CN1191821C - Plastic self-viscose magnetically osmosiring ointment and its preparing process - Google Patents
Plastic self-viscose magnetically osmosiring ointment and its preparing process Download PDFInfo
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- CN1191821C CN1191821C CNB001130951A CN00113095A CN1191821C CN 1191821 C CN1191821 C CN 1191821C CN B001130951 A CNB001130951 A CN B001130951A CN 00113095 A CN00113095 A CN 00113095A CN 1191821 C CN1191821 C CN 1191821C
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Abstract
The present invention relates to an ointment with the functions of both medical therapy and magnetic therapy, which is prepared from glue stuff, magnetic powder and medicine stuff. Permanent magnet glue stuff is prepared by mixing glue stuff and magnetic powder according to the weight ratio of 1:1 to 5; the ointment is prepared by mixing permanent magnet glue stuff and medicine powder according to the weight ratio of 100:4 to 50. The glue stuff can be optionally selected from rubber glue stuff, polyvinyl chloride glue stuff and epoxy resin glue stuff; the magnetic powder can be optionally selected from ferric oxide magnetic powder stuff, strontium ferromagnetic powder stuff, iron cobalt nickel magnetic powder stuff, Neodymium-Iron-Boron magnetic powder stuff and barium ferromagnetic powder stuff; the medicine stuff can be optionally selected from medicines with the effects on removing dampness, alleviating pain, relieving inflammation, reliving pain, lowering blood pressure, treating hemorrhoid, treating clavus and relieving cataract. The ointment has the advantage that medicine and the permanent magnet glue suff are integrated.
Description
The invention belongs to the lamellar base material is the pharmaceutical product technical field of feature.
Ointment is a kind of liniment that people use always.Traditional ointment only contains spice, treats with the effective ingredient of spice.In recent years, occur a kind of magnetic subsides or magnetic that contains spice and permanent magnetism powder on the towel field and oozed ointment, in the spice treatment, also carried out magnetic therapy.For example, Chinese patent application file 90106092.5 discloses a kind of " rare-earth magnetic plaster ".This patent application is a kind of three-decker ointment that contains anti-delamination, magnetic medicine thin film and adhesive layer of magnetic powder, and preparation technology is complicated, and because the existence of adhesive layer makes magnetic medicine thin film can not contact skin, influences therapeutic effect.
The object of the present invention is to provide a kind of plastic self-viscose magnetically osmosiring ointment that magnetic medicine layer and adhesive layer are integrated.
The object of the present invention is achieved like this, a kind of plastic self-viscose magnetically osmosiring ointment, and it is mixed with by permanent magnetism sizing material and medicated powder powder, and its weight proportion is 100: (4-50).Wherein, the permanent magnetism sizing material is mixed and made into by sizing material and magnetic powder material, and its weight proportion is 1: (1-5) permanent magnetism sizing material and the spice structure that is integrated; The permanent magnetism sizing material is made up of sizing material and magnetic powder material, sizing material is from rubber size, the polrvinyl chloride sizing material, choose any one kind of them in the epoxy resin sizing material, the constituent of magnetic powder material is magnetic powder and additive, from the iron oxide magnetic powder, the strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, the NdFeB magnetic powder material, choose any one kind of them in the barium ferrum magnetic powder material, wherein the constituent of iron oxide magnetic powder is iron sesquioxide and additive Barium monoxide, zinc oxide, the constituent of strontium ferrum magnetic powder material is strontium ferrum magnetic powder and additive zinc oxide, strontium oxide, the constituent of rare earth ferrum,cobalt and nickel magnetic powder material is rare earth ferrum,cobalt and nickel magnetic powder and additive aluminium oxide cobalt oxide, nickel sesquioxide, the constituent of NdFeB magnetic powder material is NdFeB magnetic powder and additive ferroso-ferric oxide, Dineodymium trioxide, Borax, the constituent of barium ferrum magnetic powder material are barium ferrum magnetic powder and additive sulphuric acid barium, zinc oxide.
