CN118108493A - Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions - Google Patents
Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions Download PDFInfo
- Publication number
- CN118108493A CN118108493A CN202410294902.4A CN202410294902A CN118108493A CN 118108493 A CN118108493 A CN 118108493A CN 202410294902 A CN202410294902 A CN 202410294902A CN 118108493 A CN118108493 A CN 118108493A
- Authority
- CN
- China
- Prior art keywords
- stage
- heating
- heating stage
- minutes
- ceramic glaze
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000919 ceramic Substances 0.000 title claims abstract description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 238000000605 extraction Methods 0.000 title claims description 15
- 239000002689 soil Substances 0.000 claims abstract description 45
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 37
- 239000000440 bentonite Substances 0.000 claims abstract description 29
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 29
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 27
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 23
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 20
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 20
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000001354 calcination Methods 0.000 claims abstract description 14
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 230000002708 enhancing effect Effects 0.000 claims abstract 2
- 238000010438 heat treatment Methods 0.000 claims description 76
- 238000010304 firing Methods 0.000 claims description 35
- 230000001590 oxidative effect Effects 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 12
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 230000000630 rising effect Effects 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 2
- 239000000796 flavoring agent Substances 0.000 claims 1
- 235000019634 flavors Nutrition 0.000 claims 1
- 235000014101 wine Nutrition 0.000 abstract description 29
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 abstract description 22
- HBGGXOJOCNVPFY-UHFFFAOYSA-N diisononyl phthalate Chemical compound CC(C)CCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCC(C)C HBGGXOJOCNVPFY-UHFFFAOYSA-N 0.000 abstract description 11
- 235000020097 white wine Nutrition 0.000 abstract description 11
- 230000009471 action Effects 0.000 abstract description 10
- 230000008569 process Effects 0.000 abstract description 10
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 8
- 229910044991 metal oxide Inorganic materials 0.000 abstract description 8
- 150000004706 metal oxides Chemical class 0.000 abstract description 8
- 125000003118 aryl group Chemical group 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 abstract description 5
- 239000012535 impurity Substances 0.000 abstract description 5
- 229910052751 metal Inorganic materials 0.000 abstract description 5
- 239000002184 metal Substances 0.000 abstract description 5
- 239000000126 substance Substances 0.000 description 11
- 229910052500 inorganic mineral Inorganic materials 0.000 description 10
- 239000011707 mineral Substances 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000013078 crystal Substances 0.000 description 6
- 239000002932 luster Substances 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 239000004927 clay Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 150000001340 alkali metals Chemical class 0.000 description 3
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 3
- 150000001342 alkaline earth metals Chemical class 0.000 description 3
- 229910001579 aluminosilicate mineral Inorganic materials 0.000 description 3
- 238000005341 cation exchange Methods 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 3
- 229910052622 kaolinite Inorganic materials 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 3
- 230000036314 physical performance Effects 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- 230000008961 swelling Effects 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 235000012222 talc Nutrition 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
- C04B2235/6583—Oxygen containing atmosphere, e.g. with changing oxygen pressures
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention provides a preparation method of ceramic glaze for extracting alcohol and enhancing fragrance, which belongs to the technical field of ceramics and comprises the steps of mixing 60-80 parts of agate powder, 5-15 parts of star kaolin, 5-15 parts of potassium feldspar, 3-8 parts of talcum powder and 3-8 parts of bentonite to obtain earth culture, and calcining earth blanks; in the process of storing white wine in fired ceramic, metal oxide in agate powder and potassium feldspar or metal and alcohol in wine are oxidized to produce aromatic ester, and acetaldehyde in wine accelerates its volatilization speed under the action of soil culture formed by combining bentonite and star kaolin, and wine becomes thick and aromatic under the action of the ceramic glaze. Can gradually oxidize the impurity alcohol in the wine to generate aromatic ester and volatilize the acetaldehyde in the wine.
