CN118517395A - Low-temperature vacuum pump with excellent vacuum stability - Google Patents
Low-temperature vacuum pump with excellent vacuum stability Download PDFInfo
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- CN118517395A CN118517395A CN202410684062.2A CN202410684062A CN118517395A CN 118517395 A CN118517395 A CN 118517395A CN 202410684062 A CN202410684062 A CN 202410684062A CN 118517395 A CN118517395 A CN 118517395A
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- 239000003463 adsorbent Substances 0.000 claims abstract description 15
- 238000000576 coating method Methods 0.000 claims abstract description 13
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000011248 coating agent Substances 0.000 claims abstract description 11
- 229910052802 copper Inorganic materials 0.000 claims abstract description 11
- 239000010949 copper Substances 0.000 claims abstract description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 28
- 238000010438 heat treatment Methods 0.000 claims description 20
- 230000007246 mechanism Effects 0.000 claims description 13
- 239000002028 Biomass Substances 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 9
- 238000005057 refrigeration Methods 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 22
- 230000008569 process Effects 0.000 abstract description 22
- 238000012545 processing Methods 0.000 abstract description 14
- 239000012535 impurity Substances 0.000 abstract description 11
- 239000000463 material Substances 0.000 abstract description 10
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- 239000004065 semiconductor Substances 0.000 abstract description 6
- 239000007789 gas Substances 0.000 description 43
- 229910052734 helium Inorganic materials 0.000 description 21
- 239000001307 helium Substances 0.000 description 21
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 21
- 230000000694 effects Effects 0.000 description 9
- 238000001179 sorption measurement Methods 0.000 description 7
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- 239000002994 raw material Substances 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 238000001771 vacuum deposition Methods 0.000 description 2
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- 229920001342 Bakelite® Polymers 0.000 description 1
- 241001070941 Castanea Species 0.000 description 1
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- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B37/00—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00
- F04B37/06—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for evacuating by thermal means
- F04B37/08—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for evacuating by thermal means by condensing or freezing, e.g. cryogenic pumps
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B37/00—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00
- F04B37/06—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for evacuating by thermal means
- F04B37/08—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for evacuating by thermal means by condensing or freezing, e.g. cryogenic pumps
- F04B37/085—Regeneration of cryo-pumps
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Compressors, Vaccum Pumps And Other Relevant Systems (AREA)
Abstract
The invention relates to the technical field of vacuum pumps, in particular to a low-temperature vacuum pump with excellent vacuum stability, which comprises an outer shell, a cold screen, a cold umbrella and a refrigerating device; the improved cryopump is particularly suitable for the processing processes of chip coating and the like in the semiconductor industry, provides a pure vacuum environment, has the vacuum degree of 10 ‑ 9 Pa, does not introduce other impurities, and ensures the processing precision. The refrigerator is used for refrigerating, the cold screen and the cold umbrella structure are mainly cooled, a low-temperature environment, particularly the temperature of the cold umbrella structure which can reach ultralow temperature (10K), is formed, and the adsorbent arranged on the cold umbrella can adsorb and solidify gas molecules in the environment on the low-temperature environment, so that a vacuum environment is realized. The cold screen is made of copper materials, the inner side wall of the cold screen is plated with a nickel coating, namely, a black coating is arranged on the inner wall of the cold screen, heat energy of radiation is reflected, heat is prevented from being reflected to the cold umbrella, and fluctuation of heat radiation to a vacuum environment is reduced.
Description
Technical Field
The invention relates to the technical field of vacuum pumps, in particular to a low-temperature vacuum pump with excellent vacuum stability.
Background
The cryopump has the advantages of high vacuum degree, high cleanliness, high gas capacity, high air extraction rate and the like, and is gradually and widely applied to research and production of semiconductors and integrated circuits, and the fields of molecular beam research, vacuum coating equipment, vacuum surface analysis instruments, ion implanters, space simulation devices and the like. Particularly, vacuum coating requires heating a metal or nonmetal material under high vacuum conditions to evaporate and condense the material on the surface of a coated member (metal, semiconductor or insulator) to form a thin film, and thus there is a high demand for stable vacuum environment. At present, the fluctuation of temperature or vacuum degree easily occurs in the use process of the low-temperature pump, so that the processing precision of a coating film is influenced, and meanwhile, impurities easily exist in the refrigerating gas, so that the vacuum degree is influenced; frequent cleaning of the interior of the cryopump is required, the operation steps are complicated, the disassembly and assembly are inconvenient, and the working efficiency is affected. Many of the existing cryopump technologies also depend on import, so that it is of great importance to research a cryopump structure that is simple to assemble and convenient to operate and maintain.
The main case of the scheme is an improved cryopump, the application number is CN202311658773.4, and the application date is 2023, 12 months and 05 days.
Disclosure of Invention
The invention aims to provide a low-temperature vacuum pump with excellent vacuum stability, so as to solve the problems in the prior art.
In order to solve the technical problems, the technical scheme provided by the invention is as follows: the low-temperature vacuum pump with excellent vacuum stability comprises an outer shell, a cold screen, a cold umbrella and a refrigerating device; the outer shell is of a hollow structure with one end open, the cold screen is fixedly arranged in the outer shell and is structurally matched with the outer shell, the cold umbrella is arranged in the cold screen, the surface of the cold umbrella is coated with an adsorbent, and the refrigerating device is connected with the cold umbrella to provide refrigeration for the cold screen; the cold screen inner side wall is plated with a nickel coating, a plurality of auxiliary barrier plates are uniformly arranged on the cold screen inner side wall, one ends of the auxiliary barrier plates are uniformly and fixedly arranged on the cold screen, and the other ends extend to the cold umbrella part and are provided with gaps.
On the basis of the technical scheme, the refrigerating device comprises a first-stage cold head, a second-stage cold head and a driving mechanism, wherein the first-stage cold head is used for cooling a cold screen, the second-stage cold head is used for cooling a cold umbrella, a first-stage piston is arranged in the first-stage cold head, a second-stage piston is arranged in the second-stage cold head, the second-stage piston is fixedly arranged at the top end of the first-stage piston, the tail end of the first-stage piston is connected with the driving mechanism, and refrigerating gas flows in the first-stage cold head and the second-stage cold head.
On the basis of the technical scheme, a plurality of layers of copper nets are arranged in the first-section piston, lead particles are filled in the copper nets, and air inlets and air outlets are formed in two ends of the first-section piston and/or the second-section piston.
On the basis of the technical scheme, the driving mechanism comprises a driving motor, an eccentric shaft, an eccentric wheel and a driving frame, wherein the eccentric shaft is driven by the driving motor to rotate, the eccentric wheel is fixedly sleeved on the eccentric shaft, the eccentric wheel is arranged in the driving frame, and the driving frame is connected with a section of piston.
On the basis of the technical scheme, the cold umbrella comprises a first cold umbrella structure and a second cold umbrella structure, and the second cold umbrella structure is arranged at the top end of the first cold umbrella structure; the first cold umbrella structure comprises a plurality of first cold umbrella sheets and is fixedly arranged from top to bottom in sequence, the second cold umbrella structure comprises a plurality of second cold umbrella sheets, and the diameters of the second cold umbrella sheets are sequentially increased from inside to outside.
On the basis of the technical scheme, the first cold umbrella sheet comprises an end face arranged to be a plane and a circular side face which are fixedly connected, and the end face and the side face are obliquely arranged; the second cold umbrella sheet is formed by fixedly splicing two circular ring sheets arranged in a mirror image mode.
On the basis of the technical scheme, the first cold umbrella sheets are fixedly arranged on the cold umbrella support, a plurality of first through holes are formed in the end face of one first cold umbrella sheet positioned at the top end, and a plurality of second through holes are formed in the cold umbrella support.
Based on the technical scheme, the adsorbent is modified activated carbon or biomass carbon.
On the basis of the technical scheme, the driving mechanism is provided with a shock absorber or a vibration isolator.
On the basis of the technical scheme, the air cylinder cooling device further comprises a heating device, wherein the heating device is arranged in an air cylinder shell, the end part of the heating device is fixedly arranged at the head end of the secondary cooling head, the air cylinder shell is fixedly arranged on one side of the outer shell and is in through connection, and the primary cooling head and the secondary cooling head are arranged in the air cylinder shell.
The technical scheme provided by the invention has the beneficial effects that:
1. The invention provides a low-temperature vacuum pump with excellent vacuum stability, which is particularly suitable for the processing processes of chip coating and the like in the semiconductor industry, provides a pure vacuum environment, has the vacuum degree of 10 -9 Pa, does not introduce other impurities, and ensures the processing precision. The refrigerator is used for refrigerating, the cold screen and the cold umbrella structure are mainly cooled, a low-temperature environment, particularly the temperature of the cold umbrella structure which can reach ultralow temperature (10K), is formed, and the adsorbent arranged on the cold umbrella can adsorb and solidify gas molecules in the environment on the low-temperature environment, so that a vacuum environment is realized. The cold screen is made of copper materials, the inner side wall of the cold screen is plated with a nickel coating, namely, a black coating is arranged on the inner wall of the cold screen, heat energy of radiation is reflected, heat is prevented from being reflected to the cold umbrella, and fluctuation of heat radiation to a vacuum environment is reduced.
2. The piston of the cold head in the refrigerating device is filled with lead particles, so that the cold head has the effects of cold accumulation and heat absorption, the heat exchange of passing helium is realized, the drift and fluctuation of temperature and vacuum degree are reduced, and the stability of a processing environment is ensured; especially, the lead particles filled in the helium gas filter has the function of filtering, so that impurities in the helium gas can be removed in the flowing process of the helium gas, and the working efficiency of the helium gas is improved.
3. The plurality of first cold umbrella sheets are arranged in the cold umbrella structure, and the first cold umbrella sheets are matched with the adsorbent arranged on the first cold umbrella sheets, so that molecules in gas can be quickly adsorbed at low temperature and a solidification position is provided, and a higher vacuum degree in the environment is realized; the second cold umbrella piece also can adsorb corresponding gaseous molecule, can also effectively reduce gaseous direct current and directly strike first cold umbrella structure, and the slope of second cold umbrella piece sets up simultaneously and is formed by two concatenation of symmetry, can reflect the heat radiation of environment, avoids the adverse effect of temperature to the vacuum to further guarantee holistic vacuum demand.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a cross-sectional view of the outer housing and cold screen of the present invention;
FIG. 3 is a schematic view of a refrigeration apparatus according to the present invention;
FIG. 4 is an internal cross-sectional view of FIG. 3;
FIG. 5 is a schematic view of the structure of the umbrella according to the present invention;
FIG. 6 is a schematic view of a first cold umbrella structure of the present invention;
FIG. 7 is a schematic view of the structure of a first cold umbrella blade of the present invention;
FIG. 8 is a schematic structural view of a second cold umbrella structure of the present invention;
FIG. 9 is a schematic view of a second cold umbrella blade of the present invention;
Detailed Description
The invention is further illustrated by the following examples in conjunction with the accompanying drawings:
In the present invention, unless explicitly specified and limited otherwise, the terms "mounted," "connected," "secured," and the like are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally formed; can be directly connected or indirectly connected through an intermediate medium, and can be communicated with the inside of two elements or the interaction relationship of the two elements. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art according to the specific circumstances.
In the description of the present invention, it should be understood that the terms "left", "right", "front", "rear", "top", "bottom", and the like indicate an orientation or a positional relationship based on that shown in the drawings, and are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the apparatus or element to be referred to must have a specific orientation, be configured and operated in a specific orientation, and thus should not be construed as limiting the present invention.
Example 1
As shown in fig. 1 to 9, a low temperature vacuum pump excellent in vacuum stability includes an outer case 1, a cold shield 2, a cold umbrella 3, and a refrigerating device; the shell body 1 is arranged to be of a hollow structure with one end open, the cold screen 2 is fixedly arranged in the shell body 1 and is matched with the shell body in structure, the cold umbrella 3 is arranged in the cold screen 2, the adsorbent is coated on the surface of the cold umbrella 3, and the refrigerating device is connected with the cold umbrella 3 to provide refrigeration effect in the cold screen 2.
The invention provides a low-temperature vacuum pump with excellent vacuum stability, which is particularly suitable for the processing processes of chip coating and the like in the semiconductor industry, provides a pure vacuum environment, has the vacuum degree of 10 -9 Pa, does not introduce other impurities, and ensures the processing precision. Specifically, the shell body 1 one end is sealed, and the other end opening and opening part are provided with flange, conveniently install the cryopump wholly on the process chamber or install on other equipment that need keep vacuum environment, make things convenient for the dismouting. The refrigeration device is used for refrigerating, the structures of the cold screen 2 and the cold umbrella 3 are mainly cooled, a low-temperature environment, particularly the temperature of the cold umbrella structure reaching ultralow temperature, namely 10K, is formed, and the adsorbent arranged on the cold umbrella 3 can adsorb and solidify gas molecules in the environment in the low-temperature environment, so that a vacuum environment is realized; the cold screen 2 is made of copper materials, and nickel coatings are plated on the inner side walls, namely black coatings are arranged on the inner walls of the cold screen 2, heat energy of radiation is reflected, heat is prevented from being reflected to the cold umbrella, and fluctuation of heat radiation to a vacuum environment is reduced.
As shown in fig. 2, a gap is provided between the outer casing 1 and the cold screen 2, one end of the cold screen 2 is provided with a through hole, and the height of the cold screen 2 is smaller than that of the outer casing 1.
In a preferred embodiment, a gap is provided between the outer case 1 and the cold shield 2 to form an auxiliary gas passage, so that gas enters the interior through the cold umbrella structure during the flowing process, and gas can directly enter the cold umbrella structure, and meanwhile, part of gas can enter the cold umbrella structure through the auxiliary gas passage and the through holes, so that gas molecules can be adsorbed and solidified rapidly and effectively.
