CN1579169A - Environment-protection infactant and its making method - Google Patents
Environment-protection infactant and its making method Download PDFInfo
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- CN1579169A CN1579169A CN 200410024093 CN200410024093A CN1579169A CN 1579169 A CN1579169 A CN 1579169A CN 200410024093 CN200410024093 CN 200410024093 CN 200410024093 A CN200410024093 A CN 200410024093A CN 1579169 A CN1579169 A CN 1579169A
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- myrobalan
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Abstract
The invention is a green environmental-protection disinfectant, composed of gallnut, isatis root, dehydrated alum, honeysuckle vine, rheum officinale, the fruit of Chinese magnoliavine and myrobalan fruit. It solves the disadvantages in existing technique, such as toxic and side effect, environmental pollution, etc. It can remarkably kill and inhibit bacteria, fungi and viruses, safe to apply and remarkably- disinfecting, low-cost of production and meeting the requirements of clean production and environmental protection.
Description
(1) technical field
The present invention relates to a kind of environmental type disinfectant and manufacture method thereof, belong to the Environmental Science and Engineering field.
(2) background technology
The traditional chemical disinfectant reaches the purpose of eliminating the pathogeny microorganism mostly with its strong oxidizing property, therefore also brought a series of negative effect, be example with the chlorhexidine-containing disinfectant: chlorhexidine-containing disinfectant commonly used has chlorine, chlorine dioxide, clorox etc., though can effectively kill bacterium and virus in the sewage, Cl
2Poisonous, the strong Cl of corrosivity
2Produce easily also with NaOCl that tool is carcinogenic, the organic chloride of teratogenesis (THMs).ClO
2Though do not produce organic chloride, operation, management have certain danger, can only produce on the spot, use, and the equipment complexity, operational administrative requires high.Chlorination also must be taked the dechlorination measure because the too high meeting of chlorine residue causes hydrobiological death in the surface water body when therefore draining into surface water body in addition.All the other traditional disinfectants also exist and produce to use dangerously, and corrosivity and strong toxicity are to human body and the unfavorable deficiency that waits of environment.
(3) summary of the invention
Purpose of the present invention is exactly for shortcomings such as the toxic and side effect that solves the prior art existence, contaminated environment, is the environmental type disinfectant of primary raw material and design a kind of with the Chinese medicine book on Chinese herbal medicine, and has provided its concrete preparation method.
The present invention is realized by following technical scheme:
This environmental type disinfectant is made up of gall nut, Radix Isatidis, alumen, honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, myrobalan, and their mass fraction is respectively
Gall nut 45%～50%
Radix Isatidis 10%～15%
Alumen 8%～12%
Honeysuckle rattan 8%～12%
Rheum officinale 5%～8%
Schisandra sphenanthera Rehd.et WilS 4%～6%
The myrobalan 4%～6%
This environmental type disinfectant be a kind of be the environmental friendliness disinfectant of primary raw material with the Chinese medicine book on Chinese herbal medicine, its preparation process is as follows:
1. choose gall nut, Radix Isatidis, alumen, honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, myrobalan and pulverize respectively, particle diameter is controlled at 30～60 orders, prepares burden according to mass fraction, in the traditional Chinese medicine extraction of packing into after the mixing jar, then
2. add the water of 6～12 times of quality of material in jar, heating was boiled 30～50 minutes, emitted extract in basin, added the water of 4～8 times of quality of material again, and heating was boiled 20～40 minutes, emitted extract, and secondary raffinate is merged, then
3. amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 50%～80% the time, add the deionized water of 3 times of quality of material to trapped fluid, continue micro-filtration, again will
4. the micro-filtrate that obtains is put into the low temperature enrichment facility, under 55 ℃～70 ℃ conditions, is concentrated into 25% of micro-filtrate volume, and the concentrate that obtains is thimerosal.
The present invention is the production that the Chinese medicine book on Chinese herbal medicine is used for disinfectant, so this disinfectant do not contain " environment exotic ", does not produce secondary pollution, is a kind of environmental type disinfectant.It has the uniqueness sterilization mechanism of protein precipitation, and various common disease substances such as bacterium, fungi and virus are had remarkable killing and inhibitory action, application safety, and effect is remarkable.The dregs of a decoction that produce in the disinfectant production process can be used as fertilizer and are used for agricultural production after treatment in addition, strengthen plant disease-resistant insect pest ability, meet cleaner production and requirement on environmental protection.
In a word, it is simple that the present invention has technology, and production cost is low, application safety, advantage such as Disinfection Effect is remarkable.
(4) embodiment
Embodiment 1:
Choose gall nut, Radix Isatidis, alumen, the honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, the myrobalan pulverizes respectively, particle diameter is controlled at 30 orders, prepare burden according to the kind quantity of producing prescription then, gall nut 5kg, Radix Isatidis 1.5kg, alumen 1.2kg, honeysuckle rattan 1kg, rheum officinale 0.5kg, Schisandra sphenanthera Rehd.et WilS 0.4kg, myrobalan 0.4kg, after mixing, add in the traditional Chinese medicine extraction jar, add the 60kg running water to this extractor, heating was boiled 30 minutes, emitted extract 48kg in basin, added the 48kg running water in the traditional Chinese medicine extraction jar again, heating was boiled 20 minutes, emit secondary raffinate 45kg, merge and put into basin, extracted twice liquid merges the back and amounts to 93kg.This extraction amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 50% the time, add the 30kg deionized water to trapped fluid, continue micro-filtration, finally obtain the 120kg micro-filtrate, this micro-filtrate is put into the low temperature concentrator, under 55 ℃ of conditions, obtain the 30kg concentrate, be disinfectant.Stoste through quality testing qualified after, can be canned, packing, become disinfectant products.
Embodiment 2:
Choose gall nut, Radix Isatidis, alumen, the honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, the myrobalan pulverizes respectively, particle diameter is controlled at 60 orders, prepare burden according to the kind quantity of producing prescription then, gall nut 4.5kg, Radix Isatidis 1.5kg, alumen 1kg, honeysuckle rattan 1.2kg, rheum officinale 0.8kg, Schisandra sphenanthera Rehd.et WilS 0.4kg, myrobalan 0.6kg, after mixing, add in the traditional Chinese medicine extraction jar, add the 120kg running water to this extractor, heating was boiled 50 minutes, emitted extract 96kg in basin, added the 96kg running water in the traditional Chinese medicine extraction jar again, heating was boiled 40 minutes, emit secondary raffinate 90kg, merge and put into basin, extracted twice liquid merges the back and amounts to 186kg.This extraction amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 80% the time, add the 30kg deionized water to trapped fluid, continue micro-filtration, finally obtain the 210kg micro-filtrate, this micro-filtrate is put into the low temperature concentrator, under 70 ℃ of conditions, obtain the 53kg concentrate, be disinfectant.Stoste through quality testing qualified after, can be canned, packing, become disinfectant products.
Embodiment 3:
Choose gall nut, Radix Isatidis, alumen, the honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, the myrobalan pulverizes respectively, particle diameter is controlled at 30 orders, prepare burden according to the kind quantity of producing prescription then, gall nut 5kg, Radix Isatidis 1kg, alumen 1.2kg, honeysuckle rattan 1.2kg, rheum officinale 0.8kg, Schisandra sphenanthera Rehd.et WilS 0.4kg, myrobalan 0.4kg, after mixing, add in the traditional Chinese medicine extraction jar, add the 60kg running water to this extractor, heating was boiled 30 minutes, emitted extract 48kg in basin, added the 48kg running water in the traditional Chinese medicine extraction jar again, heating was boiled 20 minutes, emit secondary raffinate 45kg, merge and put into basin, extracted twice liquid merges the back and amounts to 93kg.This extraction amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 50% the time, add the 30kg deionized water to trapped fluid, continue micro-filtration, finally obtain the 120kg micro-filtrate, this micro-filtrate is put into the low temperature concentrator, under 55 ℃ of conditions, obtain the 30kg concentrate, be disinfectant.Stoste through quality testing qualified after, can be canned, packing, become disinfectant products.
Embodiment 4:
Choose gall nut, Radix Isatidis, alumen, the honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, the myrobalan pulverizes respectively, particle diameter is controlled at 60 orders, prepare burden according to the kind quantity of producing prescription then, gall nut 5kg, Radix Isatidis 1.5kg, alumen 1.2kg, honeysuckle rattan 0.8kg, rheum officinale 0.5kg, Schisandra sphenanthera Rehd.et WilS 0.6kg, myrobalan 0.4kg, after mixing evenly, add in the traditional Chinese medicine extraction jar, add the 120kg running water to this extractor, heating was boiled 50 minutes, emitted extract 96kg in basin, added the 96kg running water in the traditional Chinese medicine extraction jar again, heating was boiled 40 minutes, emit secondary raffinate 90kg, merge and put into basin, extracted twice liquid merges the back and amounts to 186kg.This extraction amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 80% the time, add the 30kg deionized water to trapped fluid, continue micro-filtration, finally obtain the 210kg micro-filtrate, this micro-filtrate is put into the low temperature concentrator, under 70 ℃ of conditions, obtain the 53kg concentrate, be disinfectant.Stoste through quality testing qualified after, can be canned, packing, become disinfectant products.