Description
Technical Field
The invention relates to the technical field of ceramic preparation, in particular to a preparation method of ceramic glaze with alcohol extraction and aroma enhancement.
Background
Ceramic is an old and commonly used material, and is formed by molding, drying and firing minerals such as clay at high temperature. Ceramic materials have played an important role in human history, not only being used for making artworks and practical appliances, but also having a plurality of other functions and effects. Ceramics are widely used for containing chemical raw materials and other liquids, such as white spirit, due to their excellent physical and chemical properties.
Thus, there is an urgent need for a method for preparing ceramic glazes that are flavored with alcohols.
Disclosure of Invention
In view of this, the present invention gradually oxidizes the fusel in the wine by the ceramic glaze fired by the green body to produce aromatic ester and volatilize the acetaldehyde in the wine.
The technical scheme of the invention is realized as follows: a process for preparing the ceramic glaze with alcohol extraction and fragrance enhancement includes such steps as mixing agate powder (60-80 portions), star kaolin (5-15 portions), potassium feldspar (5-15 portions), talc powder (3-8 portions) and bentonite (3-8 portions), calcining.
Based on the technical scheme, preferably, the agate is peeled and then crushed into 150-200 meshes.
On the basis of the above technical solution, preferably, the calcination includes a temperature raising stage, a temperature lowering stage, a reducing atmosphere firing stage, a converting oxidizing atmosphere firing stage, and a flameout maintaining stage.
On the basis of the above technical solution, preferably, the temperature raising stage includes a first temperature raising stage, a second temperature raising stage, a third temperature raising stage, a fourth temperature raising stage, and a fifth temperature raising stage that are sequentially performed.
On the basis of the technical scheme, preferably, the first temperature rising stage is that the soil culture is gradually heated to 300 ℃ from room temperature in 90 minutes; the second heating stage, namely gradually heating the soil culture after the first heating stage to 600 ℃ from 300 ℃ within 90 minutes; a third heating stage, wherein the soil culture in the second heating stage is gradually heated to 800 ℃ from 600 ℃ in 60 minutes; a fourth heating stage, wherein the soil culture in the third heating stage is gradually heated to 850 ℃ from 800 ℃ within 30 minutes; and a fifth heating stage, wherein the soil culture at the completion of the fourth heating stage is gradually heated from 850 ℃ to 1180 ℃ in 120 minutes.
On the basis of the above technical solution, preferably, the temperature reduction stage is that the soil culture in the fifth temperature increase stage is rapidly reduced from 1180 ℃ to 1170 ℃ and maintained for 10 minutes.
On the basis of the technical scheme, preferably, the soil culture in the reducing atmosphere firing stage is gradually heated from 1170 ℃ to 1310 ℃ within 240 minutes after the cooling stage is completed.
On the basis of the above technical scheme, preferably, in the trans-oxidative atmosphere firing stage, the earth culture in the completion of the reducing atmosphere firing stage is trans-oxidative atmosphere fired at 1310 ℃ and maintained for 30 minutes.
Based on the technical scheme, the flameout maintaining stage is preferable, flameout is realized after the completion of the trans-oxidation atmosphere firing stage, sealing is maintained, and the temperature naturally drops to the room temperature.
Compared with the prior art, the preparation method of the ceramic glaze with alcohol extraction and aroma enhancement has the following beneficial effects:
In the process of storing white wine in fired ceramic, metal oxide in agate powder and potassium feldspar or metal and alcohol in wine are oxidized to produce aromatic ester, and acetaldehyde in wine accelerates its volatilization speed under the action of soil culture formed by combining bentonite and star kaolin, and wine becomes thick and aromatic under the action of the ceramic glaze. Can gradually oxidize the impurity alcohol in the wine to generate aromatic ester and volatilize the acetaldehyde in the wine.
Detailed Description
The following description of the embodiments of the present invention will clearly and fully describe the technical aspects of the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the present invention without making any inventive effort, are intended to fall within the scope of the present invention.
