CN1712150A - Continuously extruding method of magnesium alloy silk material - Google Patents
Continuously extruding method of magnesium alloy silk material Download PDFInfo
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Abstract
A continuous extruding method for preparing the Mg-alloy wire includes such steps as treating the surface of Mg alloy, loading it in the moulding cavity formed by big and small extruding cylinders, the first half of female die and the second half of female die, repeated extruding at 300-350 deg.C for fining its crystal grains and increasing its plasticity, loading it in a continuous extruder of wire material, and repeated extruding at 300-350 deg.C.
Description
Technical field
The invention belongs to technical field of nonferrous metal plastic molding, relate to a kind of pressing method of metal material, be specifically related to the continuous squeezing method of magnesium alloy silk material.
Background technology
Magnesium and magnesium alloy have low-gravity, high specific strength and specific stiffness and lower remarkable advantages such as the prices of raw and semifnished materials, have become the preferred material of industries such as Hyundai Motor, electronics, communication.The welding product of producing various magnesium alloys needs the welding rod or the welding wire of a large amount of magnesium alloy silk material preparations.Usually, welding wire available metal mold casting method when small lot batch manufacture is produced, can be by the extrusion modling manufacturing during production in enormous quantities.Conventional permanent mold casting method produces that the welding wire operation is simple, and cost is little, but production efficiency and product yield are low, and defectives such as pore, slag inclusion appear in welding wire easily, and the homogeneity of ingredients of welding wire, the content of alloying element are wayward; Rough owing to the magnesium extruded product, be easy to occur crackle, the easy obstruction of extruding path etc., therefore very big with conventional extrusion production magnesium alloy solder wire difficulty, and also the welding wire that adopts extrusion to produce at present is wrought magnesium alloy series.But, along with the expansion of magnesium alloy is used, the magnesium alloy of many alloys of high alloy content kind is more and more gradually, when welding the mother metal alloy of these high alloy content, obtain with the material soldering when just wishing to obtain, therefore need the welding wire of high alloy content with the high-quality joint of material or soldering.
In Dalian University of Technology's inscription on ancient bronze objects, in " forming technology of AZ61 magnesium alloy solder wire and the research of performance and progress " (" Shanghai non-ferrous metal " 2004 125 volumes 11 phase P1-4) article of work such as Liu Liming, narrated the technology that is hot extruded into ф 3.0mm, ф 1.6mm, ф 1.2mm welding wire at 400 ℃ of AZ61 magnesium alloy blanks with ф 44mm * (60～80) mm; In " research of magnesium alloy solder wire extrusion process extruding force " of work such as the Dong Changfu of Dalian University of Technology, Liu Liming (" plastic engineering journal " 2004 the 11 volumes 13 phase P35-38) article; put down in writing the technology that is hot extruded into ф 3.0mm, ф 2.14mm, ф 2.10mm, ф 1.6mm, ф 1.2mm welding wire at 400 ℃ of AZ31 magnesium alloy blanks with ф 44mm * (60～80) mm; and with this art applications the national patent protection; patent ZL03111456.3 " Mg alloy wire continuous squeezing method " (publication number 1443609, open day on September 24th, 2003).But these technology when extruding blank and mold temperature maintain all the time about 400 ℃～450 ℃, magnesium alloy is a semisolid, and for anti-blank fusing is blown the extrusion die exit with nitrogen, and will be under conditions such as rational lubricant, even need to adopt under the complex condition of hot extrusion and hot pull and just can finish, the requirement of mould and extruder is close to overcritical, it is high to push cost, efficient is extremely low, and can only the lower magnesium alloy of extruded alloy content.Because magnesium alloy is in semisolid in the above-mentioned extrusion process, for the magnesium alloy of high alloy content, will undergo phase transition and the very easily oxidation of hot extrusion blank, mould is in the hot operation state for a long time to also being die life disadvantageous, therefore it is higher relatively to push cost, and efficient is lower.
