CN1157229C - Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process - Google Patents
Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process Download PDFInfo
- Publication number
- CN1157229C CN1157229C CNB001130943A CN00113094A CN1157229C CN 1157229 C CN1157229 C CN 1157229C CN B001130943 A CNB001130943 A CN B001130943A CN 00113094 A CN00113094 A CN 00113094A CN 1157229 C CN1157229 C CN 1157229C
- Authority
- CN
- China
- Prior art keywords
- gram
- magnetic powder
- sizing material
- constituent
- weight proportion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Magnetic Treatment Devices (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention relates to permanent magnetic glue stock used for preparing a magnetic permeability ointment. The permanent magnetic glue stock is prepared from glue stock and magnetic powders, wherein the ratio of the glue stock to the magnetic powders is 1:1 to 5 according to the weight proportion. The glue stock is one of the following stock arbitrarily selected from rubber stock, polyvinyl chloride glue stock and epoxy resin glue stock, wherein the compositions of the rubber stock comprise rubber, solvents and modifying agents; the compositions of the polyvinyl chloride glue stock comprise polyvinyl chloride, the solvents and the modifying agents; the compositions of the epoxy resin glue stock comprise epoxy resin, plasticizing agents and the modifying agents. The magnetic powder is one of the following stock arbitrarily selected from ferric oxide magnetic powder and additive agents, strontium ferromagnetic powder and the additive agents, ferrum cobalt nickel magnetic powder and the additive agents, neodymium ferrum boron magnetic powder and the additive agents, and barium ferromagnetic powder and the additive agents. The permanent magnetic glue stock has the advantages that the permanent magnetic materials and adhesive materials are integrated; the permanent magnetic glue stock is convenient in use and low in cost.
Description
The present invention relates to a kind of permanent magnetism sizing material that is used to prepare plastic self-viscose magnetically osmosiring ointment.
Ointment is a kind of liniment that people use always.Traditional ointment only contains spice, treats with the effective ingredient of spice.In recent years, occur a kind of magnetic subsides or magnetic that contains spice and permanent magnetism powder on the market and oozed ointment, in the spice treatment, also carried out magnetic therapy.For example, Chinese patent application file 90106092.5 discloses a kind of " rare-earth magnetic plaster ".This patent application is a kind of three-decker ointment that contains anti-delamination, magnetic medicine thin film and adhesive layer of magnetic powder, and preparation technology is complicated, and because the existence of adhesive layer makes magnetic medicine thin film can not contact skin, influences therapeutic effect.
The object of the present invention is to provide a kind of permanent magnetism sizing material of the plastic self-viscose magnetically osmosiring ointment that magnetic medicine layer and adhesive layer are integrated.
The object of the present invention is achieved like this, a kind of permanent magnetism sizing material of plastic self-viscose magnetically osmosiring ointment, and it is mixed and made into by sizing material and magnetic powder material, and its weight proportion is 1: (1-5).
A, sizing material.The constituent of sizing material is macromolecular material, solvent, plasticizer, modifier.Sizing material can be chosen any one kind of them from following rubber size, polrvinyl chloride sizing material and epoxy resin sizing material.
The constituent and the weight proportion of sizing material are as follows:
(1), rubber size: rubber 10-30 gram, industrial naptha 50-100 gram, modifier 39.2-81.41 gram.Wherein the constituent of modifier and weight proportion are 40 order Colophonium powder 15-30 grams, 320 order zinc oxide 10-20 gram, vaseline 6-13 gram, liquid Paraffin 8-18 gram, sofril 0.05-0.11 gram, stearic acid 0.15-0.3 gram.
(2), polrvinyl chloride sizing material: polrvinyl chloride 10-20 gram, solvent dibutyl phthalate 25-50 gram, modifier 111-212 gram.Wherein, the constituent of modifier and weight proportion are: 40 order Colophonium powder 50-90 gram, 320 order zinc oxide 60-120 gram, Camphora 0.5-1 gram, enuatrol 0.5-1 gram.
(3), epoxy resin sizing material: epoxy resin 10-20 gram, plasticizer phthalic acid dibutyl ester 10-40 gram, modifier 7-14 gram.Wherein, modifier constituent and weight proportion are 40 order Colophonium powder 1-2 grams, 320 order zinc oxide 5-10 gram.
B, magnetic powder material.The constituent of magnetic powder material is magnetic powder and additive.The magnetic material can be chosen any one kind of them from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material and barium ferrum magnetic powder material.
The constituent and the weight proportion of magnetic powder material are as follows:
(1), iron oxide magnetic powder: granularity is a 0.5-3 μ m iron sesquioxide magnetic powder 50-150 gram; Additive 7-16 gram.Wherein, the constituent of additive and weight proportion are Barium monoxide 4-8 gram, zinc oxide 3-8 gram.
