CN105724453A - Environment-friendly antibacterial agent and preparation method thereof - Google Patents
Environment-friendly antibacterial agent and preparation method thereof Download PDFInfo
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- CN105724453A CN105724453A CN201610138392.7A CN201610138392A CN105724453A CN 105724453 A CN105724453 A CN 105724453A CN 201610138392 A CN201610138392 A CN 201610138392A CN 105724453 A CN105724453 A CN 105724453A
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- environmental protection
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- Agronomy & Crop Science (AREA)
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- Natural Medicines & Medicinal Plants (AREA)
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Abstract
The invention discloses an environment-friendly antibacterial agent. The environment-friendly antibacterial agent comprises, by weight, 20-50 parts of pericarp, 40-50 parts of plant-based raw material and 0.2-1 part of crosslinking agent, wherein the crosslinking agent is calcium chloride and magnesium chloride. The invention further discloses a preparation method of the environment-friendly antibacterial agent. The environment-friendly antibacterial agent prepared by the method is efficient, nontoxic, quick in action, wide in spectrum, high in stability, and the like.
Description
Technical field
The present invention relates to water-treatment technology field, refer in particular to a kind of environmental protection antibacterial and preparation method.
Background technology
In prior art, conventional water treatment biocide mainly has two classes, oxidative bactericide and non-oxidative bactericide.Wherein oxidative bactericide is typically all stronger oxidant, such as liquid chlorine, hypochlorite, chlorinated isocyanurates, bromo glycolylurea and chlorine dioxide etc..Have a disadvantage in that: the microorganism that this series bactericidal agent can make some and metabolism in microorganism have the enzyme of substantial connection that oxidation occurs and kill in water body, also water-supply pipeline can be caused certain corrosiveness while the quick killing microorganisms of stronger oxidisability, if dosage exceeds standard, arrive running water pipe Terminal water oxidizer residual too much, certain infringement can be caused to resident is healthy.
Non-oxidative bactericide is generally synthetics, such as chlorophenols, organosulfur compound, isothiazolone and glutaraldehyde etc..Have a disadvantage in that: the mechanism of action of this series bactericidal agent is to destroy the duplication of microprotein by chemical action and reach bactericidal effect.If this series bactericidal agent content exceeds standard also can affect the protein of human body, health be will also result in bigger harm.
In view of this, the present invention proposes a kind of environmental protection antibacterial overcoming described defect and preparation method, and this case thus produces.
Summary of the invention
It is an object of the invention to provide a kind of efficient, nontoxic, quick-acting, environmental protection antibacterial that wide spectrum, stability are strong and preparation method, it is adaptable in water purification field.
For reaching above-mentioned purpose, the solution of the present invention is:
A kind of environmental protection antibacterial, is formed by following components: peel 20-50 part, plant base raw material 40-50 part, cross-linking agent 0.2-1 part by weight ratio, and cross-linking agent is calcium chloride and magnesium chloride.
Further, described peel is the one in peel of Citrus reticulata Blanco or Fericarpium Citri Limoniae, or both any proportioning mixing.
Further, described peel is Fericarpium Citri Limoniae.
Further, described plant base raw material is the one in Rhizoma Coptidis, Radix Glycyrrhizae, Radix Rumicis, Flos Lonicerae, Herba Artemisiae Annuae, Cortex Phellodendri or Folium Artemisiae Argyi, or both any of the above proportioning mixing.
Further, described cross-linking agent is calcium chloride and magnesium chloride powder 1:1 by weight ratio mixing.
A kind of environmental protection Antibacterial agent preparation method, comprises the following steps:
One, after plant base raw material rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 34-70% by above-mentioned serosity addition mass concentration, 40-60oStir 3-6h under C, be filtrated to get extracting solution A；
Three, after peel rinsed clean, shred addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 40-60oStir 1-2h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, be then sequentially added in liquor B mass concentration be the ethanol of 80-95%, mass concentration be the calcium chloride of 0.1-2% and magnesium chloride mixture solution and extracting solution A, 60-80oStir 2-4h under C and obtain colloid solution；
Four, by above-mentioned colloid solution through vacuum filtration, dry, obtain environmental protection antibacterial.
Further, described peel is the one in peel of Citrus reticulata Blanco or Fericarpium Citri Limoniae, or both any proportioning mixing.
Further, described peel is Fericarpium Citri Limoniae.
Further, described plant base raw material is the one in Rhizoma Coptidis, Radix Glycyrrhizae, Radix Rumicis, Flos Lonicerae, Herba Artemisiae Annuae, Cortex Phellodendri or Folium Artemisiae Argyi, or both any of the above proportioning mixing.
Further, described cross-linking agent is calcium chloride and magnesium chloride powder 1:1 by weight ratio mixing.
After using such scheme, environmental type antibacterial prepared by the present invention, there is the features such as efficient, nontoxic, quick-acting, wide spectrum and stability, be applied to water and process sterilization the most effectively sterilization and will not be detrimental to health.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment one
A kind of environmental protection Antibacterial agent preparation method, comprises the following steps:
One, after Folium Artemisiae Argyi rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 40% by above-mentioned serosity addition mass concentration, 40oStir 3h under C, be filtrated to get extracting solution A；
Three, shred after orange peel rinsed clean, addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 50oStir 1h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, in liquor B, be then sequentially added into ethanol that mass concentration is 80%, mass concentration be 0.1% calcium chloride and magnesium chloride mixture solution and extracting solution A, 60oStir 2h under C and obtain colloid solution；
Four, by above-mentioned colloid solution through vacuum filtration, dry, finally give environmental protection antibacterial.
The environmental protection antibacterial prepared by said method, is formed by weight ratio by following components: orange peel 40 parts, Folium Artemisiae Argyi 59.5 parts, calcium chloride and 0.5 part of magnesium chloride.
After tested: adding 0.5g environmental type antibacterial in 100ml concentration known staphylococcus aureus solution, stand 60min after rocking uniformly, after taking process, solution carries out microorganism culturing test (38oC 24h), antibiotic rate is 68.5%.
Embodiment two
A kind of environmental protection Antibacterial agent preparation method, comprises the following steps:
One, after Radix Rumicis rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 45% by above-mentioned serosity addition mass concentration, 40oStir 4h under C, be filtrated to get extracting solution A；
Three, shred after Fericarpium Citri Limoniae rinsed clean, addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 40oStir 2h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, in liquor B, be then sequentially added into ethanol that mass concentration is 85%, mass concentration be 0.1% calcium chloride and magnesium chloride mixture solution and extracting solution A, 60oStir 2h under C and obtain colloid solution；
Four, by above-mentioned colloid solution through vacuum filtration, dry, finally give environmental type antibacterial.
The environmental protection antibacterial prepared by said method, is formed by weight ratio by following components: Fericarpium Citri Limoniae 50 parts, Radix Rumicis 49.6 parts, calcium chloride and 0.4 part of magnesium chloride.
After tested: adding 0.5g environmental type antibacterial b in 100ml concentration known staphylococcus aureus solution, stand 60min after rocking uniformly, after taking process, solution carries out microorganism culturing test (38oC 24h), antibiotic rate is 82.7%.
Embodiment three
A kind of environmental protection Antibacterial agent preparation method, comprises the following steps:
One, after Folium Artemisiae Argyi and Radix Rumicis rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 40% by above-mentioned serosity addition mass concentration, 40oStir 3h under C, be filtrated to get extracting solution A；
Three, shred after orange peel and Fericarpium Citri Limoniae rinsed clean, addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 50oStir 1h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, in liquor B, be then sequentially added into ethanol that mass concentration is 80%, mass concentration be 0.1% calcium chloride and magnesium chloride mixture solution and extracting solution A, 60oStir 2h under C and obtain colloid solution；
Three, by above-mentioned colloid solution through vacuum filtration, dry, finally give environmental type antibacterial.
The environmental protection antibacterial prepared by said method, is formed by weight ratio by following components: Fericarpium Citri Limoniae 40 parts, orange peel 10 parts, Radix Rumicis 25 parts, Folium Artemisiae Argyi 24.3 parts, calcium chloride and 0.7 part of magnesium chloride.
After tested: adding 0.5g environmental type antibacterial in 100ml concentration known staphylococcus aureus solution, stand 60min after rocking uniformly, after taking process, solution carries out microorganism culturing test (38oC24h), antibiotic rate is 99.9%.
Embodiment four
A kind of environmental protection Antibacterial agent preparation method, comprises the following steps:
One, after Flos Lonicerae, Radix Glycyrrhizae and Folium Artemisiae Argyi rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 40% by above-mentioned serosity addition mass concentration, 40oStir 3h under C, be filtrated to get extracting solution A；
Three, shred after orange peel and Fericarpium Citri Limoniae rinsed clean, addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 60oStir 1h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, in liquor B, be then sequentially added into ethanol that mass concentration is 80%, mass concentration be 0.1% calcium chloride and magnesium chloride mixture solution and extracting solution A, 60oStir 2h under C and obtain colloid solution；
Four, by above-mentioned colloid solution through vacuum filtration, dry, finally give environmental type antibacterial.
The environmental protection antibacterial prepared by said method, is formed by weight ratio by following components: Fericarpium Citri Limoniae 20 parts, orange peel 25 parts, Flos Lonicerae 35 parts, 10 parts of Radix Glycyrrhizae, Folium Artemisiae Argyi 9 parts, calcium chloride and 1 part of magnesium chloride.
After tested: adding 0.5g environmental type antibacterial d in 100ml concentration known staphylococcus aureus solution, stand 60min after rocking uniformly, after taking process, solution carries out microorganism culturing test (38oC
24h), antibiotic rate is 99.9%.
Below for antibacterial effect of the present invention test tables of data: test condition: adding 0.5g antimicrobial component in 100ml concentration known staphylococcus aureus solution, stand 60min after rocking uniformly, after taking process, solution carries out microorganism culturing test (38oC 24h).
Upper described the preferred embodiments of the present invention that are only, not the restriction to this case design, all equivalent variations done according to the design key of this case, each fall within the protection domain of this case.
Claims (9)
1. an environmental protection antibacterial, it is characterised in that: being formed by weight ratio by following components: peel 20-50 part, plant base raw material 40-50 part, cross-linking agent 0.2-1 part, cross-linking agent is calcium chloride and magnesium chloride.
2. a kind of environmental protection antibacterial as claimed in claim 1, it is characterised in that: described peel is the one in peel of Citrus reticulata Blanco or Fericarpium Citri Limoniae, or both any proportioning mixing.
3. a kind of environmental protection antibacterial as claimed in claim 2, it is characterised in that: described peel is Fericarpium Citri Limoniae.
4. a kind of environmental protection antibacterial as claimed in claim 1, it is characterised in that: described plant base raw material is the one in Rhizoma Coptidis, Radix Glycyrrhizae, Radix Rumicis, Flos Lonicerae, Herba Artemisiae Annuae, Cortex Phellodendri or Folium Artemisiae Argyi, or both any of the above proportioning mixing.
5. a kind of environmental protection antibacterial as claimed in claim 1, it is characterised in that: described cross-linking agent is calcium chloride and magnesium chloride powder 1:1 by weight ratio mixing.
6. an environmental protection Antibacterial agent preparation method, it is characterised in that: comprise the following steps:
One, after plant base raw material rinsed clean, grind to form serosity；
Two, it is the ethanol solution of 34-70% by above-mentioned serosity addition mass concentration, 40-60oStir 3-6h under C, be filtrated to get extracting solution A；
Three, after peel rinsed clean, shred addition 0.1M HCl solution, peel and addition HCl 1:10 by weight ratio, 40-60oStir 1-2h under C, be filtered to remove filtering residue after reaction completely, obtain liquor B, be then sequentially added in liquor B mass concentration be the ethanol of 80-95%, mass concentration be the calcium chloride of 0.1-2% and magnesium chloride mixture solution and extracting solution A, 60-80oStir 2-4h under C and obtain colloid solution；
Four, by above-mentioned colloid solution through vacuum filtration, dry, obtain environmental protection antibacterial.
7. a kind of environmental protection Antibacterial agent preparation method as claimed in claim 6, it is characterised in that: described peel is the one in peel of Citrus reticulata Blanco or Fericarpium Citri Limoniae, or both any proportioning mixing.
8. a kind of environmental protection Antibacterial agent preparation method as claimed in claim 7, it is characterised in that: described peel is Fericarpium Citri Limoniae.
9. a kind of environmental protection Antibacterial agent preparation method as claimed in claim 6, it is characterised in that: described plant base raw material is the one in Rhizoma Coptidis, Radix Glycyrrhizae, Radix Rumicis, Flos Lonicerae, Herba Artemisiae Annuae, Cortex Phellodendri or Folium Artemisiae Argyi, or both any of the above proportioning mixing.
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| CN201610138392.7A CN105724453A (en) | 2016-03-11 | 2016-03-11 | Environment-friendly antibacterial agent and preparation method thereof |
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| CN201610138392.7A CN105724453A (en) | 2016-03-11 | 2016-03-11 | Environment-friendly antibacterial agent and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106865652A (en) * | 2017-04-11 | 2017-06-20 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod water quality cleansing agent and preparation method |
| CN106927537A (en) * | 2017-04-12 | 2017-07-07 | 明光市国星凹土有限公司 | A kind of river course concave convex rod purification of water quality bag and preparation method |
| CN107141408A (en) * | 2017-06-12 | 2017-09-08 | 厦门建霖健康家居股份有限公司 | A kind of antibacterial polymer and preparation method thereof |
| CN107161489A (en) * | 2017-06-21 | 2017-09-15 | 芜湖蓝天工程塑胶有限公司 | Composite antibacterial makrolon crisper and preparation method thereof |
| CN108912356A (en) * | 2018-06-06 | 2018-11-30 | 苏州先蚕丝绸有限公司 | Anti-bacteria wet keeping degradation porous silk protein gel preservative film and preparation method and application |
| CN115110313A (en) * | 2021-07-13 | 2022-09-27 | 南通帝沙纺织有限公司 | Preparation method of whitening antibacterial finishing fabric and whitening antibacterial finishing fabric |
| CN117243348A (en) * | 2023-09-08 | 2023-12-19 | 湖北薯芋产业技术研究院有限公司 | Processing method of sweet potato stem tip prefabricated vegetable |
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| CN1613325A (en) * | 2004-09-20 | 2005-05-11 | 南开大学 | Natural lemon antiseptics and preparation thereof |
| CN101623010A (en) * | 2009-08-03 | 2010-01-13 | 青岛星牌作物科学有限公司 | Botanical fungicide synergistic agent, extracting technique and application thereof in agricultural fungicide |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106865652A (en) * | 2017-04-11 | 2017-06-20 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod water quality cleansing agent and preparation method |
| CN106927537A (en) * | 2017-04-12 | 2017-07-07 | 明光市国星凹土有限公司 | A kind of river course concave convex rod purification of water quality bag and preparation method |
| CN107141408A (en) * | 2017-06-12 | 2017-09-08 | 厦门建霖健康家居股份有限公司 | A kind of antibacterial polymer and preparation method thereof |
| CN107161489A (en) * | 2017-06-21 | 2017-09-15 | 芜湖蓝天工程塑胶有限公司 | Composite antibacterial makrolon crisper and preparation method thereof |
| CN108912356A (en) * | 2018-06-06 | 2018-11-30 | 苏州先蚕丝绸有限公司 | Anti-bacteria wet keeping degradation porous silk protein gel preservative film and preparation method and application |
| CN115110313A (en) * | 2021-07-13 | 2022-09-27 | 南通帝沙纺织有限公司 | Preparation method of whitening antibacterial finishing fabric and whitening antibacterial finishing fabric |
| CN117243348A (en) * | 2023-09-08 | 2023-12-19 | 湖北薯芋产业技术研究院有限公司 | Processing method of sweet potato stem tip prefabricated vegetable |
| CN117243348B (en) * | 2023-09-08 | 2024-04-16 | 湖北薯芋产业技术研究院有限公司 | Processing method of sweet potato stem tip prefabricated vegetable |
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Address after: The North Industrial Zone of Jimei Tianfeng road Xiamen City, Fujian province 361021 No. 69 Applicant after: Xiamen Jian Lin health home Limited by Share Ltd Address before: The North Industrial Zone of Jimei Tianfeng road Xiamen City, Fujian province 361021 No. 69 Applicant before: Xiamen Runner Industrial Corporation |
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Effective date of registration: 20171220 Address after: 361000 Fujian Province, Xiamen city Tongan Industrial Zone Siming Park No. 305 Applicant after: Xiamen Bailin water purification technology Co. Ltd. Address before: The North Industrial Zone of Jimei Tianfeng road Xiamen City, Fujian province 361021 No. 69 Applicant before: Xiamen Jian Lin health home Limited by Share Ltd |
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Application publication date: 20160706 |