Summary of the invention
The object of the present invention is to provide a kind of continuous squeezing method of magnesium alloy silk material, solved the deficiency on the existing extrusion process, can prepare the magnesium alloy silk material of high alloy content, and the extruding cost is low, the efficient height.
The technical solution adopted in the present invention is that continuously extruding method of magnesium alloy silk material at first will be extruded the magnesium alloy blank and be placed in the reciprocating extruding pressure device, after the passage reciprocating extrusion by design, change the continuously extruded device of a material again into, will be extruded the magnesium alloy blank and be squeezed into a material
The reciprocating extruding pressure device comprises big extruding bucket and little extruding bucket, be provided with die cavity and profile between the two and be semicircular the first half dies and the second half dies, big extruding bucket, little extruding bucket, the first half dies and the second half dies surround mold cavity, be used for placing and be extruded the magnesium alloy blank, be extruded magnesium alloy blank two ends and be placed with first pressure ram and second pressure ram respectively, first pressure ram and second pressure ram and be extruded and be lined with first dummy block and second dummy block between the magnesium alloy blank respectively, the outer wall of big extruding bucket and little extruding bucket is wound with big extruding barrel resistance heating body and little extruding bucket resistance heating body respectively, is inserted with temperature thermocouple in the first half dies;
The continuously extruded device of silk material comprises big extruding bucket, the lower end of big extruding bucket is provided with die cavity and profile is semicircular the 3 half die and the 4 half die, aperture behind the 3 half die and the 4 half die matched moulds is ф 2mm～ф 10mm, inclination angle, prod cast chamber is 100 °～150 °, big extruding bucket and the 3 half die, the 4 half die surrounds mold cavity, be used for placing and be extruded the magnesium alloy blank, be extruded and place second dummy block and second pressure ram on the magnesium alloy blank, be lined with U type dummy block below the 3 half die and the 4 half die, the outer wall of big extruding bucket twines big extruding bucket resistance heating body, is inserted with temperature thermocouple in the 3 half die;
This method is carried out according to the following steps,
At first, after with forcing press the first half dies of reciprocating extruding pressure device and the second half dies being pressed into big extruding bucket, be pressed into little extruding bucket again and carry out matched moulds, will after the rust cleaning scrubbing, coat the magnesium alloy blank that is extruded of lubricating grease again and pack in the mold cavity that big extruding bucket, little extruding bucket, the first half dies and the second half dies surround;
Then give big extruding bucket resistance heating body and the energising of little extruding bucket resistance heating body, when reaching 300 ℃～350 ℃, keep this temperature, starting pressure machine, forcing press are compressed jumping-up again by the other end of pressing first pressure ram and second pressure ram to make to be extruded the magnesium alloy blank to be extruded to attenuate, pass the first half dies and the second half dies between the first half dies and the second half dies respectively and carry out the reciprocating extrusion process;
After reaching the extruding passage of design, take off little extruding bucket resistance heating body, little extruding bucket, first pressure ram, first dummy block, temperature thermocouple, the first half dies and the second half dies, install the 3 half die, the 4 half die, temperature thermocouple respectively, and on the mould underlay that assembles U type dummy block, become the continuously extruded device of a material;
Give the energising of big extruding bucket resistance heating body again, when the temperature recovery to 300 of die cavity ℃～350 ℃, keep this temperature, the starting pressure machine, regulate press pressure, control wire vent speed, forcing press is depressed second pressure ram and second dummy block, be extruded the magnesium alloy blank and be pressed towards down motion, the hole in the middle of the 3 half die and the 4 half die promptly is squeezed into magnesium alloy silk material.
Characteristics of the present invention are that also wire vent speed is controlled to be 0.5m/min～5m/min.
The 3 half die (13) and the 4 half die (14) adopt hot die steel 4Cr5MoV1Si to make.
U type dummy block (15) adopts mould steel Cr12MoV to make.