Examples
The preparation process of ceramic glaze with alcohol extraction and fragrance enhancement includes mixing agate powder 60, star kaolin 5, potassium feldspar 5, talcum powder 3 and bentonite 3 to obtain adobe, and calcining. The star kaolin is formed by grinding crystallized kaolinite, wherein the content of ferric oxide is more than 1.3 parts; the agate powder is mainly composed of silicon dioxide, wherein metal oxide is mixed in the agate powder and has a certain color, and the color can be changed from extremely light color to dark color; potassium feldspar is an aluminosilicate mineral of alkali metal or alkaline earth metal such as potassium, sodium, calcium, etc.; the talcum has the advantages of lubricity, anti-sticking, glidant, fire resistance, acid resistance, insulativity, high melting point, inactive chemistry, good covering power, softness, good luster, strong adsorption power, no color change at high temperature, enhanced whiteness, uniform density, good luster and smooth surface after calcination; the bentonite swells when meeting water, the main reason for the natural phenomenon is that the crystal layer spacing of the bentonite mineral is increased, water molecules enter the crystal layer of the mineral, and the reason for the bentonite swelling is also cation exchange of the bentonite mineral, and when agate powder, star kaolin, potassium feldspar, talcum powder and bentonite are mixed and then added with water, the soil culture is prepared. In the process of storing white wine in fired ceramic, metal oxide in agate powder and potassium feldspar or metal and alcohol in wine are oxidized to produce aromatic ester, and acetaldehyde in wine accelerates its volatilization speed under the action of soil culture formed by combining bentonite and star kaolin, and wine becomes thick and aromatic under the action of the ceramic glaze. Can gradually oxidize the impurity alcohol in the wine to generate aromatic ester and volatilize the acetaldehyde in the wine. The inner wall of the wine set prepared by firing the glaze can form a plurality of tiny air holes, the tiny air holes can enable outside oxygen to slowly enter the white wine in the storage process, the esterification reaction of the white wine is promoted, the taste of the white wine becomes mellow, and in addition, the agate glaze contains a large amount of microelements such as iron, copper, calcium, magnesium and the like, and is tightly combined with wine molecules in the process of storing the white wine, so that the pungency of the white wine is reduced, the mellow feeling is increased, and the white wine is softer and more fragrant.
The agate is peeled and crushed to 150 meshes, and when the agate is smaller than 150 meshes, the agate is not easy to melt and fill, and the color development and aroma enhancement and purification effects of the glaze are affected.
The calcination comprises a heating-up stage, a cooling-down stage, a reducing atmosphere firing stage, a converting oxidizing atmosphere firing stage and a flameout maintaining stage.
The heating stage comprises a first heating stage, a second heating stage, a third heating stage, a fourth heating stage and a fifth heating stage which are sequentially carried out. In order to ensure the glaze performance, cracks can not occur, the surface is smoother, the glaze of the blank is fully combined in a gradual heating mode, and the glaze performance is fully exerted.
The first temperature rising stage is that the soil culture is gradually heated to 300 ℃ from room temperature within 90 minutes; the second heating stage, namely gradually heating the soil culture after the first heating stage to 600 ℃ from 300 ℃ within 90 minutes; a third heating stage, wherein the soil culture in the second heating stage is gradually heated to 800 ℃ from 600 ℃ in 60 minutes; a fourth heating stage, wherein the soil culture in the third heating stage is gradually heated to 850 ℃ from 800 ℃ within 30 minutes; and a fifth heating stage, wherein the soil culture at the completion of the fourth heating stage is gradually heated from 850 ℃ to 1180 ℃ in 120 minutes. At high temperature, the solid particles of the adobe are mutually bonded, the grains grow up, pores and grain boundaries gradually decrease, the total volume of the adobe is contracted by the transfer of substances, the density of the adobe is increased, and finally the adobe solid particles become a compact polycrystalline sintered body with a certain microstructure, and the phenomenon is called sintering. The ceramic with physical and chemical changes is prepared from star kaolin, agate powder, potassium feldspar and bentonite through different formulas, and features unique chemical composition, microscopic structure and physical performance.
