trace it to its cause, Mei Nian climate characteristic difference at first, the Chinese crude drug growing environment is just different, thereby the Chinese crude drug quality is also easy because of year.Secondly, Chinese crude drug has growth cycle, and the different growing stages quality of medicinal material is also different.As everyone knows, the harvest of fruit tree has the branch of biennial bearing the same.The difference in same time, the Chinese crude drug quality differs greatly, and is example with the Chinese crude drug Radix Ginseng only, and to the mutation analysis of Radix Ginseng different growing stages chemical constituent, content comprises: 1, Various Seasonal Radix Ginseng sugar changes with saponin content.2, the same year, the stranger did not join the variation of root total saponin content.3, different growing stages Radix Ginseng enzyme composition changes.4, different growing stages Radix Ginseng amino acids composition changes.5, different growing stages Radix Ginseng carbohydrate content changes.6, different growing stages Radix Ginseng trace element changes.7, other compositions of different growing stages Radix Ginseng change.(conventional Chinese medicine composition with will manage handbook) result shows, because the difference in time time, the influence of centering quality of medicinal material is more than multipotency differs three one-tenth.
In the Radix Ginseng of report " Various Seasonal Radix Ginseng sugar with saponin content change " results in winter methanolic extract weight be gather in the crops summer 3 times of methanolic extract in the Radix Ginseng (Echmeister.L Progress in Chemistry of the OrganicNatural Produets.46.Springer-Verlag, 1984:41).Report " the same year, the stranger did not join the variation of root total saponin content ".It is that growth with the Radix Ginseng age increases that the ginsenoside content changes, but that 5 years strangers participate in 6 years strangers is irregular not little.(the Japanese plum hall, etc. Chinese crude drug 1989; 12 (1): 8).(the Japanese plum hall, etc. Radix Ginseng research 1988; (1): 42).
In sum, various reasons all can cause the Chinese crude drug quality to differ greatly.
Therefore, according to the Chinese crude drug growth cycle, with the requirement of growth climatic environment, the cycle in the optimal acquisition time of some medical material is several years, so in the time in several years, how can keep quality and drug effect that the best time gathers medical material? preservation is crucial.Existing medical material mostly is greatly with plucking in year, and with the year preparation, decoction pieces is preserved, in order to medicinal.Dried medicine decoction pieces easily goes mouldy, damages by worms, volatilizees, decomposes." the good medicine " that can not fully many best times be collected preserved for many years, uses for many years.
Therefore, will be subjected to the Chinese crude drug of time effects, gather the back with the preparation of Chinese medicine lixiviate formulation method, especially select for use medicated wine, tincture method preparation to preserve, this has just had remarkable meaning to medicine matter, the drug effect that keeps Chinese crude drug.
The preparation of preparing as the different auxiliary material of Western medicine has different drug effects, and different Chinese medicine method for makings also can produce different drug effects.In traditional water decoction with water as solvent, will be whole raw medicinal herbs immerse the drug effect that just can reach general expectation in the water.But medicated wine, tincture have the not available advantage of water decoction, owing to introduced wine as solvent, yang invigorating disperse function by wine can make the efficacy of a drug obtain the performance of faster and bigger effectiveness, therefore select as the optimal formulation of some promoting blood circulation to remove obstruction in the collateral medicines, traditional tiger-bone medicated wine, ageratum tincture are exactly example.
Yet the application of medicated wine, tincture is limited after all, traces it to its cause, and has still adopted with its preparation that to contain alcoholic acid solvent relevant.Because, some children's, anemia of pregnant woman, heart disease, hypertensive patient and to ethanol patient hypersensitive, so alcoholic intolerance is although medicated wine, tincture have good drug effect can not be extensive use of.
Summary of the invention
The objective of the invention is to the Chinese crude drug long term storage with best time collection, stable its best medicine matter, the drug effect of keeping also enlarges suitable crowd's scope and convenient the use.
The object of the present invention is achieved like this: a kind of method of Chinese medicinal, it is characterized in that, the single medicinal material material is made medicated wine or tincture, airtight deposit standby, during use various aforesaid medicated wine or tincture are amounted to become to be equivalent to certain crude drug amount and mix by folk prescription, add a certain amount of water, decoct to stipulating that medicinal liquid must measure, promptly.
The method for making of medicated wine or tincture and amount to the amount that is equivalent to raw medicinal herbs regulation according to the nineteen ninety-five version Pharmacopoeia of the People's Republic of China.