Method of the present invention is utilized the refinement of magnesium alloy blank crystallite dimension in the reciprocating extrusion process, the characteristics that plasticity is improved, directly pushing becomes the silk of thin diameter material again, pressure is low during extruding, be easy to extruding, be applicable to various forcing presses, wire vent speed is fast, and is easy to operate, and heavy alloyed magnesium alloy temperature in extrusion process is relatively low, have only 300 ℃～350 ℃, magnesium alloy can not undergo phase transition, and can oxidation in hot extrusion blank process, and mould also can long-term work, therefore it is relatively low to push cost, and efficient is higher.The magnesium alloy silk material that this method prepares is best in quality, and this method also is applicable to the high alloy silk material of continuously extruded other various light-alloys or difficult extruding.
Description of drawings
Fig. 1 is a reciprocating extruding pressure device structural representation of realizing the inventive method;
Fig. 2 is the vertical view of Fig. 1;
Fig. 3 is the continuously extruded device schematic diagram of silk material of realizing the inventive method;
Fig. 4 is the vertical view of Fig. 3.
Among the figure, 1. little extruding bucket resistance heating body, 2. little extruding bucket, 3. first pressure ram, 4. first dummy block, 5. temperature thermocouple, 6. the first half dies, 7. big extruding bucket 8. is extruded the magnesium alloy blank, 9. a big extruding bucket resistance heating body, 10. second dummy block, 11. second pressure rams, 12. the second half dies, 13. the 3 half dies, 14. the 4 half dies, 15.U the type dummy block, 16. magnesium alloy silk materials.
The specific embodiment
The present invention is described in detail below in conjunction with the drawings and specific embodiments.
Fig. 1, Fig. 2 are the reciprocating extruding pressure device structural representations of realizing the inventive method.This device comprises big extruding bucket 7 and little extruding bucket 2, be provided with the first half dies 6 and the second half dies 12 between the two, big extruding bucket 7, little extruding bucket 2, the first half dies 6 and the second half dies 12 surround mold cavity, put into this die cavity when being extruded magnesium alloy blank 8, its two ends are placed first pressure ram 3 and second pressure ram 11 respectively, first pressure ram 3 and second pressure ram 11 and be extruded and be lined with first dummy block 4 and second dummy block 10 between the magnesium alloy blank 8 respectively, the outer wall of big extruding bucket 7 and little extruding bucket 2 twines respectively in big extruding bucket resistance heating body 9 and little extruding bucket resistance heating body 1, the first half die 6 and is inserted with temperature thermocouple 5.The die cavity and the profile of first half dies 6 and the second half dies 12 are semicircle, the semicircle aperture of the semicircle aperture at the first half die 6 centers and the second half dies 12 constitutes a complete circular hole behind the matched moulds, is extruded magnesium alloy blank 8 and is extruded by this hole and attenuates.
Fig. 3, Fig. 4 are the continuously extruded device schematic diagrames of silk material of realizing the inventive method.Big extruding bucket the 7 and the 3 half die the 13, the 4 half die 14 surrounds mold cavity, when being extruded magnesium alloy blank 8 and putting into this die cavity, be extruded and put second dummy block 10 and second pressure ram 11 on the magnesium alloy blank 8, be lined with U type dummy block 15 below this die cavity, the outer wall of big extruding bucket 7 twines in big extruding bucket resistance heating body 9, the 3 half dies 13 and is inserted with temperature thermocouple 5.The die cavity and the profile of the 3 half die 13 and the 4 half die 14 also are semicircle, the median pore radius that both form behind the matched moulds is that ф 2mm～ф 10mm, inclination angle, prod cast chamber are 100 °～150 °, last Strain During Finishing Stage 3mm～8mm, the magnesium alloy blank 8 that is extruded after reciprocating extrusion is tapered by this taper hole, finally is squeezed into a material by last shaping aperture.Adopt hot die steel 4Cr5MoV1Si to make the 3 half die 13 and the 4 half die 14, adopt mould steel Cr12MoV to make U type dummy block 15.