A, sizing material.The constituent of sizing material is macromolecular material, solvent, plasticizer, modifier.Sizing material can be chosen any one kind of them from following rubber size, polrvinyl chloride sizing material and epoxy resin sizing material.
The constituent and the weight proportion of sizing material are as follows:
(1) rubber size: rubber 10-30 gram, industrial naptha 50-100 gram, modifier 39.2-81.41 gram.Wherein the constituent of modifier and weight proportion are 40 order Colophonium powder 15-30 grams, 320 order zinc oxide 10-20 gram, vaseline 6-13 gram, liquid Paraffin 8-18 gram, sofril 0.05-0.11 gram, stearic acid 0.15-0.3 gram.
(2) polrvinyl chloride sizing material: polrvinyl chloride 10-20 gram, solvent dibutyl phthalate 25-50 gram, modifier 111-212 gram.Wherein, the constituent of modifier and weight proportion are: 40 order Colophonium powder 50-90 gram, 320 order zinc oxide 60-120 gram, Camphora 0 5-1 gram, enuatrol 0 5-1 gram.
(3) epoxy resin sizing material: epoxy resin 10-20 gram, plasticizer phthalic acid dibutyl ester 10-40 gram, modifier 7-14 gram.Wherein, modifier constituent and weight proportion are 40 order Colophonium powder 1-2 grams, 320 order zinc oxide 5-10 gram.
B, magnetic powder material.The constituent of magnetic powder material is magnetic powder and additive.The magnetic powder material is chosen any one kind of them from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material and barium ferrum magnetic powder material.
Magnetic powder material weight proportion is:
(1) iron oxide magnetic powder: granularity is a 0.5-3 μ m iron sesquioxide magnetic powder 50-150 gram; Additive 7 16 grams.The constituent of additive and weight proportion are Barium monoxide 48 gram zinc oxide 38 grams.
(2) strontium ferrum magnetic powder material: granularity is a 0.5-3 μ m strontium ferrum magnetic powder 80-120 gram; Additive 511 grams.Wherein the constituent of additive and weight proportion are: zinc oxide 2-5 gram, strontium oxide 3-6 gram.
(3) rare earth ferrum,cobalt and nickel magnetic powder material: granularity is 0.5-3 μ m, rare earth ferrum,cobalt and nickel magnetic powder 80-120 gram, additive 15-28 gram.Wherein, the constituent of additive and weight proportion are: aluminium oxide 5-10 gram, cobalt oxide 6-10 gram, nickel sesquioxide 4-8 gram.
(4) NdFeB magnetic powder material: granularity is a 0.5-3 μ m NdFeB magnetic powder 80-120 gram, additive 15-26 gram.Wherein, the constituent of additive and weight proportion are: ferroso-ferric oxide 6-8 gram, Dineodymium trioxide 5-8 gram, Borax 4-10 gram.
(5) barium ferrum magnetic powder material: granularity is a 0.5-3 μ m barium ferrum magnetic powder 80-120 gram, additive 5-11 gram.Wherein the constituent of additive and weight proportion are: barium sulfate 3-6 gram.Zinc oxide 2-5 gram.
C, spice: spice can be with the also available Western medicine of Chinese medicine, also the medicine that can form with the Chinese medicine Western medicine.
Spice can be from the damp-affection and pain relieving spice, chooses any one kind of them in anti-inflammatory analgesic spice, blood pressure lowering spice, antihaemorrhoidals material, treatment clavus spice, alleviation cataract spice and the treatment vulvitis spice.
