CN1335390A - Method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium - Google Patents

Method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium Download PDF

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Publication number
CN1335390A
CN1335390A CN 01128527 CN01128527A CN1335390A CN 1335390 A CN1335390 A CN 1335390A CN 01128527 CN01128527 CN 01128527 CN 01128527 A CN01128527 A CN 01128527A CN 1335390 A CN1335390 A CN 1335390A
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China
Prior art keywords
black liquor
nutriment
aqueous solution
edible fungus
fungus culturing
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CN 01128527
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Chinese (zh)
Inventor
阮键华
新阳
王雄
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Individual
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Individual
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Priority to CN 01128527 priority Critical patent/CN1335390A/en
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Abstract

The papermaking black liquor of soda pulp is mixed with coagulant aid, curing agent and flucculant through stirring to separate its organic matter, inorganic salt and other nutrient matters. The nutrient matters are dewatered and mixed with proper amount of sawdust, plant straw, cane sugar, bran, gypsum, lime or calcium carbonate, etc. to produce the edible fungi culturing medium. The present invention is simple, high in effect, and can utilize black liquor to avoid its environmental pollution.

Description

A kind of method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium
Technical field
The present invention relates to a kind of method of extracting black paper-making liquid of alkali pulping nutriment compounding edible fungus culturing base-material, belong to the regeneration class of slurrying alkali lye.
Background technology
Present pulping back liquor generally all is directly to enter rivers, cause serious environmental to pollute, simultaneously, organism such as the xylogen that contains in the black liquor, part Mierocrystalline cellulose, organic acid sodium salt, polyose and a large amount of carbon, hydrogen, sulphur, nitrogen, sodium element and various inorganic salts also enter rivers thereupon, both contaminate environment, cause organism and inorganics to run off again, can not regeneration; In fact, edible fungus culturing is needed just for the nutrient that organism and various inorganic salts contained such as contained xylogen, Mierocrystalline cellulose, polyose in the black liquor, and domestic technique is not mature enough in this regard at present, can not really develop black liquor and administer black liquor pollution.
Summary of the invention
The object of the present invention is to provide a kind of extraction black liquor nutriment material, the method for compounding edible fungus culturing base-material is carried out Edible Fungi thereby make full use of black liquor nutriment material, avoids black liquor pollution simultaneously.Particular content of the present invention is: the boiling slurry carries out the slurries separation after rotary spherical digester is discharged, the alkalescence black liquor is behind fiber recovery, preliminary sedimentation, utilize volume pump that black liquor is promoted in the black liquor dosing reaction tank, successively drop into coagulant aids, solidifying agent and flocculation agent, and stir, organism in the black liquor, the curing of inorganic salts nutriment material are separated out, and these nutriment materials are after processed, and its water ratio is 60~70%; The compound method of edible fungus culturing base-material is wood chip or the plant straw bits that the requirement of cultivation base-material are equipped with its quality 25~35% in water ratio is 60~70% nutriment material according to different edible mushroomss, selectivity is equipped with suitable amount of sucrose, wheat skin, gypsum, nitrogenous substances, lime or lime carbonate simultaneously, regulate pH value to prescribed value, the cultivation base-material of edible mushrooms of different varieties; Described coagulant aids is wilkinite or gelatine, and described solidifying agent is a dilute sulphuric acid, and described flocculation agent is sodium polyacrylate or polyacrylamide or acrylamide; Described coagulant aids is the aqueous solution of 1~20% concentration, and described solidifying agent is the aqueous solution of 5~30% concentration, and described flocculation agent is the aqueous solution of 0.1~1% concentration.In the leaching process of pulping back liquor nutriment, the mass ratio of black liquor and the coagulant aids aqueous solution, aqueous solution of curing agent and flocculant aqueous solution is respectively 1: 0.01~0.1,1: 0.05~0.3,1: 0.01~0.2.
Extract nutriment material in the black liquor, press mass ratio and drop into coagulant aids, need to stir through 2~5 minutes, drop into solidifying agent again, stirred 3~10 minutes, drop into flocculation agent at last, stirred 3~10 minutes, black liquor promptly solidifies nutriment materials such as separating out xylogen, Mierocrystalline cellulose, gets final product through processed.
Key of the present invention is that the coagulant aids that drops into can promote when extracting black liquor nutriment that the nutriment material solidifies, gathers in the black liquor, can also adjust the trophic structure of base-material when separating out nutriment material, compounding edible fungus culturing base-material; The solidifying agent that drops into, flocculation agent also must keep the useful matter in the black liquor not to be destroyed except can successful curing separating out in the black liquor the nutriment material.These technical characterstics have determined the above medicament of necessary use or similar with it medicament.
The present invention compared with prior art, it is not the simple black liquor treatment that carries out, and is worth but develop it at the composition of black liquor, reaches the effect of administering black liquor pollution simultaneously.In sum, technology of the present invention is simple, processing ease, and running cost is low, and effect is remarkable, both can develop value, the creation economic benefit of black liquor, has effected a radical cure black liquor pollution again, turns waste into wealth, and is applicable to the alkaline process papermaking enterprise of various scales.
The specific embodiment
Embodiment 1:
Under 30 ℃ of temperature, in the reed pulp black liquor 1000kg of 8 Baume degrees, PH=13, add dense Degree is 5% bentonite solution 10kg, stirs 3 minutes; Add afterwards concentration and be 5% rare Sulfuric acid solution 50kg stirred 2 minutes; Add again concentration and be 0.5% polyacrylamide solution 50kg, black liquor namely solidify and separate out cotton shape solid nutriment material. Solid matter and supernatant are thorough Separate, it is dark brown transparent that supernatant is. Solid nutriment material moisture content after press filtration is 60%, matter Amount is 400kg. Again to the oak wood chip that wherein adds its quality 26% and an amount of brown sugar, wheat Skin, urea, calcium superphosphate, gypsum; Add at last an amount of lime, regulate its pH value to 8, After processing, routine namely can be used as the cultivation base-material of mushroom.
Embodiment 2
Under 30 ℃ of temperature, in the reed pulp black liquor 1000kg of 10 Baume degrees, PH=12, add Concentration is 10% gelatine solution 15kg, stirs 3 minutes; Add afterwards concentration and be 10% Dilution heat of sulfuric acid 60kg stirred 2 minutes; Add again concentration and be 1% polyacrylamide solution 30kg, black liquor namely solidify and separate out cotton shape solid nutriment material. Solid matter and supernatant are thorough Separate, it is dark brown transparent that supernatant is. Solid nutriment material moisture content after press filtration is 60%, matter Amount is 412kg. Again to the straw bits that wherein add its quality 30% and an amount of brown sugar, wheat skin, Ammonium sulfate, calcium superphosphate, gypsum add an amount of calcium carbonate at last, regulate its pH value to 8, After processing, routine namely can be used as the cultivation base-material of mushroom.
Embodiment 3
Under 30 ℃ of temperature, in the pulp black liquor 1000kg of 14 Baume degrees, PH=14, add Concentration is 20% gelatine solution 20kg, stirs 3 minutes; Add afterwards concentration and be 20% Dilution heat of sulfuric acid 70kg stirred 2 minutes; Add again concentration and be 1% sodium polyacrylate solution 25kg, black liquor namely solidify and separate out cotton shape solid nutriment material. Solid matter and supernatant are thorough Separate, it is dark brown transparent that supernatant is. Solid nutriment material moisture content after press filtration is 60%, matter Amount is 438kg. Again to the Quercus acutissima wood chip that wherein adds its quality 30% and an amount of brown sugar, wheat Skin, soybean, calcium superphosphate, gypsum add an amount of calcium carbonate at last, regulate its pH value and arrive 8, after processing, routine namely can be used as the cultivation base-material of white fungus.

Claims (2)

1, a kind of method of extracting black paper-making liquid of alkali pulping nutriment compounding edible fungus culturing base-material is characterized in that:
The extracting method of A, described pulping back liquor nutriment is successively to drop into coagulant aids, solidifying agent and flocculation agent in black liquor, and stir, organism in the black liquor, the curing of inorganic salts nutriment material are separated out, and these nutriment materials are after processed, and its water ratio is 60~70%;
The compound method of B, described edible fungus culturing base-material is to be wood chip or the plant straw bits that 60~70% nutriment material is equipped with its quality 25~35% to water ratio, selectivity is equipped with suitable amount of sucrose, wheat skin, gypsum, nitrogenous substances, lime or lime carbonate simultaneously, regulate pH value to prescribed value, the cultivation base-material of edible mushrooms of different varieties;
C, described coagulant aids are wilkinite or gelatine, and described solidifying agent is a dilute sulphuric acid, and described flocculation agent is sodium polyacrylate or polyacrylamide or acrylamide;
D, described coagulant aids are the aqueous solution of 1~20% concentration, and described solidifying agent is the aqueous solution of 5~30% concentration, and described flocculation agent is the aqueous solution of 0.1~1% concentration.
2, a kind of method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium according to claim 1, it is characterized in that in the leaching process of described pulping back liquor nutriment, the mass ratio of black liquor and the coagulant aids aqueous solution, aqueous solution of curing agent and flocculant aqueous solution is respectively 1: 0.01~0.1,1: 0.05~0.3,1: 0.01~0.2.
CN 01128527 2001-08-04 2001-08-04 Method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium Pending CN1335390A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 01128527 CN1335390A (en) 2001-08-04 2001-08-04 Method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 01128527 CN1335390A (en) 2001-08-04 2001-08-04 Method of extracting nutrients from papermaking black liquor and compounding edible fungus culturing medium

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CN1335390A true CN1335390A (en) 2002-02-13

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100381041C (en) * 2004-01-19 2008-04-16 魏勇 Plants cultivation slurry and its production method
CN103159513A (en) * 2013-03-24 2013-06-19 王天喜 Method for producing biological bactericide by using paper-making wastewater
CN104909941A (en) * 2015-07-06 2015-09-16 合肥福泉现代农业科技有限公司 Water retention efficient culture medium for pholiota nameko and preparation method
CN104987179A (en) * 2015-06-16 2015-10-21 王金生 Agrocybe cylindracea cultivation medium
CN106316577A (en) * 2016-08-09 2017-01-11 全椒县香妃农业专业合作社 Shiitake mushroom collagen culture medium prepared from papermaking black liquor
CN110495351A (en) * 2019-09-20 2019-11-26 黔西南州丰宇农业发展有限公司 A kind of cultivation of agaricus bisporus matrix and preparation method thereof
CN112385477A (en) * 2020-11-20 2021-02-23 山东沃尔美肥业有限公司 Secondary fruiting method of needle mushrooms

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100381041C (en) * 2004-01-19 2008-04-16 魏勇 Plants cultivation slurry and its production method
CN103159513A (en) * 2013-03-24 2013-06-19 王天喜 Method for producing biological bactericide by using paper-making wastewater
CN104987179A (en) * 2015-06-16 2015-10-21 王金生 Agrocybe cylindracea cultivation medium
CN104909941A (en) * 2015-07-06 2015-09-16 合肥福泉现代农业科技有限公司 Water retention efficient culture medium for pholiota nameko and preparation method
CN106316577A (en) * 2016-08-09 2017-01-11 全椒县香妃农业专业合作社 Shiitake mushroom collagen culture medium prepared from papermaking black liquor
CN110495351A (en) * 2019-09-20 2019-11-26 黔西南州丰宇农业发展有限公司 A kind of cultivation of agaricus bisporus matrix and preparation method thereof
CN112385477A (en) * 2020-11-20 2021-02-23 山东沃尔美肥业有限公司 Secondary fruiting method of needle mushrooms
CN112385477B (en) * 2020-11-20 2022-06-14 山东沃尔美肥业有限公司 Secondary fruiting method of needle mushrooms

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