And in the cooling stage, the temperature of the soil culture in the fifth heating stage is rapidly reduced from 1180 ℃ to 1170 ℃ and maintained for 10 minutes. In order to ensure the firing rate of the ceramic in the cooling process, the color development of the glaze is ensured, and the efficacy of the product is ensured. And in the reducing atmosphere firing stage, the soil culture in the cooling stage is gradually heated from 1170 ℃ to 1310 ℃ within 240 minutes. And the oxidizing atmosphere firing stage is that the earth culture in the reducing atmosphere firing stage is fired at 1310 ℃ in oxidizing atmosphere and kept for 30 minutes.
And in the flameout maintaining stage, flameout is carried out after the completion of the trans-oxidation atmosphere firing stage, sealing is maintained, and the temperature naturally drops to the room temperature.
Examples
The preparation process of ceramic glaze with alcohol extraction and fragrance enhancement includes mixing agate powder 70 weight portions, star kaolin 10 weight portions, potassium feldspar 10 weight portions, talcum powder 5.5 weight portions and bentonite 5.5 weight portions to obtain clay blank, and calcining the clay blank. The agate is peeled and crushed into 175 meshes. The star kaolin is formed by grinding crystallized kaolinite, wherein the content of ferric oxide is more than 1.3 parts; the agate powder is mainly composed of silicon dioxide, wherein metal oxide is mixed in the agate powder and has a certain color, and the color can be changed from extremely light color to dark color; potassium feldspar is an aluminosilicate mineral of alkali metal or alkaline earth metal such as potassium, sodium, calcium, etc.; the talcum has the advantages of lubricity, anti-sticking, glidant, fire resistance, acid resistance, insulativity, high melting point, inactive chemistry, good covering power, softness, good luster, strong adsorption power, no color change at high temperature, enhanced whiteness, uniform density, good luster and smooth surface after calcination; the bentonite swells when meeting water, the main reason for the natural phenomenon is that the crystal layer spacing of the bentonite mineral is increased, water molecules enter the crystal layer of the mineral, and the reason for the bentonite swelling is also cation exchange of the bentonite mineral, and when agate powder, star kaolin, potassium feldspar, talcum powder and bentonite are mixed and then added with water, the soil culture is prepared. In the process of storing white wine in fired ceramic, metal oxide in agate powder and potassium feldspar or metal and alcohol in wine are oxidized to produce aromatic ester, and acetaldehyde in wine accelerates its volatilization speed under the action of soil culture formed by combining bentonite and star kaolin, and wine becomes thick and aromatic under the action of the ceramic glaze. Can gradually oxidize the impurity alcohol in the wine to generate aromatic ester and volatilize the acetaldehyde in the wine.
The calcination comprises a heating-up stage, a cooling-down stage, a reducing atmosphere firing stage, a converting oxidizing atmosphere firing stage and a flameout maintaining stage.
The heating stage comprises a first heating stage, a second heating stage, a third heating stage, a fourth heating stage and a fifth heating stage which are sequentially carried out. In order to ensure the glaze performance, cracks can not occur, the surface is smoother, the glaze of the blank is fully combined in a gradual heating mode, and the glaze performance is fully exerted.