Its constituent and weight proportion are as follows:
(1) damp-affection and pain relieving spice
Rhizoma Zingiberis Recens 300-700 gram, Herba Ephedrae 10-30 gram, Radix Aconiti 10-30 gram, Radix Aconiti Kusnezoffii 10-30 gram, Radix Angelicae Dahuricae 10-40 gram, Fructus Chaenomelis 30-70 gram is given birth to blue star 10-40 gram;
(2) anti-inflammatory analgesic spice
Venenum Bufonis 10-30 gram, Radix Aconiti 10-30 gram, Flos Carthami 10-30 gram, Borneolum Syntheticum 10-30 gram;
(3) blood pressure lowering spice
Semen Ricini 30-70 gram, Fructus Evodiae 10-30 gram, Rhizoma Zingiberis Recens 100-200 gram, Fructus Chaenomelis 10-40 gram, Borneolum Syntheticum 5-20 gram;
(4) antihaemorrhoidals material
Periostracum Serpentis 10-30 gram, Alumen 3-10 gram, Galla Chinensis 3-10 gram, Flos Celosiae Cristatae 5-15 gram, Borneolum Syntheticum 5-20 gram;
(5) treatment clavus spice
Salicylic acid 30-70 gram, Plumbum preparatium 1-5 gram, anaesthesine 1-5 gram;
(6) alleviate the cataract spice
Margarita powder 10-30 gram, Borneolum Syntheticum 1-10 gram, Borax 1-10 gram;
(7) treatment vulvitis spice
Forge Pulvis concha Mactrae 20-40 gram, Plumbum preparatium 30-50 gram, Borneolum Syntheticum 10-20 gram, catechu 10-30 gram, Radix Angelicae Dahuricae 10-30 gram.
The preparation method of plastic self-viscose magnetically osmosiring ointment is as follows:
The preparation of a, sizing material is chosen any one kind of them from following sizing material preparation
(1) preparation of rubber size:
Rubber is cut into strip, adhesive tape is pressed into film with glue pressing machine;
By weight ratio film is dipped in the industrial naptha at normal temperatures, soak time is no less than 24 hours, makes it to become latex;
Latex is packed in the batching still, at normal temperatures, stirred 2-3 hour with 50-100 rev/min rotating speed; Then, add modifier, continue to stir 1-2 hour, make rubber size;
(2) preparation of polrvinyl chloride sizing material:
The polrvinyl chloride powder is packed in the reactor, add the solvent dibutyl phthalate by weight ratio, under 80-100 ℃ of temperature, stirred 0.5-1 hour, make it to become white pasty liquid with 50-100 rev/min of rotating speed;
Be warming up to 125-145 ℃ gradually, continue to stir 0.5-1.5 hour, make it to become transparent viscous solution with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium by weight ratio, stir, make it to become yellow viscous solution; Be cooled to below 125 ℃, stirred 0.5-1.2 hour on limit adding zinc oxide, Camphora and enuatrol limit successively, makes the polrvinyl chloride sizing material;
(3) preparation of epoxy resin sizing material
By weight ratio epoxy resin and plasticizer are packed in the blender, under 50-80 ℃ of temperature, stirred 0.5-1 hour with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium, zinc oxide by weight ratio successively, under 80-120 ℃ of temperature, stirred 0.5-1 hour, make the epoxy resin sizing material with 50-100 rev/min of rotating speed;
The preparation of b, magnetic powder material
By weight ratio magnetic powder and additive mix homogeneously are put into baking oven, baking is 2-3 hour under 150-250 ℃ of temperature;
C, preparation permanent magnetism sizing material
The sizing material of will from rubber mass, polrvinyl chloride sizing material, epoxy resin sizing material, choosing any one kind of them, with the magnetic powder material of from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, choosing any one kind of them, by 1: (1-5) weight proportion, the kneader of packing into mixes, under 80-150 ℃ of temperature, kneader divides rotating speed with 50-100/, mediates repeatedly 1-3 hour, makes the permanent magnetism sizing material.
The preparation of d, spice powder
Selected back each constituent medical material of spice is cut into the bar that is not more than 20mm, under 80-150 ℃ of temperature, dries,, wear into granularity 80-100 order spice powder through pulverizing; Then with each constituent spice powder mix homogeneously.