Embodiment 5:
Choose gall nut, Radix Isatidis, alumen, the honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, the myrobalan pulverizes respectively, particle diameter is controlled at 30 orders, prepare burden according to the kind quantity of producing prescription then, gall nut 4.5kg, Radix Isatidis 1.5kg, alumen 0.8kg, honeysuckle rattan 1.2kg, rheum officinale 0.8kg, Schisandra sphenanthera Rehd.et WilS 0.6kg, myrobalan 0.6kg, after mixing, add in the traditional Chinese medicine extraction jar, add the 60kg running water to this extractor, heating was boiled 30 minutes, emitted extract 48kg in basin, added the 48kg running water in the traditional Chinese medicine extraction jar again, heating was boiled 20 minutes, emit secondary raffinate 45kg, merge and put into basin, extracted twice liquid merges the back and amounts to 93kg.This extraction amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 50% the time, add the 30kg deionized water to trapped fluid, continue micro-filtration, finally obtain the 120kg micro-filtrate, this micro-filtrate is put into the low temperature concentrator, under 55 ℃ of conditions, obtain the 30kg concentrate, be disinfectant.Stoste through quality testing qualified after, can be canned, packing, become disinfectant products.
Claims (2)
1. environmental type disinfectant is characterized in that disinfectant is made up of gall nut, Radix Isatidis, alumen, honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, myrobalan, and their mass fraction is respectively
Gall nut 45%～50%
Radix Isatidis 10%～15%
Alumen 8%～12%
Honeysuckle rattan 8%～12%
Rheum officinale 5%～8%
Schisandra sphenanthera Rehd.et WilS 4%～6%
The myrobalan 4%～6%
2. the preparation method of an environmental type disinfectant as claimed in claim 1 is characterized in that preparation process is as follows:
(1) choose gall nut, Radix Isatidis, alumen, honeysuckle rattan, rheum officinale, Schisandra sphenanthera Rehd.et WilS, myrobalan and pulverize respectively, particle diameter is controlled at 30～60 orders, prepares burden according to mass fraction, in the traditional Chinese medicine extraction of packing into after the mixing jar, then
(2) add the water of 6～12 times of quality of material in jar, heating was boiled 30～50 minutes, emitted extract in basin, added the water of 4～8 times of quality of material again, and heating was boiled 20～40 minutes, emitted extract, and secondary raffinate is merged, then
(3) amalgamation liquid is put into the ceramic membrane micro-filtration of 0.2 μ m, when the trapped fluid micro-filtration to the extract quality 50%～80% the time, add the deionized water of 3 times of quality of material to trapped fluid, continue micro-filtration, again will
(4) micro-filtrate that obtains is put into the low temperature enrichment facility, under 55 ℃～70 ℃ conditions, is concentrated into 25% of micro-filtrate volume, and the concentrate that obtains is thimerosal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410024093 CN1579169A (en) | 2004-05-17 | 2004-05-17 | Environment-protection infactant and its making method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410024093 CN1579169A (en) | 2004-05-17 | 2004-05-17 | Environment-protection infactant and its making method |
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| Publication Number | Publication Date |
|---|---|
| CN1579169A true CN1579169A (en) | 2005-02-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410024093 Pending CN1579169A (en) | 2004-05-17 | 2004-05-17 | Environment-protection infactant and its making method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102113524A (en) * | 2010-12-30 | 2011-07-06 | 戴锐 | Chinese medicinal disinfectant |
| CN102422845A (en) * | 2011-10-24 | 2012-04-25 | 辽宁禾丰牧业股份有限公司 | Chlorine-containing solid disinfectant for livestock and poultry houses |
| CN104524021A (en) * | 2015-01-27 | 2015-04-22 | 姜明一 | Disinfectant for clinical laboratories and preparation method |
| CN109497106A (en) * | 2018-11-26 | 2019-03-22 | 江西新世纪民星动物保健品有限公司 | A kind of preparation method of foamaseptic |
-
2004
- 2004-05-17 CN CN 200410024093 patent/CN1579169A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102113524A (en) * | 2010-12-30 | 2011-07-06 | 戴锐 | Chinese medicinal disinfectant |
| CN102422845A (en) * | 2011-10-24 | 2012-04-25 | 辽宁禾丰牧业股份有限公司 | Chlorine-containing solid disinfectant for livestock and poultry houses |
| CN104524021A (en) * | 2015-01-27 | 2015-04-22 | 姜明一 | Disinfectant for clinical laboratories and preparation method |
| CN109497106A (en) * | 2018-11-26 | 2019-03-22 | 江西新世纪民星动物保健品有限公司 | A kind of preparation method of foamaseptic |
| CN109497106B (en) * | 2018-11-26 | 2021-05-18 | 江西新世纪民星动物保健品有限公司 | Preparation method of foam disinfectant |
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