Adopt medicated wine or tincture to prepare medicine, can either fully extract the effective ingredient of medical material, can anticorrosionly help the long preservation of medicine again; Through decocting with water the ethanol content that can suitably volatilize, make the more people of the easier quilt of preparation accept, compound recipe mixes the medication theory that decoction meets the traditional Chinese medical science again.
Above-mentioned method of Chinese medicinal, employing be solvent extraction method, preferentially selecting for use is wherein percolation, and the single medicinal material material is made medicated wine or tincture.
Why adopting percolation, is because it can improve the stripping of effective ingredient to greatest extent, improves the preparation efficiency of medicated wine or tincture.
Above-mentioned method of Chinese medicinal, the Chinese liquor that described medicated wine adopts contains amount of alcohol 38 ~ 65%.
According to pharmacopeia regulation medicated wine should be raw material with frumentum wine.Employing contains the Chinese liquor of different concentration ethanol amount, is the extraction for the effective ingredient that helps different medical materials.
Above-mentioned method of Chinese medicinal, described tincture adopt 40% ~ 95% ethanol to make.The employing Different concentrations of alcohol also is the extraction for the effective ingredient that helps different medical materials.
Drinking utensils has rare pure character, is a kind of good solvent, no matter be free alkaloid or its esters, can both dissolve, and is convenient to immerse effective ingredient, keeps the comprehensive therapeutic effect of the various compositions of crude drug.Because medicated wine, tincture can be considered water and alcoholic acid mixed solvent.Water goes out alkaloid salts, glycoside, amaroid, acylate, tannin, protein, sugar, natural gum, pigment, polysaccharide in the medical material and enzyme and a spot of volatile oil as the solvent solubilized.Ethanol goes out alkaloid in the medical material and salt, glycoside (extracting alkaloid and the glycoside ethanol with 50-70%), sugar, resin, volatile oil (when generally extracting volatile oil with the ethanol more than 80%), alcohol, lactone, arene compounds etc. as the solvent solubilized, reaches little fat.Ethanol can be miscible with any ratio with water, so can utilize variable concentrations lixiviate selectively to go out effective ingredient, increases curative effect.
Medicated wine, tincture have antisepsis, can increase stability of formulation, so can long preservation.Because contain 20% alcoholic acid leachate and have antisepsis; The leachate that contains 40% above concentration of alcohol can delay many medicines, as the hydrolysis of compositions such as lipid, glycoside, increases stability of formulation.
Meet Chinese medical theory with the processed with wine medicine, wine itself also is Herba indigoferae Pseudotinctoriae, the time treasure say: " liquor---its acrid-sweet flavor, yang invigorating is dispersed; Its property is scorching, wins wet cold relieving.So can open looking angry strongly fragrant and downhearted long-pendingly, logical diaphragm and the phlegm retention of loosing are controlled and are rushed down malaria and end cold type of pain also ".The sweet suffering of wine is hot greatly, and energy promoting blood circulation, row medicine gesture, cold expelling, flavoring are rectified smelly.The history in existing thousands of years of medicated wine China, " interior ask through element " are loaded with " ancient times, the sage made the nutritious beverage,thick liquor and sweet liquor ", " wine with dregs sweet wine " medicated wine for referring to cure the disease.
A certain amount of water of described adding is meant the water of half as much again amount to the two sesquialter amount that adds medicated wine or tincture total amount.
Decoct with water is in order each medicine composition fully to be mixed, due chemical combination to take place, reaching the effect of Chinese medicine mixture.
Described decoction to a certain amount of total amount is meant and decocts to 20%～90% of the full dose of the medicated wine that is added or tincture and water.
By decocting with water, can also vapor away ethanol unnecessary in the mixture, make that more patients can accept such preparation.
Beneficial effect compared with prior art: adopt medicated wine or tincture to prepare the single medicinal material material, can either fully extract the effective ingredient of medical material, make the medical material in best time of component content be preserved and use; The comprehensive therapeutic effect that can keep the various compositions of crude drug again can also anticorrosionly help the long preservation of medicine; Through decocting with water, can the multiple medicine hair growth promoting of chemical combination drug effect, the ethanol that can suitably volatilize again makes that preparation is easier to be accepted by the people.Particularly the mixture of making through this method has the drug effect higher than light water decoct.
The specific embodiment
Example 1:
5 years strangers that adopted in 87 years are joined medical material, pulverize in accordance with the law and place percolator, add the 60 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Rhizoma Pinelliae of adopting in 86 years, pulverize in accordance with the law and place percolator, add the 50 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
The Radix Bupleuri of adopting in 85 years pulverized in accordance with the law place percolator, add the 50 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Fructus Evodiae of adopting in 86 years, pulverize in accordance with the law and place percolator, add the 50 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Drymotaenium miyoshianum (Mak.) Mak. of adopting in 83 years, pulverize in accordance with the law and place percolator, add the 38 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Herba Selaginellae of adopting in 93 years, pulverize in accordance with the law and place percolator, add the 50 degree Chinese liquor that are equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount.
Prescription: Radix Ginseng 10g, Rhizoma Pinelliae 10g, Radix Bupleuri 10g, Fructus Evodiae 5g, Drymotaenium miyoshianum (Mak.) Mak. 10g, Herba Selaginellae 10g.
Preparation: get the Radix Ginseng medicated wine 10ml that makes according to preceding method, amount to 2g crude drug amount; Get the Rhizoma Pinelliae medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Radix Bupleuri medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Fructus Evodiae medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Drymotaenium miyoshianum (Mak.) Mak. medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Herba Selaginellae medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount and mix, add the 180ml decocting in water open to full dose be 65ml promptly.
Therapeutic effect:
Clinical data: 70 routine cardiopalmus patients are divided into treatment at random organize 40 examples, matched group 30 examples.Wherein, male 45 examples, women 25 examples, women 14 people; 36 ~ 70 years old age.Diagnostic criteria is with reference to " tcm internal medicine today ".
Method: the treatment group adopts the medicated wine according to this law preparation, 1 dose of every day, 15 days courses of treatment.Matched group adopts the water decoction according to prescription, 1 dose of every day, 15 days courses of treatment.
Curative effect determinate standard: produce effects: the cardiopalmus transference cure, electrocardiographic oscillogram observation or dynamic ecg recordings examination obviously improve; Premature beat disappears, and it is accidental that paroxysmal supraventricular tachycardia or atrial fibrillation outbreak basic controlling or take place frequently transfers to.Effectively: the cardiopalmus symptom is most of to disappear, and electrocardiographic oscillogram observation or dynamic ecg recordings examination make moderate progress; The reduction more than 50% before the treatment of premature beat number of times, or take place frequently and transfer pilosity to, or pilosity transfers to accidental.Invalid: cardiopalmus symptom and electrocardiographic oscillogram observation or ambulatory electrocardiogram do not have change or increase the weight of.
The result:
Treatment group and matched group total effects are relatively
| Group | The example number | Produce effects | Effectively | Invalid | Total effective rate (%) |
| The treatment group | 40 | 17 | 20 | 3 | 90.25 |
| Matched group | 30 | 7 | 12 | 11 | 63.33 |
As can be seen from the above table, treatment group total effective rate is 90.25%, compares with matched group, learns by statistics and handles p＜0.01, and utmost point significant difference is arranged.And do not find any toxic and side effects.
Example 2
With the cockroach in 87 years, pulverize in accordance with the law and place percolator, add 75% ethanol that is equivalent to 5 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Rhizoma Belamcandae in 84 years, pulverize in accordance with the law and place percolator, add 80% ethanol that is equivalent to 5 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Radix Carpesii in 85 years, pulverize in accordance with the law and place percolator, add 95% ethanol that is equivalent to 5 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
The Radixs Angelicae Dahuricae in 90 years are pulverized in accordance with the law place percolator, add 50% ethanol that is equivalent to 5 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
With the Herba Asari in 92 years, pulverize in accordance with the law and place percolator, add 60% ethanol that is equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 10g/100ml crude drug amount;
With the Ramulus et Folium Dichroae febrifugae in 93 years, pulverize in accordance with the law and place percolator, add 70% ethanol that is equivalent to 4 times of amounts of medical material weight, placed 60 minutes, then carry out percolation; The percolation liquor strength of collecting can be amounted to 20g/100ml crude drug amount;
Prescription: cockroach 10g, Rhizoma Belamcandae 10g, Radix Carpesii 10g, Radix Angelicae Dahuricae 10g, Herba Asari 3g, Ramulus et Folium Dichroae febrifugae 10g.
Preparation: get the cockroach tincture 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Rhizoma Belamcandae tincture 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Radix Carpesii medicated wine 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Radix Angelicae Dahuricae tincture 25ml that makes according to preceding method, amount to 5g crude drug amount; Get the Herba Asari tincture 7.5ml that makes according to preceding method, amount to 1.5g crude drug amount; Get the Ramulus et Folium Dichroae febrifugae tincture 25ml that makes according to preceding method, amount to 5g crude drug amount and mix, add the 330ml decocting in water open to full dose be 400ml promptly.
Clinical research:
Data and method: diagnostic criteria: in " new Chinese medicine clinical research guideline ", the clinical research of treatment gout is a guideline; Adopt the Western medicine diagnose standard, the associating Chinese medical discrimination.
Clinical data: 100 examples are organized in treatment, wherein, and male 96 examples, women 4 examples; 32 ~ 83 years old age, mean aves 66.47 course of disease 2 days ~ 36 months.Matched group 50 examples, male 47 examples, women 3 examples; 38 ~ 85 years old age, the mean age 67.21; The course of disease 1 day ~ 34 months.
Method: the treatment group adopts the medicated wine according to this law preparation, 1 dose of every day, 15 days courses of treatment.Matched group adopts the water decoction according to prescription, 1 dose of every day, 15 days courses of treatment.
Curative effect determinate standard: clinical recovery: the symptom complete obiteration, joint function recovery is normal, and main physico-chemical examination index is normal.Produce effects: cardinal symptom disappears, and function of joint is recovered normally substantially, and main physico-chemical examination index is normal substantially.Effectively: cardinal symptom disappears substantially, and main function of joint and main physico-chemical examination index make moderate progress.Invalid: with the treatment before compare, each side does not all have improvement.
The result:
Treatment group and matched group total effects are relatively
| Group | Clinical recovery | Produce effects | Effectively | Invalid | Total effective rate |
| Treatment group (100 people) | 27 | 40 | 28 | 5 | 95％ |
| Matched group (50 people) | 8 | 12 | 15 | 15 | 70％ |
As can be seen from the above table, treatment group total effective rate is 95%, compares with matched group, learns by statistics and handles p＜0.01, and utmost point significant difference is arranged.And do not find any toxic and side effects.
Claims (8)
1, a kind of method of Chinese medicinal is characterized in that, the single medicinal material material is made medicated wine or tincture, airtightly deposit standbyly, during use various aforesaid medicated wine or tincture are amounted to become to be equivalent to certain crude drug amount and mix by folk prescription, add a certain amount of water, decoct to stipulating that medicinal liquid must measure, promptly.
2, method of Chinese medicinal as claimed in claim 1 is characterized in that, described single medicinal material material refers to bright medical material or crude drug decoction pieces.
3, method of Chinese medicinal as claimed in claim 1 or 2 is characterized in that, adopts percolation to make medicated wine or tincture the single medicinal material material.
4, method of Chinese medicinal as claimed in claim 1 is characterized in that, the amount of amounting to raw medicinal herbs is 20～100% of a general consumption.
5, method of Chinese medicinal as claimed in claim 1 is characterized in that, described medicated wine adopts 38～65 degree processed with wine to become.
6, method of Chinese medicinal as claimed in claim 1 is characterized in that, the ethanol of described tincture employing 40% ~ 95% is made.
7, method of Chinese medicinal as claimed in claim 1 is characterized in that, a certain amount of water of described adding is meant the water of half as much again amount to the two sesquialter amount that adds medicated wine or tincture total amount.
8, method of Chinese medicinal as claimed in claim 1 is characterized in that, described decoction to a certain amount of total amount is meant and decocts to 20%～90% of the full dose of the medicated wine that is added or tincture and water.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2006100131639A CN100548338C (en) | 2006-02-14 | 2006-02-14 | A kind of Chinese medicine preparation for the treatment of gout |
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| CNB2006100131639A CN100548338C (en) | 2006-02-14 | 2006-02-14 | A kind of Chinese medicine preparation for the treatment of gout |
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| CN1843383A true CN1843383A (en) | 2006-10-11 |
| CN100548338C CN100548338C (en) | 2009-10-14 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112331292A (en) * | 2020-10-22 | 2021-02-05 | 中日友好医院(中日友好临床医学研究所) | Traditional Chinese medicine ancient prescription decoction amount estimation method, storage medium and intelligent decoction equipment |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112331292A (en) * | 2020-10-22 | 2021-02-05 | 中日友好医院(中日友好临床医学研究所) | Traditional Chinese medicine ancient prescription decoction amount estimation method, storage medium and intelligent decoction equipment |
| CN112331292B (en) * | 2020-10-22 | 2024-03-19 | 中日友好医院(中日友好临床医学研究所) | Method for estimating decoction water quantity of ancient traditional Chinese medicine prescription, storage medium and intelligent decoction equipment |
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