E, permanent magnetism sizing material and spice powder are mixed and made into magnetic and ooze the ointment clay
By reprovision than with the permanent magnetism sizing material of c preparation with from damp-affection and pain relieving spice, anti-inflammatory analgesic spice, blood pressure lowering spice, antihaemorrhoidals material, treatment clavus spice, alleviate the spice powder that prepared of choosing any one kind of them cataract spice, the treatment vulvitis spice and pack in the kneader, under 50-100 ℃ of temperature, mediated 0.5-1 hour, make magnetic and ooze ointment clay group.
F, make magnetic and ooze ointment clay sheet, ball, bar
Magnetic is oozed ointment clay group be cooled to room temperature, be pressed into thin slice, cut into ointment table, ointment ball, ointment bar as required, in the wrapping paper of packing into, the container through roll squeezer.
G, magnetic ooze magnetizing of ointment
Ointment table, ball, bar with having installed place on the magnet charger, magnetize with 10000-15000 oersted magnetic field intensity.
Advantage of the present invention is that permanent magnet material, adhesive material and spice powder are integrated, and does not need the layering manufacturing.Magnetic ooze ointment can be directly and human body skin fit tightly, middle adhesion without adhesiver layer cuts off, the efficacy of a drug and magnetic force can directly reach skin, curative effect is better, uses more conveniently, can reduce the pharmacy cost.
Three constituent weight proportion embodiment of the present invention are as follows:
Embodiment 1: the weight proportion of permanent magnetism sizing material and spice is 404: 135.Rubber 30 grams, No. 200 gasoline 100 grams, Colophonium 28 grams, zinc oxide 16 grams, vaseline 10 grams, liquid Paraffin 10 grams, sofril 0.11 gram, stearic acid 0.3 gram; Spice: salicylic acid 118 grams, Plumbum preparatium 8.5 grams, anaesthesine 8.5 grams.
Embodiment 2: the weight proportion of permanent magnetism sizing material and spice is 347: 116.Rubber 20 grams, No. 200 gasoline 100 grams, Colophonium 25 grams, zinc oxide 20 grams, vaseline 8 grams, liquid Paraffin 16 grams, sulfur 0.08 gram, stearic acid 0.2 gram; Spice: salicylic acid 104 grams, Plumbum preparatium 6 grams, anaesthesine 6 grams.
Embodiment 3: the weight proportion of permanent magnetism sizing material and spice is 287: 96.Rubber 10 grams, No. 200 gasoline 100 grams, Colophonium 16 grams, zinc oxide 16 grams, liquid Paraffin 18 grams, sulfur 0.05 gram, spice: salicylic acid 90 grams, Plumbum preparatium 3 grams, anaesthesine 3 grams.
Claims (3)
1, a kind of plastic self-viscose magnetically osmosiring ointment is characterized in that its constituent is permanent magnetism sizing material and spice, and permanent magnetism sizing material and spice weight proportion are 100: (4-50), and permanent magnetism sizing material and the spice structure that is integrated; The permanent magnetism sizing material is made up of sizing material and magnetic powder material, sizing material is chosen any one kind of them from rubber size, polrvinyl chloride sizing material, epoxy resin sizing material, the constituent of magnetic powder material is magnetic powder and additive, from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, choose any one kind of them, wherein the constituent of iron oxide magnetic powder is iron sesquioxide and additive Barium monoxide, zinc oxide, and the constituent of strontium ferrum magnetic powder material is strontium ferrum magnetic powder and additive zinc oxide, strontium oxide.The constituent of rare earth ferrum,cobalt and nickel magnetic powder material is rare earth ferrum,cobalt and nickel magnetic powder and additive aluminium oxide, cobalt oxide, nickel sesquioxide, the constituent of NdFeB magnetic powder material is NdFeB magnetic powder and additive ferroso-ferric oxide, Dineodymium trioxide, Borax, and the constituent of barium ferrum magnetic powder material is barium ferrum magnetic powder and additive sulphuric acid barium, zinc oxide.
2, magnetic according to claim 1 oozes ointment, and the constituent that it is characterized in that permanent magnetism sizing material wherein is sizing material and magnetic powder material, and its weight proportion is 1: (1-5);
A, sizing material: the constituent of sizing material is macromolecular material, solvent, plasticizer, modifier, and sizing material is chosen any one kind of them from following rubber size, polrvinyl chloride sizing material, epoxy resin sizing material, and its constituent and weight proportion are as follows:
(1) rubber size: rubber 10-30 gram, industrial naptha 50-100 gram, modifier 39.2-81.41 gram; Wherein the constituent of modifier and weight proportion are 40 order Colophonium powder 15-30 grams, 320 order zinc oxide 10-20 gram, vaseline 6-13 gram, liquid Paraffin 8-18 gram, sofril 0.05-0.11 gram, stearic acid 0.15-0.3 gram;
(2) polrvinyl chloride sizing material: polrvinyl chloride 10-20 gram, solvent dibutyl phthalate 25-50 gram, modifier 111-212 gram; Wherein, the constituent of modifier and weight proportion are: 40 order Colophonium powder 50-90 gram, 320 order zinc oxide 60-120 gram, Camphora 0.5-1 gram, enuatrol 0.5-1 gram;
(3) epoxy resin sizing material: epoxy resin 10-20 gram, plasticizer phthalic acid dibutyl ester 10-40 gram, modifier 7-14 gram; Wherein, modifier constituent and weight proportion are 40 order Colophonium powder 1-2 grams, 320 order zinc oxide 5-10 gram;
B, magnetic powder material:
The constituent of magnetic powder material is magnetic powder and additive; The magnetic powder material is chosen any one kind of them from following iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, and its constituent and weight proportion are as follows:
(1) iron oxide magnetic powder: granularity is a 0.5-3 μ m iron sesquioxide magnetic powder 50-150 gram; Additive 7-16 gram; Additive constituent and weight proportion are Barium monoxide 4-5 gram zinc oxide 3-8 gram;
(2) strontium ferrum magnetic powder material: granularity is a 0.5-3 μ m strontium ferrum magnetic powder 80-120 gram; Additive 5-11 gram; The constituent of additive and weight proportion are: zinc oxide 2-5 gram, strontium oxide 3-6 gram;
(3) rare earth ferrum,cobalt and nickel magnetic powder material: granularity is 0.5-3 μ m, rare earth ferrum,cobalt and nickel magnetic powder 80-120 gram, additive 15-28 gram; Wherein, the constituent of additive and weight proportion are: aluminium oxide 5-10 gram, cobalt oxide 6-10 gram, nickel sesquioxide 4-8 gram;
(4) NdFeB magnetic powder material: granularity is a 0.5-3 μ m NdFeB magnetic powder 80-120 gram, additive 15-26 gram; Wherein, the constituent of additive and weight proportion are: ferroso-ferric oxide 6-8 gram, Dineodymium trioxide 5-8 gram, Borax 4-10 gram;
(5) barium ferrum magnetic powder material: granularity is a 0.5-3 μ m barium ferrum magnetic powder 80-120 gram, additive 5-11 gram; Wherein, the constituent of additive and weight proportion are: barium sulfate 3-6 gram, zinc oxide 2-5 gram.
3, a kind of method for preparing plastic self-viscose magnetically osmosiring ointment as claimed in claim 2 is characterized in that its method is as follows:
The preparation of a, sizing material is chosen any one kind of them from following sizing material preparation
(1) preparation of rubber size:
Rubber is cut into strip, adhesive tape is pressed into film with glue pressing machine;
By weight ratio film is dipped in the industrial naptha at normal temperatures, soak time is no less than 24 hours, makes it to become latex;
Latex is packed in the batching still, at normal temperatures, stirred 2-3 hour with 50-100 rev/min rotating speed; Then, add modifier, continue to stir 1-2 hour, make rubber size;
(2) preparation of polrvinyl chloride sizing material:
The polrvinyl chloride powder is packed in the reactor, add the solvent dibutyl phthalate by weight ratio, under 80-100 ℃ of temperature, stirred 0.5-1 hour, make it to become white pasty liquid with 50-100 rev/min of rotating speed;
Be warming up to 125-145 ℃ gradually, continue to stir 0.5-1.5 hour, make it to become transparent viscous solution with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium by weight ratio, stir, make it to become yellow viscous solution; Be cooled to below 125 ℃, stirred 0.5～1.2 hour on limit adding zinc oxide, Camphora and enuatrol limit successively, makes the polrvinyl chloride sizing material;
(3) preparation of epoxy resin sizing material
By weight ratio epoxy resin and plasticizer are packed in the blender, under 50-80 ℃ of temperature, stirred 0.5-1 hour with 50～100 rev/mins of rotating speeds;
Add modifier: add Colophonium, zinc oxide by weight ratio successively, under 80-120 ℃ of temperature, stirred 0.5-1 hour, make the epoxy resin sizing material with 50-100 rev/min of rotating speed;
The preparation of b, magnetic powder material
By weight ratio magnetic powder and additive mix homogeneously are put into baking oven, baking is 2-3 hour under 150-250 ℃ of temperature;
C, preparation permanent magnetism sizing material
The sizing material of will from rubber mass, polrvinyl chloride sizing material, epoxy resin sizing material, choosing any one kind of them, with the magnetic powder material of from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, choosing any one kind of them, by 1: (1-5) weight proportion, the kneader of packing into mixes, under 80-150 ℃ of temperature, kneader divides rotating speed with 50-100/, mediates repeatedly 1-3 hour, makes the permanent magnetism sizing material;
The preparation of d, spice powder
Selected back each constituent medical material of spice is cut into the bar that is not more than 20mm, under 80-150 ℃ of temperature, dries,, wear into granularity 80-100 order spice powder through pulverizing; Then each constituent spice is played the part of mix homogeneously;
E, permanent magnetism sizing material and spice powder are mixed and made into magnetic and ooze the ointment clay
By reprovision than with the permanent magnetism sizing material of c preparation with from damp-affection and pain relieving spice, anti-inflammatory analgesic spice, blood pressure lowering spice, antihaemorrhoidals material, treatment clavus spice, alleviate the spice powder that prepared of choosing any one kind of them the cataract spice and pack in the kneader, under 50-100 ℃ of temperature, mediated 0.5-1 hour, make magnetic and ooze ointment clay group;
F, make magnetic and ooze ointment clay sheet, ball, bar
Magnetic is oozed ointment clay group be cooled to room temperature, be pressed into thin slice, cut into ointment table, ointment ball, ointment bar as required, in the wrapping paper of packing into, the container through roll squeezer;
G, magnetic ooze magnetizing of ointment
Ointment table, ball, bar with having installed place magnet charger, magnetize with 10000-15000 oersted magnetic field intensity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001130951A CN1191821C (en) | 2000-07-05 | 2000-07-05 | Plastic self-viscose magnetically osmosiring ointment and its preparing process |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001130951A CN1191821C (en) | 2000-07-05 | 2000-07-05 | Plastic self-viscose magnetically osmosiring ointment and its preparing process |
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| Publication Number | Publication Date |
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| CN1330919A CN1330919A (en) | 2002-01-16 |
| CN1191821C true CN1191821C (en) | 2005-03-09 |
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| CNB001130951A Expired - Fee Related CN1191821C (en) | 2000-07-05 | 2000-07-05 | Plastic self-viscose magnetically osmosiring ointment and its preparing process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100431437C (en) * | 2007-01-10 | 2008-11-12 | 姜丽清 | Nanometer traditional Chinese medicine and electromagnetic briefs |
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2000
- 2000-07-05 CN CNB001130951A patent/CN1191821C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100431437C (en) * | 2007-01-10 | 2008-11-12 | 姜丽清 | Nanometer traditional Chinese medicine and electromagnetic briefs |
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| Publication number | Publication date |
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| CN1330919A (en) | 2002-01-16 |
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