The first temperature rising stage is that the soil culture is gradually heated to 300 ℃ from room temperature within 90 minutes; the second heating stage, namely gradually heating the soil culture after the first heating stage to 600 ℃ from 300 ℃ within 90 minutes; a third heating stage, wherein the soil culture in the second heating stage is gradually heated to 800 ℃ from 600 ℃ in 60 minutes; a fourth heating stage, wherein the soil culture in the third heating stage is gradually heated to 850 ℃ from 800 ℃ within 30 minutes; and a fifth heating stage, wherein the soil culture at the completion of the fourth heating stage is gradually heated from 850 ℃ to 1180 ℃ in 120 minutes. At high temperature, the solid particles of the adobe are mutually bonded, the grains grow up, pores and grain boundaries gradually decrease, the total volume of the adobe is contracted by the transfer of substances, the density of the adobe is increased, and finally the adobe solid particles become a compact polycrystalline sintered body with a certain microstructure, and the phenomenon is called sintering. The ceramic with physical and chemical changes is prepared from star kaolin, agate powder, potassium feldspar and bentonite through different formulas, and features unique chemical composition, microscopic structure and physical performance.
And in the cooling stage, the temperature of the soil culture in the fifth heating stage is rapidly reduced from 1180 ℃ to 1170 ℃ and maintained for 10 minutes. In order to ensure the firing rate of the ceramic in the cooling process, the color development of the glaze is ensured, and the efficacy of the product is ensured. And in the reducing atmosphere firing stage, the soil culture in the cooling stage is gradually heated from 1170 ℃ to 1310 ℃ within 240 minutes. And the oxidizing atmosphere firing stage is that the earth culture in the reducing atmosphere firing stage is fired at 1310 ℃ in oxidizing atmosphere and kept for 30 minutes.
And in the flameout maintaining stage, flameout is carried out after the completion of the trans-oxidation atmosphere firing stage, sealing is maintained, and the temperature naturally drops to the room temperature.
Examples
The preparation process of ceramic glaze with alcohol extraction and fragrance enhancement includes mixing agate powder 80 weight portions, star kaolin 15 weight portions, potassium feldspar 15 weight portions, talcum powder 8 weight portions and bentonite 8 weight portions to obtain clay blank, and calcining. The agate is peeled and crushed into 200 meshes. The star kaolin is formed by grinding crystallized kaolinite, wherein the content of ferric oxide is more than 1.3 parts; the agate powder is mainly composed of silicon dioxide, wherein metal oxide is mixed in the agate powder and has a certain color, and the color can be changed from extremely light color to dark color; potassium feldspar is an aluminosilicate mineral of alkali metal or alkaline earth metal such as potassium, sodium, calcium, etc.; the talcum has the advantages of lubricity, anti-sticking, glidant, fire resistance, acid resistance, insulativity, high melting point, inactive chemistry, good covering power, softness, good luster, strong adsorption power, no color change at high temperature, enhanced whiteness, uniform density, good luster and smooth surface after calcination; the bentonite swells when meeting water, the main reason for the natural phenomenon is that the crystal layer spacing of the bentonite mineral is increased, water molecules enter the crystal layer of the mineral, and the reason for the bentonite swelling is also cation exchange of the bentonite mineral, and when agate powder, star kaolin, potassium feldspar, talcum powder and bentonite are mixed and then added with water, the soil culture is prepared. In the process of storing white wine in fired ceramic, metal oxide in agate powder and potassium feldspar or metal and alcohol in wine are oxidized to produce aromatic ester, and acetaldehyde in wine accelerates its volatilization speed under the action of soil culture formed by combining bentonite and star kaolin, and wine becomes thick and aromatic under the action of the ceramic glaze. Can gradually oxidize the impurity alcohol in the wine to generate aromatic ester and volatilize the acetaldehyde in the wine.
The calcination comprises a heating-up stage, a cooling-down stage, a reducing atmosphere firing stage, a converting oxidizing atmosphere firing stage and a flameout maintaining stage.
The heating stage comprises a first heating stage, a second heating stage, a third heating stage, a fourth heating stage and a fifth heating stage which are sequentially carried out. In order to ensure the glaze performance, cracks can not occur, the surface is smoother, the glaze of the blank is fully combined in a gradual heating mode, and the glaze performance is fully exerted.