(2), strontium ferrum magnetic powder material: granularity is a 0.5-3 μ m strontium ferrum magnetic powder 80-120 gram; Additive 5-11 gram.Wherein, the constituent of additive and weight proportion are; Zinc oxide 2-5 gram, strontium oxide 3-6 gram.
(3), rare earth ferrum,cobalt and nickel magnetic powder material: granularity is a 0.5-3 μ m rare earth ferrum,cobalt and nickel magnetic powder 80-120 gram, additive 15-28 gram.Wherein, the constituent of additive and weight proportion are: aluminium oxide 5-10 gram, cobalt oxide 6-10 gram, nickel sesquioxide 4-8 gram.
(4), NdFeB magnetic powder material: granularity is a 0.5-3 μ m NdFeB magnetic powder 80-120 gram, additive 15-26 gram.Wherein, the constituent of additive and weight proportion are: ferroso-ferric oxide 6-8 gram, Dineodymium trioxide 5-8 gram, Borax 4-10 gram.
(5), barium ferrum magnetic powder material: granularity is a 0.5-3 μ m barium ferrum magnetic powder 80-120 gram, additive 5-11 gram.Wherein, the constituent of additive and weight proportion are: barium sulfate 3-6 gram.Zinc oxide 2-5 gram.
The preparation method of permanent magnetism sizing material is as follows:
The preparation of a, sizing material is chosen any one kind of them from following sizing material preparation
(1), the preparation of rubber size:
Rubber is cut into strip, adhesive tape is pressed into film with glue pressing machine;
By weight ratio film is dipped in the industrial naptha at normal temperatures, soak time is no less than 24 hours, makes it to become latex;
Latex is packed in the batching still, at normal temperatures, stirred 2-3 hour with 50-100 rev/min rotating speed; Then, add modifier, continue to stir 1-2 hour, make rubber size;
(2), the preparation of polrvinyl chloride sizing material:
The polrvinyl chloride powder is packed in the reactor, add the solvent dibutyl phthalate by weight ratio, under 80-100 ℃ of temperature, stirred 0.5-1 hour, make it to become white pasty liquid with 50-100 rev/min of rotating speed;
Be warming up to 125-145 ℃ gradually, continue to stir 0.5-1.5 hour, make it to become transparent viscous solution with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium by weight ratio, stir, make it to become yellow viscous solution; Be cooled to below 125 ℃, stirred 0.5-1.2 hour on limit adding zinc oxide, Camphora and enuatrol limit successively, makes the polrvinyl chloride sizing material;
(3), the preparation of epoxy resin sizing material
By weight ratio epoxy resin and plasticizer are packed in the blender, under 50-80 ℃ of temperature, stirred 0.5-1 hour with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium, zinc oxide by weight ratio successively, under 80-120 ℃ of temperature, stirred 0.5-1 hour, make the epoxy resin sizing material with 50-100 rev/min of rotating speed;
The preparation of b, magnetic powder material
By weight ratio magnetic powder and additive mix homogeneously are put into baking oven, baking is 2-3 hour under 150-250 ℃ of temperature;
C, preparation permanent magnetism sizing material
The sizing material of will from rubber mass, polrvinyl chloride sizing material, epoxy resin sizing material, choosing any one kind of them, with the magnetic powder material of from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, choosing any one kind of them, by 1: (1-5) weight proportion, the kneader of packing into mixes, under 80-150 ℃ of temperature, kneader divides rotating speed with 50-100/, mediates repeatedly 1-3 hour, makes the permanent magnetism sizing material.
When using this permanent magnetism sizing material to prepare magnetic to ooze ointment, behind spice mix homogeneously, magnetize, magnetic powder, spice and adhesive are integrated, make magnetic and ooze ointment, be used for the treatment of permanent magnetism sizing material and selection.
The present invention is used for mixing with the spice with specific therapeutical, oozes ointment to prepare plastic self-adhesion magnetic.Its advantage is that permanent magnet material is integrated with pasting sizing material, and does not need the layering manufacturing; And ointment is directly fitted tightly with human body skin, and middle adhesion without adhesiver layer partition, the efficacy of a drug and magnetic force can directly reach skin, and curative effect is better, uses more conveniently, can reduce the pharmacy cost.
The embodiment of three constituent weight proportions of the present invention is as follows:
Embodiment 1: rubber 30 grams, No. 200 gasoline 100 grams, Colophonium 28 grams, zinc oxide 16 grams, vaseline 10 grams, liquid Paraffin 10 grams, sofril 0.11 gram, stearic acid 0.3 gram; Strontium ferrum magnetic powder 200 grams, zinc oxide 4 grams, strontium oxide 6 grams.
Embodiment 2: rubber 20 grams, No. 200 gasoline 100 grams, Colophonium 25 grams, zinc oxide 20 grams, vaseline 8 grams, liquid Paraffin 16 grams, sulfur 0.08 gram, stearic acid 0.2 gram; Strontium ferrum magnetic powder 150 grams, zinc oxide 3 grams, strontium oxide 5 grams.
Embodiment 3: rubber 10 grams, No. 200 gasoline 100 grams, Colophonium 16 grams, zinc oxide 16 grams, liquid Paraffin 18 grams, sulfur 0.05 gram; Strontium ferrum magnetic powder 120 grams, zinc oxide 3 grams, strontium oxide 4 grams.
Claims (10)
1, a kind of permanent magnetism sizing material of plastic self-viscose magnetically osmosiring ointment is characterized in that its constituent is sizing material and magnetic powder material, and its weight proportion is 1: (1-5), sizing material and magnetic powder material are integrated; Sizing material selects a kind of from rubber mass, polrvinyl chloride sizing material, epoxy resin sizing material; The magnetic powder material is chosen any one kind of them from the iron sesquioxide magnetic powder material that contains additive, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material.
2, permanent magnetism sizing material according to claim 1 is characterised in that wherein the constituent and the weight proportion of sizing material are: rubber 10-30 gram, gasoline 50_100 gram, modifier 39.2-81.41 gram; The constituent of modifier and weight proportion are:; Colophonium powder 15-30 gram, zinc oxide 10-20 gram, vaseline 6-13 gram, liquid Paraffin 8-18 gram, sofril 0.05-0.11 gram, stearic acid 0.15-0.3 gram.
3, permanent magnetism sizing material according to claim 1 is characterized in that wherein the constituent and the weight proportion of sizing material are: polrvinyl chloride 10-20 gram, solvent dibutyl phthalate 25-50 gram, modifier 111-212 gram; Wherein, the constituent of modifier and weight proportion are: Colophonium powder 50-90 gram, zinc oxide 60-120 gram, Camphora 0.5-1 gram, enuatrol 0.5-1 gram.
4, permanent magnetism sizing material according to claim 1 is characterised in that the constituent of sizing material and weight proportion are: epoxy resin 10-20 gram, plasticizer phthalic acid dibutyl ester 10-40 gram, modifier 7-14 gram; The constituent of modifier and weight proportion are Colophonium 1-2 gram, zinc oxide 5-10 gram.
5, permanent magnetism sizing material according to claim 1 is characterized in that the constituent of magnetic powder material wherein and weight proportion are: iron sesquioxide magnetic powder 50-150 gram, additive 7-16 gram; Wherein the constituent of additive and weight proportion are: Barium monoxide 4-8 gram, zinc oxide 3-8 gram.
6, permanent magnetism sizing material according to claim 1 is characterized in that the constituent of magnetic powder material wherein and weight proportion are: strontium ferrum magnetic powder 80-120 gram, additive 5-11 gram; Wherein the constituent of additive and weight proportion are zinc oxide 2-5 gram, strontium oxide 3-6 gram.
7, permanent magnetism sizing material according to claim 1 is characterized in that the constituent of magnetic powder material wherein and weight proportion are: rare earth ferrum,cobalt and nickel magnetic powder 80-120 gram, additive 15-28 gram; Wherein the constituent of additive and weight proportion are aluminium oxide 5-10 gram, cobalt oxide 6-10 gram, nickel sesquioxide 4-8 gram.
8, according to the described permanent magnetism sizing material of claim 1, it is characterized in that wherein the constituent and the weight proportion of magnetic powder material are: NdFeB magnetic powder 80-120 gram additive 15-26 restrains wherein additive constituent and weight proportion is ferroso-ferric oxide 6-8 gram, Dineodymium trioxide 5-8 gram, Borax 4-10 gram.
9, permanent magnetism sizing material according to claim 1 is characterized in that the constituent of magnetic powder material wherein and weight proportion are: barium ferrum magnetic powder 80-120 gram, additive 5-11 gram; Wherein the constituent of additive and weight proportion are: barium sulfate 3-6 gram, zinc oxide 2-5 gram.
