CN1296555C - Biological pulping process for paper making - Google Patents

Biological pulping process for paper making Download PDF

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Publication number
CN1296555C
CN1296555C CNB2004100239108A CN200410023910A CN1296555C CN 1296555 C CN1296555 C CN 1296555C CN B2004100239108 A CNB2004100239108 A CN B2004100239108A CN 200410023910 A CN200410023910 A CN 200410023910A CN 1296555 C CN1296555 C CN 1296555C
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China
Prior art keywords
liquid
bio
spherical digester
raw material
active bio
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Expired - Fee Related
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CNB2004100239108A
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Chinese (zh)
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CN1683711A (en
Inventor
李书坤
马强
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huixin biological pulp and Paper Co.
Ma Qiang
Yongfa biological pulp and Paper Co.
Original Assignee
Dezhou Luping Yongfa Paper Making Co Ltd
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Application filed by Dezhou Luping Yongfa Paper Making Co Ltd filed Critical Dezhou Luping Yongfa Paper Making Co Ltd
Priority to CNB2004100239108A priority Critical patent/CN1296555C/en
Publication of CN1683711A publication Critical patent/CN1683711A/en
Application granted granted Critical
Publication of CN1296555C publication Critical patent/CN1296555C/en
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Abstract

The present invention relates to a biologically pulping process for making paper, which comprises a step of cutting off raw materials, a cooking step and subsequent steps. The present invention is characterized in that before cooking, active biological liquid is cultured, and partial cultured active biological liquid is sprayed on raw materials which are cut off until the raw materials are totally moistened; a spherical digester is placed, and simultaneously, partial active biological liquid is added to the spherical digester; after the spherical digester rotates for about 30 min, gas is introduced and the spherical digester is cooked. The present invention has the advantages of reasonable design, feasible technology, little biological strain quantity, short technological process time and little equipment investment, and is favorable to reduction of papermaking production cost. The cooked raw liquid can be reused, and does not need to be further treated.

Description

A kind of papermaking bio-pulping process
Technical field: the invention belongs to the paper technology scope, relate to a kind of bio-pulping process of paper industry.
Background technology: the history of existing centuries of paper industry, bigger development is arranged again in recent decades, still, its pulping process but develops slower, still acid-base methods that adopt more.The process of this slurrying not only needs to consume a large amount of acid, alkali, salt etc., paper cost height; And will discharge in a large number people, animal and the harmful waste water of crops, the cod index generally all reaches 2-3 ten thousand, and intractability is big, and environmental pollution is particularly very serious to phreatic pollution.The applicant had once applied for the patent of invention of " a kind of pulping Process for papermaking straw pulp " November calendar year 2001, application number is 01135183.7, this patent disclosure before boiling, carry out the bio-pulping process of biofermentation earlier, comparatively effectively overcome the existing drawback of sour subtraction pulping process.But, in this technology, raw material per ton need be with 1-3 kilogram biological inoculum in seal groove, under the what 10-30 degrees celsius anaerobic fermentation 1-10 days, not only need be big with the biological inoculum amount, the pulp preparing process time is long, and needs to build more fermentation tank, invest morely, be unfavorable for reducing the paper cost.In addition, the also not convenient usefulness of the stoste after its boiling also needs to carry out certain processing.
Summary of the invention: the objective of the invention is to have the existing above-mentioned drawback of biofermentation pulping process technology now, and a kind of improved papermaking bio-pulping process is provided for overcoming.This technology is to improve to realize on the basis of existing biofermentation pulping process technology, it comprises raw material, cut-out processing and boiling and subsequent handling thereof as forages such as wheat straw, straw, cotton stalk, bagasse and wood chip, it is characterized in that before boiling, carrying out earlier the cultivation of active bio liquid, after promptly in culture pond, adding water, admix brown sugar, maize flour and wheat face, add in lactic acid bacteria, fermentative microflora, the aspergillus flora one or more again, anaerobism was cultivated 5---7 days under the 20---45 degrees celsius; Earlier the cultured active bio liquid of part is sprayed on the raw material of handling through cut-out, all moistening to raw material, reinstall rotary spherical digester, in rotary spherical digester, add part active bio liquid simultaneously, treat that rotary spherical digester turned round cardinal principle after 30 minutes, boiling is carried out in ventilation again.
The cultivation of said active bio liquid, the weight portion proportioning of its water, brown sugar, maize flour, wheat face and biological inoculum can be: water 20000, brown sugar 8-12, maize flour 12-18, wheat face 12-18, biological inoculum 4-8.
Preferred weight portion proportioning is: water 20000, brown sugar 10, maize flour 15, wheat face 15, biological inoculum 5-6.
The weight portion proportioning of the active bio liquid of said raw material and spray and adding rotary spherical digester can be: raw material 1000, active bio liquid 2000-3000.
For further reducing the consumption of biological inoculum, reduce production costs said boiling, stoste after its boiling can play back to active bio liquid culture pond, mixes with former active bio nutrient solution, and moisturizing in the pond, to suitable, as the active bio nutrient solution use of inferior batch of material cooking with commercial weight.
For alleviating equipment corrosion, the long-time normal operation of protection equipment before the ventilation boiling, can add the ammoniacal liquor of a small amount of 1.5-2% or the urea of 2-4% in rotary spherical digester.
The present invention is reasonable in design, feasible process, and the biological inoculum consumption is little, and the technical process time is short, and equipment investment is few, helps reducing the paper cost, and the stoste after the boiling can be utilized again, need not to be for further processing.
The specific embodiment:
Embodiment 1: inject 20 tons in water to active bio liquid culture pond, admix 10 kilograms in brown sugar, 15 kilograms of maize flours, 15 kilograms in wheat face adds lactic acid bacteria 5-6 kilogram, and culture pond is sealed, anaerobism was cultivated 6 days under cardinal principle 30 degrees celsius, promptly made the active bio nutrient solution; Get 1 ton of above-mentioned active bio nutrient solution, spray 1 ton on the wheat straw forage that cut-out is handled well, and with the forage rotary spherical digester of packing into, other gets above-mentioned active bio nutrient solution and adds rotary spherical digester for 1.5 tons, opens the rotary spherical digester running 30 minutes substantially, makes forage be able to abundant enzymolysis; Fed the steam boiling then 3 hours, and promptly made papermaking magma, this papermaking magma is conventional defibrination, machine hand's preface through the rear portion, can copy the system toilet paper.
Embodiment 2: according to embodiment 1, wherein brown sugar is 8 kilograms, and maize flour is 12 kilograms, and the wheat face is 18 kilograms, and 8 kilograms of zymophytes were cultivated 5 days in 45 degrees centigrade of anaerobism of cardinal principle, and all the other are with embodiment 1.
Embodiment 3: according to embodiment 1, wherein brown sugar is 8 kilograms, and maize flour is 12 kilograms, and the wheat face is 18 kilograms, and 8 kilograms of zymophytes were cultivated 7 days in 20 degrees centigrade of anaerobism of cardinal principle, and all the other are with embodiment 1.
Embodiment 4: according to embodiment 1, wherein brown sugar is 12 kilograms, maize flour is 18 kilograms, the wheat face is 12 kilograms, 2 kilograms of lactic acid bacterias, 2 kilograms of fermentative microfloras, cultivated 7 days in 40 degrees centigrade of anaerobism of cardinal principle, other gets the active bio nutrient solution that adds rotary spherical digester is 2 tons, and digestion time is 4 hours, and all the other are with embodiment 1.
Embodiment 5: according to embodiment 1, wherein brown sugar is 10 kilograms, maize flour is 18 kilograms, the wheat face is 12 kilograms, 4 kilograms of fermentative microfloras, 2 kilograms of aspergillus floras, cultivated 7 days in 40 degrees centigrade of anaerobism of cardinal principle, other gets the active bio nutrient solution that adds rotary spherical digester is 1 ton, and digestion time is 2 hours, and all the other are with embodiment 1.
Embodiment 6: according to embodiment 1, the stoste after the boiling played back to active bio liquid culture pond, mixes with former active bio nutrient solution, and moisturizing in the pond, to suitable, as the active bio nutrient solution use of inferior batch of forage boiling with commercial weight.
Embodiment 7: according to embodiment 1, before the ventilation boiling, add the ammoniacal liquor of a small amount of 1.5-2% in rotary spherical digester.

Claims (5)

1, a kind of papermaking bio-pulping process, comprise that raw material cuts off processing and boiling and subsequent handling thereof, it is characterized in that before boiling, carrying out earlier the cultivation of active bio liquid, after promptly in culture pond, adding water, admix brown sugar, maize flour and wheat face, add biological inoculum again, anaerobism is cultivated and was obtained active bio liquid in 5-7 days under the 20-45 degrees celsius, and described biological inoculum is one or more in lactic acid bacteria, fermentative microflora, the aspergillus flora; Cultured active bio liquid is sprayed on the raw material through cutting off processing, all moistening to raw material, reinstall rotary spherical digester, in rotary spherical digester, add active bio liquid simultaneously, treat that the rotary spherical digester running is after 30 minutes, feed steam again and carry out boiling, the weight portion proportioning of described active bio liquid is: water: 20000, and brown sugar: 8-12, maize flour: 12-18, wheat face: 12-18, biological inoculum: 4-8.
2, papermaking bio-pulping process according to claim 1 is characterized in that the weight portion proportioning of described active bio liquid is: water: 20000, and brown sugar: 10, maize flour: 15, the wheat face: 15, biological inoculum: 5-6.
3, papermaking bio-pulping process according to claim 1 and 2 is characterized in that said raw material adds the active bio liquid weight portion proportioning of using in the rotary spherical digester with reaching of spray usefulness and is: raw material: 1000, and active bio liquid: 2000-3000.
4, papermaking bio-pulping process according to claim 1, it is characterized in that the liquid that raw material is leached is stoste after boiling, stoste is transported in the active bio liquid culture pond mixes with the original activity bio-culture solution, and moisturizing in the pond, reach the turnover balance, use as time active bio nutrient solution of batch material cooking then.
5,, before the boiling that it is characterized in that ventilating, in rotary spherical digester, add the ammoniacal liquor of raw material weight 1.5-2% or the urea of 2-4% according to claim 1,2 or 3 described papermaking bio-pulping process.
CNB2004100239108A 2004-04-12 2004-04-12 Biological pulping process for paper making Expired - Fee Related CN1296555C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2004100239108A CN1296555C (en) 2004-04-12 2004-04-12 Biological pulping process for paper making

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Application Number Priority Date Filing Date Title
CNB2004100239108A CN1296555C (en) 2004-04-12 2004-04-12 Biological pulping process for paper making

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CN1683711A CN1683711A (en) 2005-10-19
CN1296555C true CN1296555C (en) 2007-01-24

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101824771B (en) * 2009-06-13 2012-04-04 汇鑫生物浆纸股份有限公司 Production process of high-strength corrugated base paper
CN104130034A (en) * 2014-06-19 2014-11-05 临沂市清宇环境资源综合利用研究院 Method for producing fiber board and organic fertilizer by utilizing garden waste
CN107313278A (en) * 2017-07-12 2017-11-03 山西朱好古麻笺纸业有限公司 A kind of preparation method of the save-resistant numb writing paper of microorganism
CN107287973B (en) * 2017-07-14 2019-04-02 贵州册亨现代生态农业综合开发有限公司 A kind of smooth leaf paper mulberry rhizome and the compound method for preparing paper pulp of big straw skin

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1310258A (en) * 2001-03-16 2001-08-29 山东大学 Biological pretreatment process of preparing chemical mechanical straw pulp
CN1420229A (en) * 2001-11-15 2003-05-28 马强 Pulping Process for papermaking straw pulp

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1310258A (en) * 2001-03-16 2001-08-29 山东大学 Biological pretreatment process of preparing chemical mechanical straw pulp
CN1420229A (en) * 2001-11-15 2003-05-28 马强 Pulping Process for papermaking straw pulp

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Owner name: YONGFA BIOLOGICAL PAPER CO., LTD.

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