CN1616626A - Bird feather detergent and its producing method - Google Patents
Bird feather detergent and its producing method Download PDFInfo
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- CN1616626A CN1616626A CNA2004100647338A CN200410064733A CN1616626A CN 1616626 A CN1616626 A CN 1616626A CN A2004100647338 A CNA2004100647338 A CN A2004100647338A CN 200410064733 A CN200410064733 A CN 200410064733A CN 1616626 A CN1616626 A CN 1616626A
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- ether
- xylo
- mucine
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Abstract
The bird feather detergent is produced through mixing water, EDTA disodium, sodium dodecyl benzene sulfonate, dodecanol polyoxyethylene ether, ethoxyl hendecyl carboxymethyl imidazoline, emulsifier NP and ethyl glycol acetate via stirring; adding sodium carboxymethyl cellulose aqua; and finally adding citric acid to regulate the pH to 5-6. The washed bird feather washed with the detergent has COD lower than 10 mg each 100g, cleanliness higher than 450 mm and fat residue rate lower than 1 %. The detergent has high defatting and detergence efficiency, less foam, antistatic effect, bird feather puffing and softening effect, low cost, convenient use, no toxicity and no environmental pollution.
Description
Technical field
The present invention relates to a kind of prescription and manufacture method thereof of handling the Betengent product of fowl plumage.
Background technology
The fowl plumage belongs to natural protein fibre, mainly is used to the weighting material of clothes and bedclothes.The fowl plumage of purchase is also adhering to greasy dirt and a large amount of microorganism except that containing dust, so must be through just using after the special purpose detergent washing oven dry.The present washing composition that mostly is function singleness that adopts on the market, this class washing composition ubiquity have many bubbles, and degreasing power is low, and the rinsing water amount is big, and it is low to wash the back down cleanliness, Oil and Fat Content height, the problem of loft difference.
Summary of the invention
The objective of the invention is for washing efficient low foaming bird feather detergents such as all kinds of goose feather, goose down, drake feather, duck's down, chicken feather.
The present invention includes following preparation: Nonyl pheno (6) ether, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, ethyl cellosolve acetate, Xylo-Mucine, disodium ethylene diamine tetraacetate, water.
The mass percent that each composition accounts for total amount is: Nonyl pheno (6) ether 5～30%, Sodium dodecylbenzene sulfonate 2～20%, lauryl alcohol polyoxyethylene (9) ether 2～25%, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 1～10%, ethyl cellosolve acetate 1～10%, Xylo-Mucine 0.1～2.0%, disodium ethylene diamine tetraacetate 1～6%, citric acid a little, water surplus.
The present invention also provides the manufacture method of the bird feather detergent of above-mentioned high-effective low foam, may further comprise the steps:
(1) Xylo-Mucine is made the Xylo-Mucine water-sol.
(2) in the container of slow stirrer is housed, add entry, disodium ethylene diamine tetraacetate, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the above-mentioned Xylo-Mucine water-sol again.
(3) regulate the potential of hydrogen of above-mentioned mixture with citric acid, make pH value 5～6.
The present invention is formed by preparation of raw material such as nonionogenic tenside, anion surfactant, zwitterionics, washing auxiliary detergent, solvents.It has the following advantages and effect:
1, degreasing detersive efficiency height.Owing to adopted the composite of kinds of surface promoting agent, washing auxiliary detergent, solvent, bring into play its best washing function, the fowl plumage oil residue after the washing is low, and oxygen-consumption is low.
2, low bubble, easily rinsing.Previous washings because of producing a large amount of foams, causes feather and foamy to mix in washing process, makes overall volume increase, and feather overflows washing trough, needs simultaneously with a large amount of water and rinsing for a long time.The present invention has then overcome these deficiencies, has improved detersive efficiency, and the fowl plumage degree of cleaning height after the washing.
3, the fowl plumage after the washing has good static resistance and loft.Because the effect of tensio-active agent, the fowl plumage surface static electrification not that makes washing, the fowl plumage can not adhere to each other, thereby is convenient to separating of feather and eider down, also helps the fowl plumage adds man-hour at follow-up goods stuffing operation.
When 4, this product used, directly dilute with water did not need heat, and room temperature washing is not hindered feather, and is convenient, safe, nontoxic, pollution-free.
Specific embodiment
Embodiment one, preparation 100kg washing composition:
Take by weighing each reagent by following requirement respectively:
Nonyl pheno (6) ether 15kg
Sodium dodecylbenzene sulfonate 6kg
Lauryl alcohol polyoxyethylene (9) ether 8kg
Hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 5kg
Ethyl cellosolve acetate 4kg
Xylo-Mucine 1kg
Disodium ethylene diamine tetraacetate 3kg
Processing step:
(1) in container, above-mentioned 1kg Xylo-Mucine is dispersed in the 10kg water, the slight stirring is made into 10% the water-sol.
(2) in the container of slow stirrer is housed, add about 48kg water, the disodium ethylene diamine tetraacetate of above-mentioned weight, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the Xylo-Mucine water-sol again by last method preparation.
(3) continue to stir, regulate the potential of hydrogen of washing composition at last with citric acid, make pH value 5～6.
Washing is used:
Take by weighing 30g eider down (down content 50%); bath raio 1: 50 (detergent concentration 0.1%) is put into the 3000mL Erlenmeyer flask; place on the horizontal shaker; vibrational frequency is 2.5Hz; about Oscillation Amplitude 20mm, 25 ℃ of wash temperatures, washing 20min; use water rinse 40min is then dried down at 50 ℃ with constant temperature oven.
Washing effect:
Washing effect test (pressing the GB 10289-88 outlet washed feather ﹠ down method of inspection)
Oxygen-consumption: 3.8mg/100g
Oil and Fat Content: 0.83%
Degree of cleaning: 550mm
Loft: 15.4cm
Oder levels: 1
The physical and chemical index of product of the present invention:
Outward appearance: clarification or milky white liquid
pH：5.0～6.0
Viscosity: 〉=1000mPa.S
Heat-resisting: 50 ℃ ± 1 ℃, 24h is stable
Cold-resistant :-10 ℃ ± 1 ℃, 24h is stable
Foam :≤50mm (Ross-Miles method)
Embodiment two, preparation 100kg washing composition:
Take by weighing each reagent by following requirement respectively:
Nonyl pheno (6) ether 30kg
Sodium dodecylbenzene sulfonate 2kg
Lauryl alcohol polyoxyethylene (9) ether 5kg
Hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 10kg
Ethyl cellosolve acetate 6kg
Xylo-Mucine 2kg
Disodium ethylene diamine tetraacetate 6kg
Processing step:
(1) in container, above-mentioned 2kg Xylo-Mucine is dispersed in the 20kg water, the slight stirring is made into 20% the water-sol.
(2) in the container of slow stirrer is housed, add about 19kg water, the disodium ethylene diamine tetraacetate of above-mentioned weight, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the Xylo-Mucine water-sol again by last method preparation.
(3) continue to stir, regulate the potential of hydrogen of washing composition at last with citric acid, make pH value 5～6.
This product can be used for the eider down washing of down content higher (greater than 70%).
Embodiment three, preparation 100kg washing composition:
Take by weighing each reagent by following requirement respectively:
Nonyl pheno (6) ether 5kg
Sodium dodecylbenzene sulfonate 20kg
Lauryl alcohol polyoxyethylene (9) ether 2kg
Hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 1kg
Ethyl cellosolve acetate 1kg
Xylo-Mucine 0.1kg
Disodium ethylene diamine tetraacetate 1kg
Processing step:
(1) in container, above-mentioned 0.1kg Xylo-Mucine is dispersed in the 1kg water, the slight stirring is made into 10% the water-sol.
(2) in the container of slow stirrer is housed, add about 68kg water, the disodium ethylene diamine tetraacetate of above-mentioned weight, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the Xylo-Mucine water-sol again by last method preparation.
(3) continue to stir, regulate the potential of hydrogen of washing composition at last with citric acid, make pH value 5～6.
This product can be used for the feather washing.
Embodiment four, preparation 100kg washing composition:
Take by weighing each reagent by following requirement respectively:
Nonyl pheno (6) ether 10kg
Sodium dodecylbenzene sulfonate 2kg
Lauryl alcohol polyoxyethylene (9) ether 25kg
Hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 6kg
Ethyl cellosolve acetate 6kg
Xylo-Mucine 1.5kg
Disodium ethylene diamine tetraacetate 2kg
Processing step:
(1) in container, above-mentioned 1.5kg Xylo-Mucine is dispersed in the 15kg water, the slight stirring is made into the Xylo-Mucine water-sol.
(2) in the container of slow stirrer is housed, add about 32kg water, the disodium ethylene diamine tetraacetate of above-mentioned weight, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the Xylo-Mucine water-sol again by last method preparation.
(3) continue to stir, regulate the potential of hydrogen of washing composition at last with citric acid, make pH value 5～6.
This example product can be used for the higher eider down washing of fat content.
Claims (3)
1, bird feather detergent is characterized in that comprising following preparation: Nonyl pheno (6) ether, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, ethyl cellosolve acetate, Xylo-Mucine, disodium ethylene diamine tetraacetate, water.
2, according to the described bird feather detergent of claim 1, it is characterized in that the mass percent that accounts for total amount of each preparation is: Nonyl pheno (6) ether 5～30%, Sodium dodecylbenzene sulfonate 2～20%, lauryl alcohol polyoxyethylene (9) ether 2～25%, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline 1～10%, ethyl cellosolve acetate 1～10%, Xylo-Mucine 0.1～2.0%, disodium ethylene diamine tetraacetate 1～6%.
3, the manufacture method of bird feather detergent is characterized in that may further comprise the steps:
A, Xylo-Mucine is made the Xylo-Mucine water-sol;
B, in the container of slow stirrer is housed, add entry, disodium ethylene diamine tetraacetate, Sodium dodecylbenzene sulfonate, lauryl alcohol polyoxyethylene (9) ether, hydroxyethyl undecyl carboxymethyl tetrahydroglyoxaline, Nonyl pheno (6) ether, ethyl cellosolve acetate while stirring successively, after stirring, add the above-mentioned Xylo-Mucine water-sol again;
C, with the potential of hydrogen that citric acid is regulated above-mentioned mixture, making pH value is 5～6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100647338A CN1236035C (en) | 2004-09-21 | 2004-09-21 | Bird feather detergent and its producing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100647338A CN1236035C (en) | 2004-09-21 | 2004-09-21 | Bird feather detergent and its producing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1616626A true CN1616626A (en) | 2005-05-18 |
| CN1236035C CN1236035C (en) | 2006-01-11 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100647338A Expired - Fee Related CN1236035C (en) | 2004-09-21 | 2004-09-21 | Bird feather detergent and its producing method |
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| CN (1) | CN1236035C (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101003721B (en) * | 2006-12-21 | 2010-07-07 | 中国海洋石油总公司 | Humidification type dustlaying agent |
| CN102660396A (en) * | 2012-05-22 | 2012-09-12 | 河北永泰皮化化工有限公司 | Fur fat removal agent |
| CN103451955A (en) * | 2013-07-24 | 2013-12-18 | 安徽润丰羽绒有限公司 | Down washing and finishing agent and preparation method thereof |
| CN107245872A (en) * | 2017-07-12 | 2017-10-13 | 安徽华翎羽毛制品有限公司 | A kind of process that down jackets drake feather grease is removed using compound degreasing agent |
| CN107446717A (en) * | 2017-07-12 | 2017-12-08 | 安徽华翎羽毛制品有限公司 | A kind of down jackets drake feather cleaning agent and its preparation and cleaning method |
| CN111218350A (en) * | 2020-02-12 | 2020-06-02 | 陕西科技大学 | Fulvic acid feather cleaning agent and preparation method thereof |
| WO2020218100A1 (en) * | 2019-04-25 | 2020-10-29 | ライオン・スペシャリティ・ケミカルズ株式会社 | Cleaning agent for raw material feather and down and cleaning liquid for raw material feather and down |
| CN113652314A (en) * | 2021-09-10 | 2021-11-16 | 中国热带农业科学院农产品加工研究所 | Duck down detergent |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101638577B (en) * | 2009-08-28 | 2012-02-01 | 西安石油大学 | Natural feather plugging fiber used for drilling of oil and gas wells in oil fields and preparation method thereof |
-
2004
- 2004-09-21 CN CNB2004100647338A patent/CN1236035C/en not_active Expired - Fee Related
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101003721B (en) * | 2006-12-21 | 2010-07-07 | 中国海洋石油总公司 | Humidification type dustlaying agent |
| CN102660396A (en) * | 2012-05-22 | 2012-09-12 | 河北永泰皮化化工有限公司 | Fur fat removal agent |
| CN103451955A (en) * | 2013-07-24 | 2013-12-18 | 安徽润丰羽绒有限公司 | Down washing and finishing agent and preparation method thereof |
| CN103451955B (en) * | 2013-07-24 | 2015-09-02 | 安徽润丰羽绒有限公司 | Eider down washing finishing agent and preparation method thereof |
| CN107245872A (en) * | 2017-07-12 | 2017-10-13 | 安徽华翎羽毛制品有限公司 | A kind of process that down jackets drake feather grease is removed using compound degreasing agent |
| CN107446717A (en) * | 2017-07-12 | 2017-12-08 | 安徽华翎羽毛制品有限公司 | A kind of down jackets drake feather cleaning agent and its preparation and cleaning method |
| WO2020218100A1 (en) * | 2019-04-25 | 2020-10-29 | ライオン・スペシャリティ・ケミカルズ株式会社 | Cleaning agent for raw material feather and down and cleaning liquid for raw material feather and down |
| CN113710790A (en) * | 2019-04-25 | 2021-11-26 | 狮王特殊化学株式会社 | Detergent for raw feather and washing liquid for raw feather |
| CN111218350A (en) * | 2020-02-12 | 2020-06-02 | 陕西科技大学 | Fulvic acid feather cleaning agent and preparation method thereof |
| CN114292710A (en) * | 2020-02-12 | 2022-04-08 | 陕西科技大学 | Feather cleaning agent and preparation method thereof |
| CN113652314A (en) * | 2021-09-10 | 2021-11-16 | 中国热带农业科学院农产品加工研究所 | Duck down detergent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1236035C (en) | 2006-01-11 |
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