10, the preparation method of permanent magnetism sizing material according to claim 1 is characterized in that its preparation method is as follows:
The preparation of a, sizing material is chosen any one kind of them from following sizing material preparation
(1) preparation of rubber size:
Rubber is cut into strip, adhesive tape is pressed into film with glue pressing machine;
By weight ratio film is dipped in the industrial naptha at normal temperatures, soak time is no less than 24 hours, makes it to become latex;
Latex is packed in the batching still, at normal temperatures, stirred 2-3 hour with 50-100 rev/min rotating speed; Then, add modifier, continue to stir 1-2 hour, make rubber size;
(2) preparation of polrvinyl chloride sizing material:
The polrvinyl chloride powder is packed in the reactor, add the solvent dibutyl phthalate by weight ratio, under 80-100 ℃ of temperature, stirred 0.5-1 hour, make it to become white pasty liquid with 50-100 rev/min of rotating speed;
Be warming up to 125-145 ℃ gradually, continue to stir 0.5-1.5 hour, make it to become transparent viscous solution with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium by weight ratio, stir, make it to become yellow viscous solution; Be cooled to below 125 ℃, stirred 0.5-1.2 hour on limit adding zinc oxide, Camphora and enuatrol limit successively, makes the polrvinyl chloride sizing material;
(3) preparation of epoxy resin sizing material
By weight ratio epoxy resin and plasticizer are packed in the blender, under 50-80 ℃ of temperature, stirred 0.5-1 hour with 50-100 rev/min of rotating speed;
Add modifier: add Colophonium, zinc oxide by weight ratio successively, under 80-120 ℃ of temperature, stirred 0.5-1 hour, make the epoxy resin sizing material with 50-100 rev/min of rotating speed;
The preparation of b, magnetic powder material
By weight ratio magnetic powder and additive mix homogeneously are put into baking oven, baking is 2-3 hour under 150-250 ℃ of temperature;
C, preparation permanent magnetism sizing material
The sizing material of will from rubber mass, polrvinyl chloride sizing material, epoxy resin sizing material, choosing any one kind of them, with the magnetic powder material of from iron oxide magnetic powder, strontium ferrum magnetic powder material, rare earth ferrum,cobalt and nickel magnetic powder material, NdFeB magnetic powder material, barium ferrum magnetic powder material, choosing any one kind of them, by 1: (1-5) weight proportion, the kneader of packing into mixes, under 80-150 ℃ of temperature, kneader divides rotating speed with 50-100/, mediates repeatedly 1-3 hour, makes the permanent magnetism sizing material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001130943A CN1157229C (en) | 2000-07-05 | 2000-07-05 | Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001130943A CN1157229C (en) | 2000-07-05 | 2000-07-05 | Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1330956A CN1330956A (en) | 2002-01-16 |
| CN1157229C true CN1157229C (en) | 2004-07-14 |
Family
ID=4582911
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB001130943A Expired - Fee Related CN1157229C (en) | 2000-07-05 | 2000-07-05 | Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1157229C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108245317B (en) * | 2018-01-10 | 2020-11-13 | 江西宜信堂医疗科技有限公司 | Infrared cough relieving plaster and preparation method thereof |
-
2000
- 2000-07-05 CN CNB001130943A patent/CN1157229C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1330956A (en) | 2002-01-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110551299B (en) | Self-adhesive polyacrylamide composite hydrogel and preparation method and application thereof | |
| US20050191337A1 (en) | Patch with a magnetic field effect | |
| CN101705005B (en) | Method for modifying performance of compound resin by using tetrapod-like zinc oxide whiskers | |
| WO2001017548A3 (en) | Use of natriuretic peptides as antibiotically effective substances for treating bacterial infections | |
| CN1157229C (en) | Permanent-magnet colloid for plastic self-viscose magnetcally osmosizing ointment and its preparing process | |
| CN1624824A (en) | Flexible binding neodymium ferroboron magnet and manufacturing method thereof | |
| CN106340367B (en) | The compound bonded permanent magnet preparation process of a kind of ferrite, neodymium iron boron | |
| CN108159480A (en) | A kind of preparation method and application of injectable polysaccharide clay plural gel | |
| CN101041766A (en) | Antistatic hot-melting glue and coating method thereof | |
| CN105206370B (en) | A kind of high temperature resistant isotropism NdFeB Bonded Magnets and preparation method thereof | |
| CN101962276B (en) | Tourmaline composite material and preparation method thereof | |
| CN104490609A (en) | Preparation of graphene oxide and nanosized silica composite filler reinforced binder for dentistry | |
| CN1330919A (en) | Plastic self-viscose magnetically osmosiring ointment and its preparing process | |
| CN1070051C (en) | Substrate for medical paste | |
| CN110491614B (en) | Magnetic material with high compressive strength and preparation method thereof | |
| CN1058713A (en) | A kind of talcum powder | |
| JPH0661023A (en) | Rare earth bonded magnet | |
| JPS62152107A (en) | Magnetic powder for synthetic resin magnet | |
| CN2676917Y (en) | Chitosan medicine film | |
| JPH02161701A (en) | Manufacture of permanent magnet | |
| JPS6044806B2 (en) | Method for producing a composition for permanent magnets | |
| CN1355053A (en) | Magnetotherapeutic sheet and manufacturing method | |
| DE3518188C1 (en) | Aluminium lactate solution and a process for the preparation thereof and the use thereof | |
| CN2517449Y (en) | Sheet for magnetic treatment | |
| CN1140052A (en) | Multifunctional prickly-heat powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |