CN118217197A - Composition with anti-wrinkle effect and preparation method thereof - Google Patents
Composition with anti-wrinkle effect and preparation method thereof Download PDFInfo
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- CN118217197A CN118217197A CN202410263713.0A CN202410263713A CN118217197A CN 118217197 A CN118217197 A CN 118217197A CN 202410263713 A CN202410263713 A CN 202410263713A CN 118217197 A CN118217197 A CN 118217197A
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a composition with anti-wrinkle effect and a preparation method thereof, belonging to the technical field of cosmetics, wherein the composition comprises the following raw materials: mistletoe extract, quince extract, yarrow extract, alpine leontopodium extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract, ylang-ylang flower extract, provitamin B5 and a solvent. The invention combines mistletoe extract, quince extract, yarrow extract and alpine leonia extract, and respectively starts with the multi-dimension of inhibiting collagenase, inhibiting elastase, promoting the elastic recovery of skin fibrous tissues and promoting the generation of endothelin, and the prepared composition finished product has excellent anti-wrinkle effect by synergism; the Chinese aralia extract, the grifola frondosa extract and the Chinese angelica extract are combined to cooperate, so that the prepared composition has excellent moisturizing effect; meanwhile, the invention further strengthens the action and effect of the composition by the ylang-ylang flower extract and provitamin B5.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a composition with an anti-wrinkle effect and a preparation method thereof.
Background
With the increase of the age and the continuous improvement of the living standard of people, the demands of consumers on skin care products gradually develop from basic cleaning to higher anti-wrinkle, moisturizing and other aspects. The root causes of skin wrinkles are collagen loss of skin, lack of natural moisturizing factors, and excessive water loss of stratum corneum. Therefore, products with the effects of resisting wrinkles, moisturizing and moisturizing are paid attention to, and become one of the hot spots in the current cosmetic industry. The existing cosmetic with anti-wrinkle effect is in full view, but the effect is poor, and the important point is how to resist wrinkles, and the problem that the anti-wrinkle effect can be achieved substantially only by simultaneously supplementing water and resisting wrinkles is neglected, in other words, the existing composition on the market has single function and slightly poor effect. Therefore, the composition with the anti-wrinkle, water-retaining and moisturizing effects is very important to meet the increasing consumer demands.
Disclosure of Invention
The invention aims to provide a composition with anti-wrinkle effect and a preparation method thereof, wherein mistletoe extract, quince extract, achillea extract and alpine leonardite extract are combined, and the composition has excellent anti-wrinkle effect by cooperation from the multi-dimension of inhibiting collagenase, inhibiting elastase, promoting elastic recovery of skin fibrous tissues and promoting endothelin generation; the Chinese aralia extract, the grifola frondosa extract and the Chinese angelica extract are combined to cooperate, so that the prepared composition has excellent moisturizing effect; meanwhile, the invention further strengthens the action and effect of the composition by using the ylang-ylang flower extract and provitamin B5; solves the problem of poor crease resistance, moisturizing effect of the composition in the prior art.
The aim of the invention can be achieved by the following technical scheme:
the composition with the anti-wrinkle effect comprises the following raw materials in parts by weight:
As a preferred technical scheme of the invention, the mistletoe extract, the quince extract, the yarrow extract, the aralia chinensis extract and the angelica sinensis extract are all obtained by extracting the raw materials and the extracting solvent according to the ratio of 1:10 by a conventional room temperature soaking method and concentrating the extracting solution to be dry; the alpine leontopodium herb extract and the grifola frondosa extract are obtained by extracting the raw materials and the extracting solvent according to the ratio of 1:15 by a conventional room temperature soaking method and concentrating the extracting solution to dryness.
The extract of herba Visci is prepared from dried leaves, stems and branches of herba Visci of Moraceae; the quince extract is prepared from the fruit of Cydonia oblonga belonging to the family Rosaceae; the yarrow extract is prepared from whole plant of yarrow of Compositae; the extract of herba Lespedezae Cuneatae is prepared from whole plant of herba Lespedezae Cuneatae of Lespedezae genus of Compositae family; the extract of Aralia elata is prepared from root of Aralia elata of Araliaceae; the extraction raw material of the grifola frondosa extract is fruiting body of grifola frondosa; the extract of Angelica sinensis (oliv.) Diels is prepared from dried root of Angelica sinensis (oliv.) Diels of Umbelliferae.
As a preferable technical scheme of the invention, the extraction solvents of the mistletoe extract, the quince extract, the yarrow extract and the aralia chinensis extract are ethanol solution with the volume fraction of 50 percent; the extraction solvent of the alpine leontopodium herb extract, the grifola frondosa extract and the angelica sinensis extract is ethanol solution with the volume fraction of 30 percent.
As a preferred embodiment of the present invention, the solvent includes any one of deionized water and propylene glycol.
As a preferred embodiment of the present invention, the composition further comprises 5-9 parts by weight of ylang-ylang flower extract.
As a preferable technical scheme of the invention, the ylang flower extract is obtained by extracting the raw materials and the extracting solvent according to the ratio of 1:10 by a conventional room temperature soaking method and concentrating the extracting solution to be dry.
As a preferable technical scheme of the invention, the extract of the ylang flowers is prepared from flowers of ylang flowers of the Annonaceae ylang genus plants; the extraction solvent of the ylang flower extract is ethanol solution with the volume fraction of 30 percent.
As a preferred embodiment of the present invention, the composition further comprises 10 to 18 parts by weight of provitamin B5.
A method for preparing a composition with anti-wrinkle effect, which specifically comprises the following steps:
s1, uniformly mixing mistletoe extract, quince extract, yarrow extract, alpine leonurus extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract and ylang-ylang flower extract to obtain a mixture for later use;
s2, uniformly mixing the solvent and the provitamin B5, then adding the mixture, and stirring at a controlled temperature to obtain the composition with the anti-wrinkle effect.
As a preferable technical scheme of the invention, the temperature of the temperature-controlled stirring in the step S2 is 25-30 ℃ and the time is 1-1.5h.
As a preferable scheme of the invention, the composition with anti-wrinkle effect is applied by adding the composition into a skin care product according to the mass percentage of 4-6%.
As a preferred embodiment of the present invention, the skin care product includes, but is not limited to, cream, lotion, moisturizing water, essence, mask.
The invention has the beneficial effects that:
(1) According to the invention, the mistletoe extract is added to inhibit collagenase, the quince extract is added to inhibit elastase, the mistletoe extract and the quince extract effectively reduce the loss of collagen and elastin, maintain the elasticity and compactness of skin, and reduce the generation of wrinkles to a certain extent; on the basis, the achillea extract is added to proliferate the epidermal keratinocytes, so as to promote the recovery of the skin fibrous tissue elasticity; the addition of the alpine leontopodium herb extract promotes the generation of endothelin so as to further maintain the skin elasticity; namely mistletoe extract, quince extract, yarrow extract and alpine leontopodium extract respectively start from the multi-dimensional degree of inhibiting collagenase, inhibiting elastase, promoting the elastic recovery of skin fibrous tissues and promoting the generation of endothelin, and the prepared composition finished product has excellent anti-wrinkle effect by synergism.
(2) According to the invention, the aralia chinensis extract is used for inhibiting hyaluronidase, so that decomposition of hyaluronic acid is inhibited, meanwhile, the ash flower extract is used for promoting generation of hyaluronic acid, so that moisture is absorbed by skin, on the basis, the angelica extract is used for promoting generation of natural moisturizing factors in epidermal cells, so that moisture is absorbed and combined, and the moisture content of skin cuticle is maintained, so that the three components can cooperate to ensure that the prepared composition has excellent moisturizing effect.
(3) The factors influencing the skin permeation speed and degree are various, wherein the skin hydration is one of the main factors, and the ylang flower extract added in the invention can effectively promote the activity of the protein lyase related to mRNA, improve the hydration capacity of the cortex, and simultaneously, the vitamin B5 is added to open the skin channel and help the skin to absorb other active ingredients; namely, the ylang flower extract and provitamin B5 respectively start from improving the hydration capacity of the cortex and opening the skin channel, so that other active ingredients in the composition can be better absorbed, and the action and effect of the composition are enhanced; in addition, the ylang-ylang flower extract can improve the hydration capability of the cortex, so that the moisturizing effect of the composition can be enhanced by the aralia chinensis extract, the grifola frondosa extract and the angelica sinensis extract.
Detailed Description
The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
The composition with the anti-wrinkle effect comprises the following raw materials in parts by weight:
the preparation method of the composition with the anti-wrinkle effect specifically comprises the following steps:
s1, uniformly mixing mistletoe extract, quince extract, yarrow extract, alpine leonurus extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract and ylang-ylang flower extract to obtain a mixture for later use;
S2, uniformly mixing the solvent and the provitamin B5, then adding the mixture prepared in the step S1, and stirring for 1h at the temperature of 25 ℃ to obtain the composition with the anti-wrinkle effect.
The composition with the anti-wrinkle effect is added into a skin care product according to the mass percentage of 4%, wherein the skin care product is essence.
Example 2
The composition with the anti-wrinkle effect comprises the following raw materials in parts by weight:
the preparation method of the composition with the anti-wrinkle effect specifically comprises the following steps:
s1, uniformly mixing mistletoe extract, quince extract, yarrow extract, alpine leonurus extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract and ylang-ylang flower extract to obtain a mixture for later use;
S2, uniformly mixing the solvent and the provitamin B5, then adding the mixture prepared in the step S1, and stirring for 1h at the temperature of 28 ℃ to obtain the composition with the anti-wrinkle effect.
The composition with the anti-wrinkle effect is added into a skin care product according to the mass percentage of 5%, wherein the skin care product is emulsion.
Example 3
The composition with the anti-wrinkle effect comprises the following raw materials in parts by weight:
the preparation method of the composition with the anti-wrinkle effect specifically comprises the following steps:
s1, uniformly mixing mistletoe extract, quince extract, yarrow extract, alpine leonurus extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract and ylang-ylang flower extract to obtain a mixture for later use;
s2, uniformly mixing the solvent and the provitamin B5, then adding the mixture prepared in the step S1, and stirring for 1.5 hours at the temperature of 30 ℃ to obtain the composition with the anti-wrinkle effect.
The composition with the anti-wrinkle effect is added into a skin care product according to the mass percentage of 6%, wherein the skin care product is moisturizing water.
Comparative examples 1 to 4
The difference compared to example 1 is that the parts by weight of mistletoe extract, quince extract, tragacanth extract and alpine leontopodium extract in comparative examples 1-4 are shown in table 1, and the remaining parameters and operation steps are unchanged.
TABLE 1
Comparative examples 5 to 7
The difference compared with example 1 is that the parts by weight of the aralia chinensis extract, the Grifola frondosa extract and the Angelica sinensis extract in comparative examples 5 to 7 are shown in Table 2, and the remaining parameters and the operation steps are not changed.
TABLE 2
Comparative example 8
In comparison with example 1, the difference is that no orchid extract was added in comparative example 8, and the remaining parameters and the procedure were unchanged.
Comparative example 9
In comparison with example 1, the difference is that no provitamin B5 was added in comparative example 9, and the remaining parameters and the procedure were unchanged.
Test example 1
Anti-wrinkle test: 90 female volunteers 30-65 years old were randomly selected as subjects, and were randomly divided into 9 groups of 10 persons each; each group of volunteers used a finished essence product (the addition amount of the composition in the fine bloom was 4%) prepared by adding the compositions having anti-wrinkle effect prepared in the steps S2 of examples 1 to 3, comparative examples 1 to 4 and comparative examples 8 to 9, respectively, to the same essence base. After the subject had been allowed to sit still for 30 minutes in a constant temperature and humidity environment at 23℃and 60% humidity after washing the face before the test, a photograph of the face was taken as primary data by VISA-CR.
The specific using method comprises the following steps: subjects uniformly apply 1mL of the corresponding essence to the face and massage the face until the essence is completely absorbed, use the essence 1 time a day, and continue to use for 28 days. After washing the face on day 0 and day 28, facial wrinkle tests were performed with VISA-CR, designated as D0 and D28, respectively. Each set of D0 and D28 values is the average of the set of these values, and the lower the score, the more wrinkles are indicated by the instrumental software calculation of the improvement in facial wrinkles before and after use; the results are shown in Table 3.
TABLE 3 Table 3
As can be seen from table 3, the composition with anti-wrinkle effect prepared by the present invention has excellent anti-wrinkle effect. Specifically, as can be seen from comparative examples 1 to 4, the present invention combines the four extracts of mistletoe extract, quince extract, tragacanth extract and alpine leontopodium extract, and the obtained composition has excellent anti-wrinkle effect by cooperation starting from the multi-dimensions of inhibiting collagenase, inhibiting elastase, promoting elastic recovery of skin fibrous tissue and promoting endothelin production, respectively. As can be seen from comparative examples 8 to 9, the ylang flower extract and provitamin B5 added in the present invention can make the anti-wrinkle effect of the composition having anti-wrinkle effect more excellent to some extent.
Test example 2
And (3) water supplementing and moisturizing test: 48 male and female volunteers (96 total) aged 38-52 years were randomly selected and randomly divided into 8 groups of 12 volunteers each, and each group of volunteers was finished essence products (the addition amount of the composition in the fine bloom was 4%) prepared by adding the compositions with anti-wrinkle effects prepared in steps S2 of examples 1-3 and comparative examples 5-9 to the same essence base.
The application method comprises uniformly applying 1mL of the essence product on the cheek region of face, massaging to completely absorb, and applying once a day in the morning and evening for 28 days without using other skin care products.
Measuring the skin moisture content of the application part by using a skin moisture content tester before and after the product is used for 28 days, wherein the test of the same subject is carried out by the same instrument and the same tester, thereby evaluating the moisture content of the skin before and after the essence finished product is used; the results are shown in Table 4.
TABLE 4 Table 4
As can be seen from Table 4, the composition with anti-wrinkle effect prepared by the present invention has excellent moisturizing effect. In detail, as can be seen from comparative examples 5 to 7, the three added in the present invention, the aralia chinensis extract, the grifola frondosa extract and the angelica sinensis extract, can synergistically make the prepared composition have excellent moisturizing effect. As can be seen from comparative examples 8 to 9, the provitamin B5 added in the present invention can enhance the effect of the composition; the added ylang flower extract can further assist the water supplementing and moisturizing effects of the composition reinforced by the aralia chinensis extract, the grifola frondosa extract and the angelica sinensis extract.
In the description of the present specification, the descriptions of the terms "one embodiment," "example," "specific example," and the like, mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiments or examples. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing is merely illustrative and explanatory of the invention, as various modifications and additions may be made to the particular embodiments described, or in a similar manner, by those skilled in the art, without departing from the scope of the invention or exceeding the scope of the invention as defined in the claims.
Claims (10)
1. The composition with the anti-wrinkle effect is characterized by comprising the following raw materials in parts by weight:
2. The composition with anti-wrinkle effect according to claim 1, wherein the mistletoe extract, quince extract, yarrow extract, aralia chinensis extract, angelica extract are all obtained by extracting raw materials and extracting solvent in a ratio of 1:10 by a conventional room temperature soaking method and concentrating the extract to dryness; the alpine leontopodium herb extract and the grifola frondosa extract are obtained by extracting the raw materials and the extracting solvent according to the ratio of 1:15 by a conventional room temperature soaking method and concentrating the extracting solution to dryness.
3. The composition with anti-wrinkle effect according to claim 2, wherein the extraction solvents of mistletoe extract, quince extract, tragacanth extract, aralia chinensis extract are all ethanol solutions with volume fraction of 50%; the extraction solvent of the alpine leontopodium herb extract, the grifola frondosa extract and the angelica sinensis extract is ethanol solution with the volume fraction of 30 percent.
4. The composition having anti-wrinkle effect according to claim 1, wherein the solvent comprises any one of deionized water and propylene glycol.
5. The composition having anti-wrinkle effect according to claim 1, further comprising 5 to 9 parts by weight of ylang-ylang flower extract.
6. The composition with anti-wrinkle effect according to claim 5, wherein the ylang-orchid extract is obtained by extracting raw materials and an extraction solvent in a ratio of 1:10 by a conventional room temperature immersion method and concentrating the extract to dryness.
7. The composition with anti-wrinkle effect according to claim 6, wherein the extraction solvent of the ylang-ylang flower extract is an ethanol solution with a volume fraction of 30%.
8. The composition with anti-wrinkle effect according to claim 5, further comprising 10-18 parts by weight of provitamin B5.
9. A method for preparing a composition having anti-wrinkle effect according to claim 8, comprising the steps of:
s1, uniformly mixing mistletoe extract, quince extract, yarrow extract, alpine leonurus extract, aralia elata extract, grifola frondosa extract, angelica sinensis extract and ylang-ylang flower extract to obtain a mixture for later use;
s2, uniformly mixing the solvent and the provitamin B5, then adding the mixture, and stirring at a controlled temperature to obtain the composition with the anti-wrinkle effect.
10. The method for preparing an anti-wrinkle composition according to claim 9, wherein the temperature of the temperature-controlled stirring in step S2 is 25-30 ℃ for 1-1.5h.
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| CN103687586A (en) * | 2012-01-23 | 2014-03-26 | 雷斯托尔西有限公司 | Cosmetic |
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| CN115350128A (en) * | 2022-09-22 | 2022-11-18 | 广州市涵美化妆品有限公司 | Skin-brightening anti-wrinkle composition and preparation method and application thereof |
| CN118001205A (en) * | 2024-04-10 | 2024-05-10 | 威莱(广州)日用品有限公司 | Anti-wrinkle active composition and application thereof, and anti-wrinkle cream |
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| CN103687586A (en) * | 2012-01-23 | 2014-03-26 | 雷斯托尔西有限公司 | Cosmetic |
| CN107149588A (en) * | 2012-01-23 | 2017-09-12 | 雷斯托尔西有限公司 | Cosmetic composition |
| CN104055713A (en) * | 2014-07-08 | 2014-09-24 | 广州千百度化妆品有限公司 | Wrinkle-dispelling cosmetic composition and preparation method thereof |
| CN108430487A (en) * | 2015-10-20 | 2018-08-21 | 瓦尔比奥蒂斯公司 | Including the composition of the molecule mixture extracted from golden yellow chamomile, arithoke and matrimony vine and its acting on the purposes of carbohydrate and/or fat metabolism |
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Effective date of registration: 20241011 Address after: Building 6, No. 22 Chuncheng Road, High tech Zone, Luoyang Area, China (Henan) Pilot Free Trade Zone, Luoyang City, Henan Province 471000 Applicant after: Luoyang Lanhua Medical Beauty Co.,Ltd. Country or region after: China Address before: Room 205, Building 2, No. 28 Luogang Mumiantang East Road, Junhe Street, Baiyun District, Guangzhou City, Guangdong Province, 510080 Applicant before: Quanzhi (Guangdong) Biotechnology Co.,Ltd. Country or region before: China |