Continuously extruding method of magnesium alloy silk material of the present invention, carry out according to the following steps:
At first, reciprocating extruding pressure device shown in Figure 1 is placed on the forcing press, with forcing press the first half dies 6 and the second half dies 12 are pressed into big extruding bucket 7 after, be pressed into little extruding bucket 2 again and carry out matched moulds, will after processing and appearance eliminate rust scrubbing, coat MoS again
2The magnesium alloy blank 8 that is extruded of lubricating grease is packed in the mold cavity that big extruding bucket 7, little extruding bucket 2, the first half dies 6 and the second half dies 12 surround;
Then give big extruding bucket resistance heating body 9 and 1 energising of little extruding bucket resistance heating body, measure heating-up temperature by temperature thermocouple 5, when reaching 300 ℃～350 ℃, keep this temperature, the starting pressure machine, forcing press attenuates by pressing first pressure ram 3 and second pressure ram 11 to make to be extruded magnesium alloy blank 8 to be extruded between the first half dies 6 and the second half dies 12 respectively, the other end that passes the first half dies 6 and the second half dies 12 is compressed jumping-up again and carries out the reciprocating extrusion process, by applying the pressure of different directions alternately, make and be extruded magnesium alloy blank 8 and push repeatedly and jumping-up, after the passage reciprocating extrusion of design, make blank produce kneading action, just can produce strong plastic deformation, simultaneously dynamic recrystallization take place and make crystal grain obtain remarkable refinement;
Then, take off little extruding bucket resistance heating body 1, little extruding barrel 2, first pressure ram 3, first dummy block 4, temperature thermocouple 5, the first half dies 6 and the second half dies 12, install the 3 half die the 13, the 4 half die 14, temperature thermocouple 5 respectively, and on the mould underlay that assembles U type dummy block 15, become Fig. 3, device shown in Figure 4;
Give big extruding bucket resistance heating body 9 energisings again, measure heating-up temperature by temperature thermocouple 5, when the temperature recovery to 300 of die cavity ℃～350 ℃, keep this temperature, the starting pressure machine, pressure size control wire vent speed by the setting pressure machine, wire vent speed is controlled in 0.5m/min～5m/min scope, forcing press is depressed second pressure ram 11 and second dummy block 10, be extruded magnesium alloy blank 8 and be pressed towards down motion, promptly be squeezed into magnesium alloy silk material 16 through the hole of magnesium alloy blank 8 in the middle of the 3 half die 13 and the 4 half die 14 that be extruded of grain refining.
Embodiment
The magnesium alloy silk material of continuously extruded one-tenth ф 5mm behind the reciprocating extrusion AZ91D magnesium alloy.
Get the raw materials ready industrial attitude AZ91D magnesium alloy ingot founding is again become the columniform ingot casting of diameter than the big 1mm～2mm of recipient diameter of bore, after stress relief annealing, again this pig moulding machine is processed into the columniform ingot casting of diameter, removes the processing greasy dirt and coat MoS at sidewall and upper surface than the little 0.2mm of recipient diameter of bore
2Lubricating grease;
At first, the reciprocating extruding pressure device is placed on the forcing press, after with forcing press the first half dies 6 and the second half dies 12 being pressed into big extruding bucket 7, be pressed into little extruding bucket 2 again and carry out matched moulds, the AZ91D magnesium alloy ingot 8 that is extruded of above-mentioned processing is packed in the mold cavity that big extruding bucket 7, little extruding bucket 2, the first half dies 6 and the second half dies 12 surround;
Then give little extruding bucket resistance heating body 1 and 9 energisings of big extruding bucket resistance heating body, the temperature that is recorded by temperature thermocouple 5 keeps this temperature when reaching 300 ℃, the starting pressure machine, forcing press attenuates by pressing first pressure ram 3 and second pressure ram 11 to make to be extruded AZ91D magnesium alloy ingot 8 to be extruded between the first half dies 6 and the second half dies 12 respectively, the other end that passes the first half dies 6 and the second half dies 12 is compressed jumping-up again and carries out the reciprocating extrusion process, remain 300 ℃ temperature in this process, after reciprocating extrusion 6 passages, the crystal grain that is extruded AZ91D magnesium alloy ingot 8 obtains remarkable refinement;
Then, take off little extruding bucket resistance heating body 1, little extruding barrel 2, first pressure ram 3, first dummy block 4, temperature thermocouple 5, the first half dies 6 and the second half dies 12, install the 3 half die the 13, the 4 half die 14, temperature thermocouple 5 respectively, and on the mould underlay that assembles U type dummy block 15, the aperture that the 3 half die the 13, the 4 half die 14 surrounds is ф 5mm, and inclination angle, prod cast chamber is 100 °;
Give resistance heating body 9 energisings of big extruding bucket again, when temperature recovery to 300 ℃, the starting pressure machine, the pressure size 5～8MPa of setting pressure machine, making wire vent speed is 5m/min, forcing press is depressed second pressure ram, 11, the second dummy blocks 10 and is being pressed and be extruded AZ91D magnesium alloy ingot 8 and move downward, and is extruded the magnesium alloy silk material 16 that the holes of AZ91D magnesium alloy ingot 8 in the middle of the 3 half die 13 and the 4 half die 14 promptly are squeezed into ф 5mm.
Method thinking novelty of the present invention, owing to adopt 300 ℃～350 ℃ temperature range reciprocating extrusion and continuously extruded, this temperature can not make the magnesium alloy of high alloy content that tissue inter-variable takes place in hot extrusion process, simultaneously, the 3 half die 13 and the 4 half die 14 that adopt hot die steel 4Cr5MoV1Si to make also can be in this temperature range long-term works, the silk material any surface finish flawless of this method preparation, dense internal organization, and easy to operate, the production efficiency height.
The present invention is suitable for the continuously extruded of various light-alloys or difficult extruded alloy, is particularly suitable for the continuously extruded of magnesium alloy, can obtain the silk material of ф 2mm～ф 10mm.
Claims (4)
1. a continuously extruding method of magnesium alloy silk material at first will be extruded magnesium alloy blank (8) and be placed in the reciprocating extruding pressure device, after the passage reciprocating extrusion by design, change the continuously extruded device of a material again into, and will be extruded magnesium alloy blank (8) and be squeezed into a material,
Described reciprocating extruding pressure device comprises big extruding bucket (7) and little extruding bucket (2), be provided with die cavity and profile between the two and be semicircular the first half dies (6) and the second half dies (12), big extruding bucket (7), little extruding bucket (2), the first half dies (6) and the second half dies (12) surround mold cavity, be used for placing and be extruded magnesium alloy blank (8), be extruded magnesium alloy blank (8) two ends and be placed with first pressure ram (3) and second pressure ram (11) respectively, first pressure ram (3) and second pressure ram (11) and be extruded and be lined with first dummy block (4) and second dummy block (10) between the magnesium alloy blank (8) respectively, the outer wall of big extruding bucket (7) and little extruding bucket (2) is wound with big extruding barrel resistance heating body (9) and little extruding barrel resistance heating body (1) respectively, is inserted with temperature thermocouple (5) in the first half dies (6);
The continuously extruded device of described silk material comprises big extruding bucket (7), the lower end of big extruding bucket (7) is provided with die cavity and profile is semicircular the 3 half die (13) and the 4 half die (14), aperture behind the 3 half die (13) and the 4 half die (14) matched moulds is φ 2mm～φ 10mm, inclination angle, prod cast chamber is 100 °～150 °, big extruding bucket (7) and the 3 half die (13), the 4 half die (14) surrounds mold cavity, be used for placing and be extruded magnesium alloy blank (8), be extruded magnesium alloy blank (8) and go up placement second dummy block (10) and second pressure ram (11), be lined with U type dummy block (15) below the 3 half die (13) and the 4 half die (14), the outer wall of big extruding bucket (7) twines big extruding bucket resistance heating body (9), is inserted with temperature thermocouple (5) in the 3 half die (13);
It is characterized in that this method is carried out according to the following steps,
At first, after with forcing press the first half dies (6) of reciprocating extruding pressure device and the second half dies (12) being pressed into big extruding bucket (7), be pressed into little extruding bucket (2) again and carry out matched moulds, will after the rust cleaning scrubbing, coat the magnesium alloy blank (8) that is extruded of lubricating grease again and pack in the mold cavity that big extruding bucket (7), little extruding bucket (2), the first half dies (6) and the second half dies (12) surround;
Then give big extruding bucket resistance heating body (9) and little extruding bucket resistance heating body (1) energising, when reaching 300 ℃～350 ℃, keep this temperature, starting pressure machine, forcing press are compressed jumping-up again by the other end of pressing first pressure ram (3) and second pressure ram (11) to make to be extruded magnesium alloy blank (8) to be extruded to attenuate, pass the first half dies (6) and the second half dies (12) between the first half dies (6) and the second half dies (12) respectively and carry out the reciprocating extrusion process;
After reaching the extruding passage of design, take off little extruding bucket resistance heating body (1), little extruding barrel (2), first pressure ram (3), first dummy block (4), temperature thermocouple (5), the first half dies (6) and the second half dies (12), install the 3 half die (13), the 4 half die (14), temperature thermocouple (5) respectively, and on the mould underlay that assembles U type dummy block (15), become the continuously extruded device of a material;
Give big extruding bucket resistance heating body (9) energising again, when the temperature recovery to 300 of die cavity ℃～350 ℃, keep this temperature, the starting pressure machine, regulate press pressure, control wire vent speed, forcing press is depressed second pressure ram (11) and second dummy block (10), be extruded magnesium alloy blank (8) and be pressed towards down motion, the hole in the middle of the 3 half die (13) and the 4 half die (14) promptly is squeezed into magnesium alloy silk material (16).
2. according to the described continuous squeezing method of claim 1, it is characterized in that described wire vent speed is controlled to be 0.5m/min～5m/min.
3. according to the described continuous squeezing method of claim 1, it is characterized in that described the 3 half die (13) and the 4 half die (14) adopt hot die steel 4Cr5MoVlSi to make.
4. according to the described continuous squeezing method of claim 1, it is characterized in that described U type dummy block (15) adopts mould steel Cr12MoV to make.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2005100429906A CN1298452C (en) | 2005-07-25 | 2005-07-25 | Continuously extruding method of magnesium alloy silk material |
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| CNB2005100429906A CN1298452C (en) | 2005-07-25 | 2005-07-25 | Continuously extruding method of magnesium alloy silk material |
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| CN1712150A true CN1712150A (en) | 2005-12-28 |
| CN1298452C CN1298452C (en) | 2007-02-07 |
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| CN101947705A (en) * | 2010-09-19 | 2011-01-19 | 哈尔滨理工大学 | Methods for producing magnesium alloy welding wires by adopting magnesium alloy foundry scraps |
| CN101947705B (en) * | 2010-09-19 | 2012-11-14 | 哈尔滨理工大学 | Methods for producing magnesium alloy welding wires by adopting magnesium alloy foundry scraps |
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| CN112620370A (en) * | 2020-11-26 | 2021-04-09 | 江苏科技大学 | Method for preparing superfine crystal magnesium alloy |
| CN113941035A (en) * | 2021-09-18 | 2022-01-18 | 西安理工大学 | Degradable blood vessel stent magnesium alloy pipe for inhibiting tumor proliferation and preparation method thereof |
| CN114669618A (en) * | 2022-04-07 | 2022-06-28 | 新乡市七星钎焊科技有限公司 | Brazing filler metal extrusion production process |
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