On the basis of the technical scheme, the refrigerating device comprises a primary cold head 4, a secondary cold head 5 and a driving mechanism 6, wherein the primary cold head 4 is used for cooling the cold screen 2, the secondary cold head 5 is used for cooling the cold umbrella 3, a first section of piston 41 is arranged in the primary cold head 4, a second section of piston 51 is arranged in the secondary cold head 5, the second section of piston 51 is fixedly arranged at the top end of the first section of piston 41, the tail end of the first section of piston 41 is connected with the driving mechanism, and refrigerating gas flows in the primary cold head 4 and the secondary cold head 5.
Specifically, the primary cold head 4 is in thermal contact with the cold screen 2, and the secondary cold head 5 is in thermal contact with the cold umbrella 3, wherein the head end of the secondary cold head 5 is fixedly connected with the cold umbrella bracket 33 through a fixing frame; in the reciprocating motion process of the first-stage piston 41 and the second-stage piston 51 in the cold head, the refrigerating gas is driven to do work, expansion absorbs heat and refrigeration, the temperature of the cold screen 2 and the cold umbrella 3 is reduced to the required temperature, and therefore adsorption and solidification of gas molecules in the environment are realized, and the required vacuum degree requirement is met.
On the basis of the technical scheme, the driving mechanism 6 comprises a driving motor 61, an eccentric shaft 62, an eccentric wheel 63 and a driving frame 64, the eccentric shaft 62 is driven to rotate by the driving motor 61, the eccentric wheel 63 is fixedly sleeved on the eccentric shaft 62, the eccentric wheel 63 is arranged in the driving frame 64, and the driving frame 64 is connected with a section of piston 41.
Wherein the driving frame 64 is arranged in a Chinese character 'zhong' shape; the driving motor 61 drives the eccentric shaft 62 and the eccentric wheel 63 thereon to move, and drives the driving frame 64 to reciprocate, so as to drive the first-stage piston 41 and the second-stage piston 51 to do work on helium, the compressed helium absorbs heat in the compression and expansion processes, the temperatures of the first-stage cold head 4 and the second-stage cold head 5 are reduced, the cold screen 2 and the cold umbrella 3 are in a low-temperature state, and the adsorption of molecules in gas by the cold umbrella structure is realized in the low-temperature state.
The refrigerating gas realizes air inlet and outlet control through the gas control device 7, the gas control device 7 comprises a base 71, an air inlet valve, an air outlet valve and a valve switch 72, the base 71 is fixedly connected with the cold head base 10, the cold head base 10 is fixedly arranged at the tail end of the primary cold head 4, the air inlet valve and the air outlet valve are respectively arranged in the base 71, and the valve switch 72 is respectively arranged corresponding to the air inlet valve and the air outlet valve and controls the opening and closing of the air inlet valve and the air outlet valve.
The valve switch 72 comprises a time valve swing arm 721, a thimble 722 and an eccentric bearing 723, wherein one side of the time valve swing arm 721 is connected with an air inlet valve or an air outlet valve through the thimble 722, the other side of the time valve swing arm is abutted with the eccentric bearing 723, and the eccentric bearing 723 is sleeved on the eccentric shaft 62.
It can be understood that two eccentric bearings 723 are disposed on the eccentric shaft 62 corresponding to the air inlet valve and the air outlet valve sleeve, and correspondingly, two valve swing arms 721 are disposed on one side of the air inlet valve or one side of the air outlet valve respectively, and the driving motor drives different valves on different eccentric bearings 62 during the rotation process of the eccentric shaft 62, so as to realize the air inlet or air outlet process.
On the basis of the technical scheme, the cold umbrella 3 comprises a first cold umbrella structure and a second cold umbrella structure, and the second cold umbrella structure is arranged at the top end of the first cold umbrella structure; the first cold umbrella structure comprises a plurality of first cold umbrella sheets 31 and is fixedly arranged from top to bottom in sequence, the second cold umbrella structure comprises a plurality of second cold umbrella sheets 32, and the diameters of the second cold umbrella sheets 32 are sequentially increased from inside to outside.
In the cold umbrella structure, a plurality of first cold umbrella sheets 31 are arranged and matched with the adsorbent arranged on the first cold umbrella sheets, so that molecules in gas can be quickly adsorbed at low temperature and a solidification position is provided, and a higher vacuum degree in the environment is realized; the second cold umbrella piece 32 also can adsorb corresponding gas molecule, can also effectively reduce the first cold umbrella structure of gaseous direct current direct impact, and the second cold umbrella piece 32 slope sets up simultaneously and is formed by two concatenation of symmetry, can reflect the heat radiation of environment, avoids the adverse effect of temperature to the vacuum to further guarantee holistic vacuum demand.
The above-mentioned upper is defined according to the side close to the opening of the outer casing, and the opposite side away from the opening of the outer casing is the lower side; the inner and outer are defined by taking the direction close to the inner side wall of the cold screen as the outer side and the direction far away from the inner side wall of the cold screen as the inner side; the above description is only for convenience of understanding and description of the technical solution, and does not constitute a limitation of the present application.
On the basis of the above technical solution, the first cold umbrella 31 includes an end surface 311 configured as a plane and a circular side surface 312, and is fixedly connected, and the end surface 311 and the side surface 312 are obliquely arranged; the second cold umbrella sheet 32 is formed by fixedly splicing two circular ring sheets 321 which are arranged in a mirror image mode.
Preferably, the included angle between the end surface 311 and the side surface 312 of the first cold umbrella 31 is an obtuse angle. The side of the cold umbrella can reflect a part of heat radiation, so that adverse effects of heat on temperature and vacuum degree are reduced, and fluctuation of the vacuum degree is reduced.
The first cold umbrella pieces 31 are fixedly arranged on the cold umbrella support 33, and the cold umbrella support 33 is fixedly connected with the refrigerating device; the second cold umbrella sheets 32 are connected through a fixing rod 34, and the free end of the fixing rod 34 is fixedly arranged on the inner side wall of the cold screen 2.
As shown in the figure, besides the first cold umbrella piece 31 positioned at the topmost end, other first cold umbrella pieces 31 are provided with notches on the side surfaces thereof, mainly for adapting to the installation of the cold head part in the cold device; the central positions of the other first cold umbrella pieces 31 are provided with openings, through grooves are formed in the radial direction, and the cold umbrella supports 33 are arranged in the through grooves, so that the first cold umbrella pieces 31 are conveniently fixed, and meanwhile, the rapid flow of gas and the adsorption and solidification of molecules contained in the gas are promoted.
On the basis of the above technical solution, the first cold umbrella pieces 31 are fixedly disposed on the cold umbrella support 33, a plurality of through holes are formed in the end face of one first cold umbrella piece 31 located at the top end, and a plurality of through holes are formed in the cold umbrella support 33.
Through being provided with cold umbrella support 33, can assist the fixed and dismouting of a plurality of first cold umbrella pieces 31, the through-hole that sets up on it of cooperation, make things convenient for the flow of gas and drive the molecule that exists in the environment and carry out more comprehensive absorption, satisfy the vacuum environment of high vacuum requirement.
Based on the technical scheme, the adsorbent is modified activated carbon. In this embodiment, the preparation method of the modified activated carbon includes the following steps:
Step one: the activated carbon is placed on a mesh screen for screening, so that more uniform activated carbon is obtained;
step two: placing the activated carbon obtained in the first step in a beaker, adding an acid solution, stirring, heating in the stirring process, and keeping the temperature at 120 ℃ for continuous stirring for 30min;
step three: filtering the solution obtained in the second step, repeatedly washing with deionized water to be neutral, and drying to obtain the modified activated carbon.
Wherein the acid solution adopts dilute hydrochloric acid solution; the more uniform activated carbon is obtained through screening; then, metal impurities doped in the activated carbon or impurities such as dust on the surface of the activated carbon can be subjected to acid washing. Through carrying out activation modification operation to the activated carbon, the surface of the activated carbon is smoother, and simultaneously more and smaller holes can appear, so that the adsorption effect of the activated carbon can be effectively improved, and the gas molecules are realized
In this embodiment, a plurality of auxiliary barrier plates are also uniformly disposed on the inner side wall of the cold screen 2, one end of each of the plurality of auxiliary barrier plates is uniformly and fixedly disposed on the cold screen 2, and the other end extends toward the cold umbrella 3 and is provided with a gap.
In the preferred embodiment, be provided with a plurality of auxiliary barrier boards on cold screen 2's inside wall, can assist to adsorb and solidify the gas molecule, realize the vacuum state fast, can also reflect the heat radiation that produces simultaneously, avoid the temperature to produce great drift, influence the stability of vacuum environment.
The condensation temperatures of the first cold umbrella sheet 31 and the second cold umbrella sheet 32 are different.
The outer surfaces of the first cold umbrella sheet 31 and the second cold umbrella sheet 32 are coated with an adsorbent, and more preferably, the adsorbent in this embodiment is activated carbon, and in a limited space, molecules can be quickly adsorbed and solidified thereon to form a high vacuum state. In a preferred embodiment, the condensation temperature of the first cold umbrella sheet 31 is 15K, the condensation temperature of the second cold umbrella sheet 32 is 80K, and the arrangement of the second cold umbrella structure can effectively reduce direct impact of gas direct current on the first cold umbrella structure, so that a part of molecules can be adsorbed firstly, and then the gas enters the first cold umbrella structure and then is further adsorbed and solidified; meanwhile, according to the difference of condensation temperatures of the first cold umbrella sheet 31 and the second cold umbrella sheet 32, the first cold umbrella sheet 31 and the second cold umbrella sheet 32 adsorb different kinds of molecules in the cavity respectively, so that the adsorption is more complete, and the needed vacuum environment is ensured.
On the basis of the technical scheme, a shock absorber or a vibration isolator is arranged on the driving mechanism 6.
Preferably, a shock absorber or an isolator is arranged on the driving motor 61, so that vibration transmission of the driving motor 61 in the working process is reduced, adverse effects on processing of chips in a process chamber are avoided, processing precision is guaranteed, and meanwhile, the working environment is effectively improved.
More preferably, the damper in the present embodiment is one of a rubber damper, a spring damper, or an air cushion damper. The vibration isolator is one of an active vibration isolator, a rubber vibration isolator, an air spring vibration isolator and an air cushion vibration isolator. Particularly, the device for actively eliminating the vibration of the active vibrator can realize the effect of eliminating the vibration by monitoring and collecting vibration signals in real time and generating anti-vibration force with opposite phase and amplitude through a built-in control system.
On the basis of the technical scheme, the device also comprises a detection device 12 arranged on the outer shell 1, wherein the detection device 12 comprises a temperature detector and a vacuum degree detector.
The vacuum degree detector adopts a vacuum gauge and is used for detecting the vacuum degree in the pump; the temperature detector adopts a temperature sensor, preferably a silicon diode temperature sensor, and realizes accurate temperature detection, especially low temperature detection of 10K, namely-263.15 ℃, in a cryopump.
When the low-temperature pump is used, the low-temperature pump is hung on a process chamber, which is called a process chamber for short, of a chip processing process chamber, and a plurality of low-temperature pump devices can be arranged on the process chamber according to actual use requirements so as to ensure the vacuum degree in the process chamber; pressurizing helium through a compressor and conveying the helium into a low-temperature pump, wherein a helium inlet pipe and a helium outlet pipe are correspondingly arranged on an air inlet valve and an air outlet valve, so that the process of air inlet and air outlet of the helium is realized; then under the driving action of the driving mechanism, the first-stage piston and the second-stage piston realize reciprocating motion, helium gas expands, absorbs heat and refrigerates, realizes the low-temperature states of the first-stage cold head, the second-stage cold head, the cold screen and the cold umbrella, and needs to reach the temperature of 10K263.15 ℃ to discharge the helium gas after heat exchange; the adsorbent attached to the cold umbrella can adsorb and solidify gas molecules in the environment at a low temperature close to absolute zero to form a high vacuum environment, can realize vacuum pressure of 10 -9 Pa and pure vacuum space, and is particularly suitable for the semiconductor industry with high processing precision requirements, such as the processing of heavy metal coating films of chips. When needing to regenerate the cryopump, can adopt the electrical heating stick to heat in to two-stage cold head and the cold umbrella, adsorb the molecule of solidification in the cold umbrella and release, conveniently clear up and change the impurity of inside cold umbrella isotructure, the air blowing valve on the shell body of cooperation simultaneously, supplementary clear up the process, it is more convenient to use.
Example 2
Based on the above technical solution, in this embodiment, a plurality of layers of copper mesh 42 are disposed inside the first-stage piston 41, lead particles are filled in the copper mesh 42, and air inlet holes and air outlet holes are disposed at two ends of the first-stage piston 41 and/or the second-stage piston 51.
It will be appreciated that the mesh diameter of the copper mesh 42 is smaller than the diameter of the lead particles, which limits the range of lead particles.
Preferably, the refrigeration gas is helium; by arranging the air inlet holes and the air outlet holes on the first-stage piston 41 or the second-stage piston 51 or both pistons, the refrigerating gas flows in the first-stage piston 41 or the second-stage piston 51; in the preferred embodiment, lead particles and a plurality of layers of compact copper nets 42 are arranged in the first section of piston 41, so that the heat exchange of passing helium is realized, the drift and fluctuation of temperature and vacuum degree are reduced, and the stability of a processing environment is ensured; especially, the lead particles filled in the helium gas filter has the function of filtering, so that impurities in the helium gas can be removed in the flowing process of the helium gas, and the working efficiency of the helium gas is improved.
Preferably, the first-stage piston 41 and the second-stage piston 51 need to maintain high coaxiality, and meanwhile, the inner side wall of the cylinder housing 11 needs to maintain high smoothness and smoothness, so as to achieve uniformity of helium gas entering and exiting, reduce running noise and refrigeration effect.
The shells of the first-stage piston 41 and the second-stage piston 51 are made of bakelite, and the wear resistance, the low temperature resistance and the pressure resistance are good.
The head end and the tail end are defined according to the direction of approaching the cold umbrella position, and the tail end is defined for the convenience of understanding and describing the technical scheme, and do not limit the application.
Example 3
In this embodiment, the adsorbent is biomass charcoal, and the preparation method of biomass charcoal includes the following steps:
step one, cleaning and drying the collected biomass material;
Step two, placing the biomass material obtained in the step one in a tube furnace for calcination, and performing heat treatment for 6 hours at 500 ℃ in an inert atmosphere to obtain a biomass charcoal material;
And thirdly, grinding the biomass charcoal material obtained in the second step to obtain the final biomass charcoal.
The biomass material includes, but is not limited to, chestnut shell, walnut shell, coconut shell, straw.
In the embodiment, biomass is used as a basic raw material to prepare the carbon adsorption substance, the raw material is wide, the preparation method is simple, the stability is good, and the adsorption of gas molecules can be realized in a low-temperature state to reach the required vacuum degree.
Example 4
On the basis of the technical scheme, the air conditioner further comprises a heating device 8, wherein the heating device 8 is arranged in an air cylinder shell 11, the end part of the heating device is fixedly arranged at the head end of the secondary cold head 5, the air cylinder shell 11 is fixedly arranged on one side of the outer shell 1 and is in through connection, and the primary cold head 4 and the secondary cold head 5 are arranged in the air cylinder shell 11.
It can be appreciated that the cylinder shell 11 is communicated with the outer shell 1, so that the assembly between the secondary cold head 5 and the cold umbrella 3 is facilitated. Preferably, in this embodiment, the heating device 8 is configured as a heating rod, the heating rod is disposed in the cylinder housing 11 in a penetrating manner, one end of the heating rod is disposed at the head end of the secondary cold head 5, that is, at the cold umbrella 3, so that the cold umbrella 3 is heated conveniently, and the other end is connected with a power supply. More preferably, the heating rod is fixedly connected with the cylinder shell 11 through a plurality of fixing sheets, so that the heating rod is convenient to assemble, disassemble and fix.
The heating rod is arranged, so that the temperature of the cold head and the connected cold umbrella 3 structure can be raised; when the low-temperature pump is required to be regenerated and maintained, when the molecules adsorbed and solidified in the cold umbrella 3 are released, the heating rod is adopted to heat the cold head, the vacuum degree is released, the daily maintenance such as impurity removal or cold umbrella part replacement is convenient, and the use is more convenient and quick.
On the basis of the technical scheme, the air blowing valve 9 is arranged on the outer shell 1, and the output end of the air blowing valve 9 is arranged in the cold screen 2.
Through being provided with the air valve 9 on outer housing 1, conveniently clean cold umbrella 3 or cold screen 2 inner chamber, in the regeneration period of cryopump, can assist the impurity that cold screen 2 inside exists to carry out timely clear away, the operation is more convenient, makes things convenient for daily maintenance.
While the basic principles and main features of the present invention have been shown and described above, it will be apparent to those skilled in the art that the present invention is not limited to the details of the above-described exemplary embodiments, and thus the embodiments should be regarded as illustrative rather than restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes that come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.
Claims (10)
1. The low-temperature vacuum pump with excellent vacuum stability is characterized by comprising an outer shell (1), a cold screen (2), a cold umbrella (3) and a refrigerating device; the cold screen (2) is fixedly arranged in the outer shell (1) and is structurally matched with the outer shell (1), the cold umbrella (3) is arranged in the cold screen (2), an adsorbent is coated on the surface of the cold umbrella (3), and the refrigerating device is connected with the cold umbrella (3) to provide refrigeration for the inside of the cold screen (2); the cold screen (2) is characterized in that a nickel coating is plated on the inner side wall of the cold screen (2), a plurality of auxiliary screen plates are uniformly arranged on the inner side wall of the cold screen (2), one ends of the auxiliary screen plates are uniformly and fixedly arranged on the cold screen (2), and the other ends of the auxiliary screen plates extend to the cold umbrella (3) and are provided with gaps.
2. The cryogenic vacuum pump with excellent vacuum stability according to claim 1, wherein the refrigerating device comprises a primary cold head (4), a secondary cold head (5) and a driving mechanism (6), the primary cold head (4) is used for cooling a cold screen (2), the secondary cold head (5) is used for cooling a cold umbrella (3), a first section of piston (41) is arranged in the primary cold head (4), a second section of piston (51) is arranged in the secondary cold head (5), the second section of piston (51) is fixedly arranged at the top end of the first section of piston (41), the tail end of the first section of piston (41) is connected with the driving mechanism, and refrigerating gas flows in the primary cold head (4) and the secondary cold head (5).
3. The low-temperature vacuum pump with excellent vacuum stability according to claim 2, wherein a plurality of layers of copper nets (42) are arranged in the first-stage piston (41), lead particles are filled in the copper nets (42), and air inlets and air outlets are formed at two ends of the first-stage piston (41) and/or the second-stage piston (51).
4. The cryogenic vacuum pump with excellent vacuum stability according to claim 2, wherein the driving mechanism (6) comprises a driving motor (61), an eccentric shaft (62), an eccentric wheel (63) and a driving frame (64), the eccentric shaft (62) is driven to rotate by the driving motor (61), the eccentric wheel (63) is fixedly sleeved on the eccentric shaft (62), the eccentric wheel (63) is arranged in the driving frame (64), and the driving frame (64) is connected with a section of piston (41).
5. The cryogenic vacuum pump with excellent vacuum stability according to claim 1, characterized in that the cold umbrella (3) comprises a first cold umbrella structure and a second cold umbrella structure, the second cold umbrella structure being arranged at the top end of the first cold umbrella structure; the first cold umbrella structure comprises a plurality of first cold umbrella pieces (31) and is fixedly arranged from top to bottom in sequence, the second cold umbrella structure comprises a plurality of second cold umbrella pieces (32), and the diameter of the second cold umbrella pieces (32) is sequentially increased from inside to outside.
6. The cryogenic vacuum pump with excellent vacuum stability according to claim 5, wherein the first cold umbrella sheet (31) comprises an end surface (311) arranged as a plane and a circular side surface (312) and is fixedly connected, and the end surface (311) and the side surface (312) are obliquely arranged; the second cold umbrella sheet (32) is formed by fixedly splicing two circular ring sheets (321) which are arranged in a mirror image mode.
7. The low-temperature vacuum pump with excellent vacuum stability according to claim 5, wherein the first cold umbrella sheets (31) are fixedly arranged on the cold umbrella support (33), a plurality of through holes are formed in the end face of one first cold umbrella sheet (31) positioned at the top end, and a plurality of through holes are formed in the cold umbrella support (33).
8. The cryogenic vacuum pump of claim 1, wherein the adsorbent is modified activated carbon or biomass carbon.
9. A cryopump having excellent vacuum stability according to claim 2, characterized in that the drive mechanism (6) is provided with a damper or vibration isolator.
10. The cryogenic vacuum pump with excellent vacuum stability according to claim 2, further comprising a heating device (8), wherein the heating device (8) is arranged in a cylinder housing (11) and the end part is fixedly arranged at the head end of the secondary cold head (5), the cylinder housing (11) is fixedly arranged at one side of the outer housing (1) and is in through connection, and the primary cold head (4) and the secondary cold head (5) are arranged in the cylinder housing (11).
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CN202410684062.2A CN118517395A (en) | 2023-12-05 | 2023-12-05 | Low-temperature vacuum pump with excellent vacuum stability |
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CN202410684062.2A CN118517395A (en) | 2023-12-05 | 2023-12-05 | Low-temperature vacuum pump with excellent vacuum stability |
CN202311658773.4A CN117489563B (en) | 2023-12-05 | 2023-12-05 | Improved cryogenic pump |
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CN202410684062.2A Pending CN118517395A (en) | 2023-12-05 | 2023-12-05 | Low-temperature vacuum pump with excellent vacuum stability |
CN202410684057.1A Pending CN118462540A (en) | 2023-12-05 | 2023-12-05 | Low-temperature pump convenient to control |
CN202311658773.4A Active CN117489563B (en) | 2023-12-05 | 2023-12-05 | Improved cryogenic pump |
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CN202410684057.1A Pending CN118462540A (en) | 2023-12-05 | 2023-12-05 | Low-temperature pump convenient to control |
CN202311658773.4A Active CN117489563B (en) | 2023-12-05 | 2023-12-05 | Improved cryogenic pump |
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JP2008035604A (en) * | 2006-07-27 | 2008-02-14 | Sumitomo Heavy Ind Ltd | Gm freezer, pulse tube freezer, cryopump, mri device, super-conductive magnet system, nmr device, and freezer for cooling of semiconductor |
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KR200444603Y1 (en) * | 2007-11-09 | 2009-05-25 | 주식회사스타백 | Absortion structure for Cryo pump cold panel |
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JP5527110B2 (en) * | 2010-08-27 | 2014-06-18 | アイシン精機株式会社 | Cryopump |
JP5398780B2 (en) * | 2011-05-12 | 2014-01-29 | 住友重機械工業株式会社 | Cryopump |
CN203404038U (en) * | 2013-08-10 | 2014-01-22 | 安徽万瑞冷电科技有限公司 | High-efficiency regenerating cryogenic pump |
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CN115324868A (en) * | 2022-09-20 | 2022-11-11 | 安徽万瑞冷电科技有限公司 | Water vapor pumping low-temperature pump and water vapor pumping speed testing method |
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2023
- 2023-12-05 CN CN202410684062.2A patent/CN118517395A/en active Pending
- 2023-12-05 CN CN202410684057.1A patent/CN118462540A/en active Pending
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CN117489563A (en) | 2024-02-02 |
CN118462540A (en) | 2024-08-09 |
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