The first temperature rising stage is that the soil culture is gradually heated to 300 ℃ from room temperature within 90 minutes; the second heating stage, namely gradually heating the soil culture after the first heating stage to 600 ℃ from 300 ℃ within 90 minutes; a third heating stage, wherein the soil culture in the second heating stage is gradually heated to 800 ℃ from 600 ℃ in 60 minutes; a fourth heating stage, wherein the soil culture in the third heating stage is gradually heated to 850 ℃ from 800 ℃ within 30 minutes; and a fifth heating stage, wherein the soil culture at the completion of the fourth heating stage is gradually heated from 850 ℃ to 1180 ℃ in 120 minutes. At high temperature, the solid particles of the adobe are mutually bonded, the grains grow up, pores and grain boundaries gradually decrease, the total volume of the adobe is contracted by the transfer of substances, the density of the adobe is increased, and finally the adobe solid particles become a compact polycrystalline sintered body with a certain microstructure, and the phenomenon is called sintering. The ceramic with physical and chemical changes is prepared from star kaolin, agate powder, potassium feldspar and bentonite through different formulas, and features unique chemical composition, microscopic structure and physical performance.
And in the cooling stage, the temperature of the soil culture in the fifth heating stage is rapidly reduced from 1180 ℃ to 1170 ℃ and maintained for 10 minutes. In order to ensure the firing rate of the ceramic in the cooling process, the color development of the glaze is ensured, and the efficacy of the product is ensured. And in the reducing atmosphere firing stage, the soil culture in the cooling stage is gradually heated from 1170 ℃ to 1310 ℃ within 240 minutes. And the oxidizing atmosphere firing stage is that the earth culture in the reducing atmosphere firing stage is fired at 1310 ℃ in oxidizing atmosphere and kept for 30 minutes.
And in the flameout maintaining stage, flameout is carried out after the completion of the trans-oxidation atmosphere firing stage, sealing is maintained, and the temperature naturally drops to the room temperature.
The foregoing description of the preferred embodiments of the invention is not intended to be limiting, but rather is intended to cover all modifications, equivalents, alternatives, and improvements that fall within the spirit and scope of the invention.
Claims (9)
1. The preparation method of the ceramic glaze material for extracting alcohol and enhancing flavor is characterized by comprising the following steps of: comprises 60-80 parts of agate powder, 5-15 parts of star kaolin, 5-15 parts of potassium feldspar, 3-8 parts of talcum powder and 3-8 parts of bentonite, and is used for obtaining the soil culture after mixing, and calcining the soil blank.
2. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement as claimed in claim 1, wherein the method comprises the following steps: the agate is peeled and crushed into 150-200 meshes.
3. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement as claimed in claim 2, wherein the method comprises the following steps: the calcination comprises a heating-up stage, a cooling-down stage, a reducing atmosphere firing stage, a converting oxidizing atmosphere firing stage and a flameout maintaining stage.
4. A method for preparing an alcohol-extracted and flavored ceramic glaze according to claim 3, wherein the method comprises the following steps: the heating stage comprises a first heating stage, a second heating stage, a third heating stage, a fourth heating stage and a fifth heating stage which are sequentially carried out.
5. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement according to claim 4, wherein the method comprises the following steps: the first temperature rising stage is that the soil culture is gradually heated to 300 ℃ from room temperature within 90 minutes; the second heating stage, namely gradually heating the soil culture after the first heating stage to 600 ℃ from 300 ℃ within 90 minutes; a third heating stage, wherein the soil culture in the second heating stage is gradually heated to 800 ℃ from 600 ℃ in 60 minutes; a fourth heating stage, wherein the soil culture in the third heating stage is gradually heated to 850 ℃ from 800 ℃ within 30 minutes; and a fifth heating stage, wherein the soil culture at the completion of the fourth heating stage is gradually heated from 850 ℃ to 1180 ℃ in 120 minutes.
6. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement according to claim 5, wherein the method comprises the following steps: and in the cooling stage, the temperature of the soil culture in the fifth heating stage is rapidly reduced from 1180 ℃ to 1170 ℃ and maintained for 10 minutes.
7. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement according to claim 6, wherein the method comprises the following steps: and in the reducing atmosphere firing stage, the soil culture in the cooling stage is gradually heated from 1170 ℃ to 1310 ℃ within 240 minutes.
8. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement according to claim 7, wherein the method comprises the following steps: and the oxidizing atmosphere firing stage is that the earth culture in the reducing atmosphere firing stage is fired at 1310 ℃ in oxidizing atmosphere and kept for 30 minutes.
9. The method for preparing the ceramic glaze with alcohol extraction and aroma enhancement according to claim 8, wherein the method comprises the following steps: and in the flameout maintaining stage, flameout is carried out after the completion of the trans-oxidation atmosphere firing stage, sealing is maintained, and the temperature naturally drops to the room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202410294902.4A CN118108493A (en) | 2024-03-15 | 2024-03-15 | Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202410294902.4A CN118108493A (en) | 2024-03-15 | 2024-03-15 | Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN118108493A true CN118108493A (en) | 2024-05-31 |
Family
ID=91213861
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202410294902.4A Pending CN118108493A (en) | 2024-03-15 | 2024-03-15 | Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN118108493A (en) |
-
2024
- 2024-03-15 CN CN202410294902.4A patent/CN118108493A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102731066B (en) | Porcelain with Junyu glaze and manufacturing method thereof | |
| CN106007669A (en) | Totally closed zero-air-outlet double-layer Jun porcelain heat preserving cup and production method thereof | |
| CN111320458A (en) | Preparation method of tea dust glaze light porcelain | |
| CN109608045B (en) | Wear-resistant high-hardness ceramic glaze and preparation method thereof | |
| CN112125648B (en) | Silver partridge spot build cup manufacturing process | |
| CN114773033B (en) | Daily ceramic product with transparent glaze and preparation method thereof | |
| CN105777092A (en) | Pelelith healthcare clay material and method for preparing clay product from same | |
| CN102408223A (en) | Technology for fabricating big vessel shaped Ru porcelain bottle | |
| CN110228993A (en) | A kind of crackle celadon bottle for cosmetics processing technology with the non-crack glaze of inner face | |
| CN1769245A (en) | Oil drop glaze preparation method | |
| CN107010922B (en) | Preparation method of transmutation glaze purple sand fine pottery | |
| CN105777069A (en) | Medical stone life-nourishing ceramic mud and method for manufacturing ceramic product from medical stone life-nourishing ceramic mud | |
| CN100453009C (en) | Western tableware of iron and ceramic and its making process | |
| CN104876442B (en) | Turquoise glaze for colored pottery products | |
| CN118108493A (en) | Preparation method of ceramic glaze with alcohol extraction and aroma enhancement functions | |
| CN107892554A (en) | A kind of preparation method of spun gold white glaze pottery handicraft | |
| CN109704578B (en) | Antibacterial ceramic glaze with clear glaze surface and preparation method thereof | |
| CN116217080A (en) | Copper-colored metallic luster glaze, preparation method thereof and ceramic product | |
| CN103030366A (en) | Red porcelain and method for producing same | |
| CN111348889B (en) | Ceramic carrier for art porcelain, ceramic with formaldehyde adsorption function and application of ceramic | |
| CN109020480A (en) | A kind of width temperature range sintering Nixing pottery | |
| CN113135733A (en) | Oxidation-fired sanitary ceramic and preparation process thereof | |
| CN112552019A (en) | Formula of slip glaze for high-temperature firing of bone domestic porcelain | |
| CN106957169A (en) | A kind of manufacture craft of iron stoneware | |
| CN1122764A (en) | Composition of activated ceramic container, and mfg. method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication |