CN1258974C - Silkworm silk gland protection type dyestuff and process for making same - Google Patents
Silkworm silk gland protection type dyestuff and process for making same Download PDFInfo
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- CN1258974C CN1258974C CN 200410064826 CN200410064826A CN1258974C CN 1258974 C CN1258974 C CN 1258974C CN 200410064826 CN200410064826 CN 200410064826 CN 200410064826 A CN200410064826 A CN 200410064826A CN 1258974 C CN1258974 C CN 1258974C
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- protectant
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- pigment
- silk gland
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Abstract
The present invention relates to a silkworm silk gland protection type colorant and a preparation method thereof. The silkworm silk gland protection type colorant comprises non-poisonous organic biochromes and water. The present invention is characterized in that the colorant also comprises a silk gland protecting agent which comprises amino acid, dextrose and antibiotic, and the biochromes, the protecting agent and the water have the proportion range of 0.04% to 4% of the biochromes, 0.01% to 1% of the protecting agent and 95% to 99.95% of the water. The amino acid, the dextrose and the antibiotic respectively account for one third of the total quantity of the protecting agent, namely 1: 1: 1. The colorant of the present invention has no bad influence on the development of silkworms, but can enhance the self disease resisting capability of the silkworms, the yield of colorful cocoons is relatively high, 40.75kg of the colorful cocoons can be produced on one piece of paper with graines, and the preparation method can be easily mastered.
Description
Technical field
The present invention relates to a kind of colouring agent, be specifically related to a kind of colouring agent that makes domestic natural silk gland change color and preparation method thereof.
Background technology
The existing kind silk gland protein of silkworm is water white transparency, and the cocoon of bearing, silk are white.How to make domestic natural silk gland painted, bear motley cocoon, and put down by high temperature that still to keep its color behind the silk be the difficult problem of current silkworm industry scientific research.
Ground such as Gunma Prefecture, Japan have added chemical substance in the feed of artificial diet rearing silkworm, influence the intestines wall of silkworm and the pigment permeability of silk gland cell, make the practical production kind that does not possess pigment genetic control gene can spue coloured.
" Anhui agricultural science " magazine, 2002,30 (5) have delivered " research of silkworm natural colorful cocoon ", and this literary composition discloses in silkworm artificial feed or mulberry leaf and has added pigment, can make silkworm bear the method for chromatic cocoon.
Though said method can obtain the silk cocoon of cocoon such as Huang Hong system, also has some defectives:
Promptly chemical substance of Tian Jiaing or single pigment are grown silkworm certain harmful effect, causes weak, the hypoevolutism of silkworm body, is prone to big young silkworm, raise difficulty and strengthen, and the cocoon of bearing yields poorly.
Summary of the invention
In order to solve the problem that only adopts single pigment feeding technology to exist in the prior art; the present invention discloses a kind of silkworm silk gland protection type dyestuff and preparation method thereof, solves effectively with single pigment to add the problem that the silkworm rearing difficulty is big, cocoon yields poorly of eating and causing.
Technical scheme of the present invention: a kind of silkworm silk gland protection type dyestuff, it is characterized in that forming by non-toxic organic biochrome, water and sericterium protectant, the sericterium protectant is made up of amino acid, glucose and antibiotic, described amino acid, glucose and antibiotic, the three respectively accounts for 1/3rd of protectant total amount, is 1: 1: 1; The content ratio scope of pigment, protectant and water is:
Pigment 0.04%-4%, protectant 0.01%-1%, water 95%-99.95%.
Described antibiotic is that silkworm is used erythromycin.The optimum content ratio of described pigment, protectant and water is a pigment 0.9%, protectant 0.1%, water 99%.
A kind of preparation method of silkworm silk gland protection type dyestuff is characterized in that:
A. with pigment in the 0.04%-4% ratio be dissolved in≤60 ℃, ratio are in the warm boiling water or distilled water of 95%-99.5%;
B. add protectant in the 0.01%-1% ratio in solution, protectant is made up of amino acid, glucose and antibiotic, described amino acid, glucose and antibiotic, and the three respectively accounts for 1/3rd of protectant total amount, is 1: 1: 1; Make the dissolving of amino acid and glucose earlier, add silkworm again and use erythromycin, wherein the total amount of pigment, protectant and water is 100%.
Silkworm silk gland protection type dyestuff is a carrier with silkworm artificial feed or mulberry leaf, after silkworm is edible silkworm body resistance is strengthened, and pigment enters blood through canalis alimentarius simultaneously, enters sericterium from blood, makes silk painted, thereby makes the silkworm colored silk that spues.
Beneficial effect of the present invention: colouring agent of the present invention has no adverse effects to silkworm development, can also strengthen the resistance against diseases of silkworm body self on the contrary, and color cocoon output is higher relatively, average kind of the color cocoon 40.75Kg of production that opens, and preparation method is easy to grasp.
Embodiment
Pigment: select for use nontoxic organic-biological pigment as basic chromophore because of.As: acid fuchsin, basic yellow, neutral orange, methyl orchid etc., pigment accounts for the 0.04%-4% of colouring agent weight.
The sericterium protectant: silkworm is a more delicate life entity, and using any pigment to freshen food all has bad reaction to the silkworm body, and only reaction is strong and weak different.In order to allow the normal growth that silkworm can normal development, particularly sericterium, in colouring agent, add a certain amount of sericterium protectant, it accounts for the 0.01%-1% of colouring agent weight.Protectant contains amino acid, glucose and silkworm uses erythromycin, respectively accounts for 1/3rd of protectant total amount, promptly 1: 1: 1.
| The non-toxic organic biochrome | Protectant | Water | ||
| Silkworm is used erythromycin | Amino acid | Glucose | ||
| Acid fuchsin 3.5% | 0.3％ | 0.3％ | 0.3％ | 95.6％ |
| Basic yellow 3% | 0.25％ | 0.25％ | 0.25％ | 96.25％ |
| Neutral orange 2% | 0.2％ | 0.2％ | 0.2％ | 97.4％ |
| Methyl orchid 0.05% | 0.02％ | 0.02％ | 0.02％ | 99.944％ |
Silkworm silk gland protection type dyestuff each component percentage by weight example
The silkworm silk gland protection type dyestuff preparation method:
(1) water: with warm boiling water or distilled water, water temperature does not surpass 60 ℃, generally is advisable at 30-40 ℃.
(2) configuration sequence: earlier with the pigment of powdery warm dissolved in boiled water with 40 ℃, treat to add again after pigment dissolves fully the grape powder, amino acid, molten finishing of powdery after, put into silkworm after again and use erythromycin.
Prepare red domestic natural silk gland colouring agent embodiment 1:
1. get acid fuchsin 8g, the warm boiling water of putting into earlier about 200ml dissolves.
2. get amino acid 0.5g, glucose 0.5g dissolves with the warm boiling water about 200ml again.
3. the pigment, amino acid, the glucose that dissolve more than inciting somebody to action are poured in the container of 1000ml (1L).
4. the silkworm that adds 1 2ml 500mg is used erythromycin.
5. constant volume is mixed to 1000ml (being 1L), is haematochrome domestic natural silk gland colouring agent.This 1000ml colouring agent can make 2000-3000 silk gland painted.
Prepare blue look domestic natural silk gland colouring agent embodiment 2:
1. get the blue 0.4g of methyl, the warm boiling water of putting into earlier about 200ml dissolves.
2. get amino acid 0.05g, glucose 0.05g dissolves with the warm boiling water about 200ml again.
3. the pigment, amino acid, the glucose that dissolve more than inciting somebody to action are poured in the container of 1000ml (1L).
4. the silkworm that adds 1 2ml 500mg is used erythromycin.
5. constant volume is mixed to 1000ml (being 1L), is blue pigment domestic natural silk gland colouring agent.This 1000ml colouring agent can make 500-600 silk gland painted.
Claims (3)
1, a kind of silkworm silk gland protection type dyestuff, it is characterized in that forming by non-toxic organic biochrome, water and sericterium protectant, the sericterium protectant is made up of amino acid, glucose and antibiotic, described amino acid, glucose and antibiotic, the three respectively accounts for 1/3rd of protectant total amount, is 1: 1: 1; Described antibiotic is that silkworm is used erythromycin; The content ratio scope of pigment, protectant and water is: pigment 0.04%-4%, protectant 0.01%-1%, water 95%-99.95%.
2, silkworm silk gland protection type dyestuff according to claim 1, the content ratio that it is characterized in that described pigment, protectant and water is a pigment 0.9%, protectant 0.1%, water 99%.
3, a kind of preparation method of silkworm silk gland protection type dyestuff is characterized in that:
A. with pigment in the 0.04%-4% ratio be dissolved in≤60 ℃, ratio are in the warm boiling water or distilled water of 95%-99.5%;
B. add protectant in the 0.01%-1% ratio in solution, protectant is made up of amino acid, glucose and antibiotic, described amino acid, glucose and antibiotic, and the three respectively accounts for 1/3rd of protectant total amount, is 1: 1: 1; Make the dissolving of amino acid and glucose earlier, add antibiotic again, described antibiotic is that silkworm is used erythromycin; Wherein the total amount of pigment, protectant and water is 100%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410064826 CN1258974C (en) | 2004-09-30 | 2004-09-30 | Silkworm silk gland protection type dyestuff and process for making same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410064826 CN1258974C (en) | 2004-09-30 | 2004-09-30 | Silkworm silk gland protection type dyestuff and process for making same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1629391A CN1629391A (en) | 2005-06-22 |
| CN1258974C true CN1258974C (en) | 2006-06-14 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410064826 Expired - Fee Related CN1258974C (en) | 2004-09-30 | 2004-09-30 | Silkworm silk gland protection type dyestuff and process for making same |
Country Status (1)
| Country | Link |
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| CN (1) | CN1258974C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101285215B (en) * | 2008-06-12 | 2010-09-15 | 江苏苏豪国际集团股份有限公司 | Process for preparing yellow silk |
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2004
- 2004-09-30 CN CN 200410064826 patent/CN1258974C/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN1629391A (en) | 2005-06-22 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
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Owner name: INSTITUTE OF SERICULTURE, ANHUI ACADEMY OF AGRICU Free format text: FORMER OWNER: INSTITUTE OF SERICULTURE, ANHUI ACADEMY OF AGRICULTURAL SCIENCES; ANHUI PROVINCE SILKCO., LTD. Effective date: 20071026 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20071026 Address after: 230061 No. 15, Mount Holyoke Road, Hefei, Anhui Co-patentee after: Anhui Tian Cai silk Co., Ltd. Patentee after: Inst of Silkworm and Mulberry Tree, Anhui Academy of Agricultral Sciences Address before: 230061 No. 15, Mount Holyoke Road, Hefei, Anhui Co-patentee before: Anhui silk Limited by Share Ltd Patentee before: Inst of Silkworm and Mulberry Tree, Anhui Academy of Agricultral Sciences |
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| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060614 Termination date: 20130930 |