CN118121525A - Perfume containing armyworm scent gland secretion and preparation method and application thereof - Google Patents
Perfume containing armyworm scent gland secretion and preparation method and application thereof Download PDFInfo
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- CN118121525A CN118121525A CN202410371718.5A CN202410371718A CN118121525A CN 118121525 A CN118121525 A CN 118121525A CN 202410371718 A CN202410371718 A CN 202410371718A CN 118121525 A CN118121525 A CN 118121525A
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- 210000001104 scent gland Anatomy 0.000 title claims abstract description 124
- 241001477931 Mythimna unipuncta Species 0.000 title claims abstract description 85
- 239000002304 perfume Substances 0.000 title claims abstract description 54
- 230000028327 secretion Effects 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title abstract description 14
- 229940098465 tincture Drugs 0.000 claims abstract description 86
- 241000282375 Herpestidae Species 0.000 claims abstract description 44
- 239000003205 fragrance Substances 0.000 claims abstract description 26
- 241000402754 Erythranthe moschata Species 0.000 claims abstract description 22
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 239000008213 purified water Substances 0.000 claims description 16
- 241000578422 Graphosoma lineatum Species 0.000 claims description 13
- FACFHHMQICTXFZ-UHFFFAOYSA-N 2-(2-phenylimidazo[1,2-a]pyridin-3-yl)ethanamine Chemical compound N1=C2C=CC=CN2C(CCN)=C1C1=CC=CC=C1 FACFHHMQICTXFZ-UHFFFAOYSA-N 0.000 claims description 12
- 229940067137 musk ketone Drugs 0.000 claims description 12
- 230000002431 foraging effect Effects 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 8
- ALHUZKCOMYUFRB-OAHLLOKOSA-N Muscone Chemical compound C[C@@H]1CCCCCCCCCCCCC(=O)C1 ALHUZKCOMYUFRB-OAHLLOKOSA-N 0.000 claims description 7
- ALHUZKCOMYUFRB-UHFFFAOYSA-N muskone Natural products CC1CCCCCCCCCCCCC(=O)C1 ALHUZKCOMYUFRB-UHFFFAOYSA-N 0.000 claims description 7
- 230000032683 aging Effects 0.000 claims description 6
- 241000196324 Embryophyta Species 0.000 claims description 5
- 241000972155 Moschus Species 0.000 claims description 5
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 210000004907 gland Anatomy 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 230000007774 longterm Effects 0.000 abstract description 2
- 239000000834 fixative Substances 0.000 abstract 1
- 210000001015 abdomen Anatomy 0.000 description 22
- 239000003153 chemical reaction reagent Substances 0.000 description 9
- 241000258937 Hemiptera Species 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 239000000126 substance Substances 0.000 description 5
- 239000003755 preservative agent Substances 0.000 description 4
- 238000001514 detection method Methods 0.000 description 3
- 229910001385 heavy metal Inorganic materials 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 241000243812 Arenicola marina Species 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000001479 atomic absorption spectroscopy Methods 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
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- Fats And Perfumes (AREA)
Abstract
The invention discloses a perfume containing armywood scent gland secretion, a preparation method and application thereof. The perfume consists of one hundred parts of armyworm scent gland tincture and seven parts of perfume fixative according to the volume parts. The tincture is armyworm scent gland tincture, and the perfume fixing agent is musk tincture or civet tincture. The perfume of the invention can improve the comprehensive application value of army bugs, and the designed perfume has good fragrance retaining effect, clean and fresh fragrance, elegant and pleasant fragrance, and can calm spirit and calm and refresh mind after long-term use.
Description
Technical Field
The invention belongs to the technical field of perfumes, and particularly relates to a perfume containing armyworm scent gland secretion and a preparation method thereof.
Background
The perfume is a liquid with fragrance, has aromatic and strong fragrance, has different types of fragrance according to the differences of different raw materials and the preparation method, has the main functions of being sprayed on the positions of a placket, handkerchief, hairline and the like, emits pleasant fragrance, and is one of important cosmetics. The existing perfume mainly takes plants and few animals as raw materials, but the perfume taking insects as raw materials is not involved. People often prey on stinkbug insects, and consider that the stinkbug insects are closely connected with 'stinkbook', so that people cannot avoid the stinkbug insects.
Disclosure of Invention
The invention provides a perfume manufacturing thought and a perfume manufacturing method using stinkbug insects scent gland as raw materials, which break through the impression of people on stinkbug insects in the background technology.
In order to achieve the above object, the present invention is realized by the following experimental technique:
A perfume containing the secretion of armyworm scent gland, characterized in that: it comprises 100 parts of tincture and 7 parts of fragrance fixing agent; the tincture is armyworm scent gland tincture, and the perfume fixing agent is musk tincture or civet tincture.
The invention further discloses a preparation method of the perfume containing the armyworm scent gland secretion, which is characterized by comprising the following steps:
S1, dissecting and extracting armyworm scent gland: selecting male armyworms (armyworms used in the invention are all purchased from the Coriolis organisms), dissecting and extracting scent gland; in the step S1, the male armyworm is required to be inserted into the chest with its abdomen facing upward and fixed by a pin, and the chest and abdomen are separated by pulling the abdomen outward with forceps. Gently spreading the belly shell to find orange scent gland, picking up scent gland with a dissecting needle, putting into a 2ml reagent bottle, and covering a reagent bottle cap to prevent scent gland smell from escaping;
S2, preparing a armyworm scent gland tincture: grinding the dissected scent gland, and adding the double dealdehyding alcohol (the double dealdehyding alcohol used in the invention is purchased from Micheles and the purity is 96%) to obtain armywood scent gland tincture; adding 0.01-0.06 ml of didehydroaldehyde alcohol into each armyworm scent gland;
S3, preparing musk tincture:
Mixing muscone (the muscone used in the invention is purchased from microphone with the purity of 97%) with didehydroaldehyde alcohol, shaking, standing for aging for one week, and adding purified water to obtain musk tincture; the musk ketone is as follows: double dealdehyding alcohol: the volume ratio of the purified water is 1:500:500;
S4, preparing a civet tincture:
mixing civet (the civet used in the invention is purchased from source leaves and has the purity of 80%) with double dealdehydized alcohol, shaking and standing for aging for one week, wherein the civet is prepared by the following steps: the volume ratio of the double dealdehyding alcohols is 1:1000;
s5, armyworm perfume ratio
Mixing armyworm scent gland tincture, musk tincture or civet tincture, shaking, and aging for 1 hr to obtain perfume containing armyworm scent gland secretion; the volume ratio of the armyworm scent gland tincture to the musk tincture is 100:7, preparing a base material; the volume ratio of the stinkbug scent gland tincture to the civet tincture is 10:1.
The invention further discloses application of the armyworm scent gland secretion perfume in preparing perfume with fresh and unique smell; wherein the perfume containing fresh and unique odor means: the wet air after rain kneads the fresh taste of the plant juice. Experimental results prove that: the tincture of armywood scent gland is mixed with the perfume fixing agent, which retains the fresh and unique smell contained in the secretion of armywood scent gland and adds the taste of plant juice kneaded in the wet air after rain.
The invention mainly solves the problem of blank application of armyworm in perfume preparation, and mainly examines the preparation process of animal-source perfume, and has the main difficulty in retaining and concentrating the odor of armyworm scent gland.
The detection of technical indexes in the armyworm scent gland secretion-containing perfume prepared by the invention mainly comprises the following steps:
(1) Heavy metal content test: the invention uses atomic absorption spectrometry to detect some heavy metal elements such as lead, mercury, cadmium and the like, which have potential threat to human health, and the invention does not contain heavy metals through detection.
(2) Preservative content test: preservatives in perfumes may produce allergic or irritating reactions to human skin. The invention accurately tests the content of the preservative, ensures the safety of the product, and does not contain the preservative after detection.
(3) Chemical composition test: the safety of chemical components in perfume is evaluated, the measurement method is gas chromatography-mass spectrometry (GC-MS), and the chemical components are detected, so that the safety of the chemical components is shown in table 1.
TABLE 1 GC chemical composition test results of MS
The formula of the prepared perfume containing the armyworm scent gland secretion relates to musk tincture, civet tincture and armyworm scent gland tincture, so that the armyworm is fresh and unique in fragrance, the comprehensive application value of armyworms can be improved, the designed perfume has fresh taste of plant juice when being rubbed into humid air after rain, and thin water vapor and light green meaning are like a forest just after rain.
Detailed Description
The invention is described below by means of specific embodiments. The technical means used in the present invention are methods well known to those skilled in the art unless specifically stated. Further, the embodiments should be construed as illustrative, and not limiting the scope of the invention, which is defined solely by the claims. Various changes or modifications to the materials ingredients and amounts used in these embodiments will be apparent to those skilled in the art without departing from the spirit and scope of the invention. The raw materials and reagents used in the invention are all commercially available.
Wherein army bugs used in the embodiments of the invention are purchased from Henan Corp. The double dealdehyding alcohol is purchased from Shanghai Michelson Biochemical technology Co., ltd, and the purity is 96%; musk ketone is purchased from Shanghai Meilin Biotechnology Co., ltd, and the purity is 97%; the civirudin was purchased from Shanghai Secoides Biotechnology Co., ltd and had a purity of 80%.
Example 1
A perfume containing the secretion of armyworm scent gland, which is prepared from the following components in parts by volume;
Armyworm scent gland tincture (0.03 ml of didehydroalditol is added to each armyworm scent gland): the musk tincture (the volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500) is 100:7, preparing a base material; the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.03ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing muscone with double dealdehyded alcohol, shaking, standing for aging for one week, and adding purified water to obtain Moschus tincture. The volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500.
Mixing the tincture of armyworm scent gland and the tincture of musk, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the musk tincture is 100:7.
Example 2
A perfume containing the secretion of armyworm scent gland, which is prepared from the following components in parts by volume;
Armyworm scent gland tincture (0.03 ml of didehydroalditol is added to each armyworm scent gland): the volume ratio of the civet tincture (civet to the didehydroaldehyde alcohol is 1:1000) is 100:7. the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.03ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing the civet with the double dealdehyded alcohol, shaking, standing and aging for one week to obtain the civet tincture. The volume ratio of the civet to the double dealdehyded alcohol is 1:1000.
Mixing the tinctures of armyworm scent gland and civet, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the civet tincture is 100:7.
Example 3
A perfume containing the secretion of armyworm scent gland, which is prepared from the following components in parts by volume;
Armyworm scent gland tincture (0.03 ml of didehydroalditol is added to each armyworm scent gland): musk tincture (the volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500): the volume ratio of the civet tincture (civet to the didehydro alcohol is 1:1000) is 1000:35:35; the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.03ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing muscone with double dealdehyded alcohol, shaking, standing for aging for one week, and adding purified water to obtain Moschus tincture. The volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500.
Mixing the civet with the double dealdehyded alcohol, shaking, standing and aging for one week to obtain the civet tincture. The volume ratio of the civet to the double dealdehyded alcohol is 1:1000.
Mixing the tinctures of armyworm scent gland, musk and civet, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the civet tincture is 1000:35:35.
Example 4
The perfume containing the secretion of armyworm scent gland is prepared from the following components in parts by volume;
armyworm scent gland tincture (0.01 ml of didehydroalditol is added to each armyworm scent gland): the musk tincture (the volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500) is 10:1, a step of; the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.01ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing muscone with double dealdehyded alcohol, shaking, standing for aging for one week, and adding purified water to obtain Moschus tincture. The volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500.
Mixing the tincture of armyworm scent gland and the tincture of musk, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the musk tincture is 10:1.
Example 5
The perfume containing the secretion of armyworm scent gland is prepared from the following components in parts by volume;
Armyworm scent gland tincture (0.01 ml of didehydroalditol is added to each armyworm scent gland): the volume ratio of the civet tincture (civet to the didehydro alcohol is 1:1000) is 10:1, a step of; the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.01ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing the civet with the double dealdehyded alcohol, shaking, standing and aging for one week to obtain the civet tincture. The volume ratio of the civet to the double dealdehyded alcohol is 1:1000.
Mixing the tinctures of armyworm scent gland and civet, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the civet tincture is 10:1.
Example 6
A perfume containing the secretion of armyworm scent gland, which is prepared from the following components in parts by volume;
Armyworm scent gland tincture (0.01 ml of didehydroalditol is added to each armyworm scent gland): musk tincture (the volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500): the volume ratio of the civet tincture (civet to the didehydroaldehyde alcohol is 1:1000) is 100:5:5, a step of; the preparation method comprises the following steps:
selecting male armyworm, dissecting and extracting scent gland. Male army bugs were placed with their abdomen facing upwards and inserted into the chest with the pin to secure them, and the chest and abdomen were separated by pulling them outward with forceps. The abdomen was gently unrolled to find a yellow-orange color scent gland, and the flask was then placed in a 2ml reagent bottle with a dissecting needle picked up scent gland and capped to prevent scent gland odor from escaping.
Grinding the dissected scent gland, adding double dealdehydes alcohol, and adding 0.01ml double dealdehydes alcohol into each armyworm scent gland to obtain armyworm scent gland tincture.
Mixing muscone with double dealdehyded alcohol, shaking, standing for aging for one week, and adding purified water to obtain Moschus tincture. The volume ratio of musk ketone to double dealdehyded alcohol to purified water is 1:500:500.
Mixing the civet with the double dealdehyded alcohol, shaking, standing and aging for one week to obtain the civet tincture. The volume ratio of the civet to the double dealdehyded alcohol is 1:1000.
Mixing the tinctures of armyworm scent gland, musk and civet, shaking, and standing for 1 hr to obtain perfume containing secretion of armyworm scent gland. The volume ratio of the stinkbug scent gland tincture to the civet tincture is 100:5:5.
Actual usage effect of the tested group is described as follows:
the effect test was carried out on the perfume containing the secretion of armywood scent gland provided in examples 1 to 6, as follows:
the subjects 10 persons, average age 26.8 years. Each individual sprayed samples of examples 1-6 at different locations on the back and arms, recorded the sensation of use, and scored against the standard for different test indicators.
The scores of 3 indexes (preference degree of fragrance, fragrance retention and warmth) are tested, the score of each index is 0-3, and then the average scores of the three indexes are calculated respectively. The higher the score, the higher the like degree, the lasting fragrance is remained, and the fragrance is mild. Wherein: preference (0: dislike; 1: general; 2: preferred; 3: very preferred; 1: not remaining fragrance; 1: general remaining fragrance; 2: longer lasting fragrance; 3: very long lasting fragrance remaining; 0: pungent; 1: not pungent; 2: milder; 3: very mild;) mildness (2: very mild; 3: very mild) and interview recorded the feeling of the subject.
Actual use effect statistics of the tested population:
the use feeling is as follows:
User a: firstly, the fragrance is very unique, and can simulate natural smell well, so that people can look like to be in the nature. Meanwhile, the durability of the product is quite good, and the product can continuously emit fresh fragrance, so that people feel comfortable and relaxed.
User b: the perfume is fresh, clean and not harsh, and the addition of musk makes the fragrance more mellow and silky.
Of 10 subjects, eight mentioned "unique fragrance", "unique raw material", nine mentioned "mild fragrance and no pungent" and two mentioned "fragrance not durable".
Conclusion:
The perfume of the lugworm scent gland secretion prepared by the invention has good fragrance retaining effect by adopting lugworm scent gland secretion and double dealdehydized alcohol as base raw materials and matching with musk ketone or civet, has clean, fresh, elegant and pleasant fragrance, and can calm and keep happy after long-term use.
Claims (3)
1. A perfume containing the secretion of armyworm scent gland, characterized in that: it comprises 100 parts of tincture and 7 parts of fragrance fixing agent; the tincture is armyworm scent gland tincture, and the perfume fixing agent is musk tincture or civet tincture.
2. The method for preparing the perfume containing armyworm scent gland secretion as claimed in claim 1, which is characterized by comprising the following steps:
s1, dissecting and extracting armyworm scent gland: selecting male armyworm, dissecting and extracting scent gland;
S2, preparing a armyworm scent gland tincture: grinding the dissected scent gland, adding didehydroaldehyde alcohol to obtain a tinctura of armywood scent gland; adding 0.01-0.06 ml of didehydroaldehyde alcohol into each armyworm scent gland;
S3, preparing musk tincture:
mixing muscone and double dealdehyded alcohol, shaking, standing for aging for one week, and adding purified water to obtain Moschus tincture; the musk ketone is as follows: double dealdehyding alcohol: the volume ratio of the purified water is 1:500:500;
S4, preparing a civet tincture:
Mixing the civet with the double dealdehyded alcohol, shaking and standing for aging for one week, wherein the civet is prepared by the following steps of: the volume ratio of the double dealdehyding alcohols is 1:1000;
s5, armyworm perfume ratio
Mixing armyworm scent gland tincture, musk tincture or civet tincture, shaking, and aging for 1 hr to obtain perfume containing armyworm scent gland secretion; the volume ratio of the armyworm scent gland tincture to the musk tincture is 100:7, preparing a base material; the volume ratio of the stinkbug scent gland tincture to the civet tincture is 10:1.
3. The use of the armyworm-scent gland-containing secretion perfume of claim 1 for preparing a perfume containing a fresh and unique odor; wherein the perfume containing fresh and unique odor means: the wet air after rain kneads the fresh taste of the plant juice.
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