CN107892554A - A kind of preparation method of spun gold white glaze pottery handicraft - Google Patents

A kind of preparation method of spun gold white glaze pottery handicraft Download PDF

Info

Publication number
CN107892554A
CN107892554A CN201711130574.0A CN201711130574A CN107892554A CN 107892554 A CN107892554 A CN 107892554A CN 201711130574 A CN201711130574 A CN 201711130574A CN 107892554 A CN107892554 A CN 107892554A
Authority
CN
China
Prior art keywords
parts
hours
slurry
kiln
biscuit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711130574.0A
Other languages
Chinese (zh)
Inventor
张自军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201711130574.0A priority Critical patent/CN107892554A/en
Publication of CN107892554A publication Critical patent/CN107892554A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/24Manufacture of porcelain or white ware
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/89Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2204/00Glasses, glazes or enamels with special properties
    • C03C2204/04Opaque glass, glaze or enamel
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2209/00Compositions specially applicable for the manufacture of vitreous glazes
    • C03C2209/02Compositions specially applicable for the manufacture of vitreous glazes to produce non-uniformly coloured glazes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3472Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5463Particle size distributions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562Heating rate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658Atmosphere during thermal treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/661Multi-step sintering
    • C04B2235/662Annealing after sintering
    • C04B2235/664Reductive annealing

Abstract

The present invention relates to a kind of preparation method of spun gold white glaze pottery handicraft, comprise the following steps:Step 1: obtained slurry is through filter mud and after mixing mud, it is standby;Step 2: after slurry injection base substrate in-mold molding or hand pulled blank forming, dry, repair, the biscuit burnt till takes out standby;Step 3: raw material ground-coat enamel material is taken according to parts by weight, it is standby;Step 4: raw material glaze material is taken according to parts by weight, it is standby;Step 5: carrying out applying ground-coat enamel and cover-coat enamel in biscuit outer surface, after the completion of pouring glaze, base substrate is repaired;Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas.Pottery handicraft produced by the present invention has white background color, and irregular spun gold is distributed on background color, and the length of spun gold and respectively density change according to ceramic type and glazing thickness, has unique artistic effect.

Description

A kind of preparation method of spun gold white glaze pottery handicraft
Technical field
The present invention relates to pottery technical field of artware manufacture, and in particular to a kind of making of spun gold white glaze pottery handicraft Method.
Background technology
Rarity-pottery of state, starts from Tang, is contained in Song, because originating in an ancient unit of weight state of Gu(Modern Yuzhou)And gain the name.Pottery is with typical case Two liquid phase separation glazes based on, have opal effect a kind of porcelain product.Northern Song Dynasty mid-term, pottery product take off among celadon system Grain husk and go out, gradually form oneself unique technique, progressively ripe in kiln around centered on the god Hou of Yuzhou, late period in the Northern Song Dynasty Frightened generation glamour and powerful vitality are burst out as new porcelain kind, achieves significant achievements.Northern Song Dynasty pottery based on small-sized implements, Tire color is greyish white and tire matter is fine and smooth, and glaze colours is simple and elegant uniform, and nature of glass opalescence sense is strong, based on reddish black, sky blue, bluish white, pale blue.Separately Outside, in pottery firing start to apply using cupric oxide as photoghraphic coupler, and it is naturally dizzy dissipate, wonderful interest is infinite, there is that " pottery is hung up red festoons, valency Say in value Liancheng ".During the ancestor of emblem, Eight Diagrams hole is set up hired kiln and burnt paper as sacrificial offerings imperial palace porcelain near Gu Juntai, is referred to as an ancient unit of weight platform kiln afterwards, its Product is mainly to display device, based on floral organ and living utensil, represents the highest level of pottery technique.In the late Qing Dynasty, with collection Heat is risen, and pottery has the saying of " there is ten thousand strings of cash in family, be not as a piece of as pottery ", for referring to the product of an ancient unit of weight platform kiln, and historical facts.
The content of the invention
It is an object of the invention to provide a kind of preparation method of spun gold white glaze pottery handicraft, obtained pottery handicraft tool There is white background color, irregular spun gold is distributed on background color, the length of spun gold and respectively density are according to ceramic type and glazing Thickness and change, there is unique artistic effect.
The technical solution adopted by the present invention is:A kind of preparation method of spun gold white glaze pottery handicraft, comprises the following steps:
Step 1: take Tang's ditch soil 35~40%, Datong District's soil 30~35%, camwood knag soil 6~10%, white arid soil according to percentage by weight 12~16% and albite 8~12%, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 40%, Start wet-milling 12 hours, the slurry by wet-milling crosses 200 mesh sieves, takes out and stands 24 hours, and obtained slurry through filter mud and is mixed It is standby after mud;
Step 2: after slurry prepared by step 1 injects base substrate in-mold molding or hand pulled blank forming, molding blank is taken Go out, dry, repair, firing 3.5-4 hours in 800-900 DEG C of kiln are put into after wiping base with water, truce is cooled to room temperature, burnt till Biscuit takes out standby;
Step 3: take nepheline 15-20 parts according to parts by weight, burn talcum 20-30 parts, feldspar 10-15 parts, kaolin 6-8 parts, just Beautiful 2-6 parts, 3 parts of manganese carbonate, actinolite 5-8 parts, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material gross weight 32% water, start wet-milling 15 hours, the slurry by wet-milling crosses 300 mesh sieves, takes out and stands 12 hours, by the water content of slurry 45% is adjusted to, obtains ground-coat enamel material, it is standby;
Step 4: according to parts by weight take plant ash 25-35 parts, kaolin 8-10 parts, Zijin soil 6-10 parts, talcum 10-15 parts, Actinolite 15-20 parts, corundum 4-6 parts, apatite 6-8 parts, manganese carbonate 1-5 parts, calcite 5-10 parts and di-iron trioxide 1-5 Part, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 30%, start wet-milling 16 hours, through overly moist The slurry of mill crosses 350 mesh sieves, takes out and stands 12 hours, the water content of slurry is adjusted into 46%, obtains glaze material, standby;
Step 5: wiping base is carried out to biscuit made of step 2 with water, with waddy according to the clockwise or inverse time while wiping base The direction of pin is stirred to ground-coat enamel material made of step 3, during stirring since the center of slurry, and is gradually moved to circumference, Mixing time is 20 minutes, after the completion of stirring, the biscuit after wiping base is put into ground-coat enamel slurry, poured in biscuit outer surface Glaze, after the completion of pouring glaze, after body drying, by way of glaze spraying, glaze material made from step 4 is uniformly imposed on base substrate, Biscuit is obtained after drying;
Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas, open gas tank valve, starting point timing of fighting is opened Begin, it is using the time point as starting point that the following time, which calculates, and pressure is adjusted to 0.01MPa, and rear flashboard pulls open 120cm, and wicket is beaten Open 280cm;2.2 hours are fired, kiln temperature rises to 140 DEG C, and pressure is adjusted to 0.02 MPa;3 hours are fired, kiln temperature rises to 320 ℃;6 hours are fired, kiln temperature rises to 560 DEG C;Fire 5.5 hours, kiln temperature rises to 780 DEG C;Programming rate control is at 3 DEG C/minute afterwards Clock, when kiln temperature is controlled at 900-920 DEG C, with tight flashboard;Fire 6.5 hours afterwards, when kiln temperature rises to 1000 DEG C, pressure is adjusted to 0.03 MPa, start to be incubated;8 hours kiln temperatures are fired afterwards and rise to 1100 DEG C, and into reduction phase, pressure is adjusted to 1.5 MPa;Work as burning 8 hours kiln temperatures of system rise to 1250 DEG C, into strong reduction phase;10 hours kiln temperatures are fired afterwards rises to 1350 DEG C;Kiln temperature control afterwards exists Between 1250 DEG C -1350 DEG C, weak reduction is carried out, is fired 12 hours, it is rear to stop firing, fire and complete.
Beneficial effect
Pottery handicraft produced by the present invention has white background color, and irregular spun gold, the length of spun gold are distributed on background color Density changes according to ceramic type and glazing thickness respectively, has unique artistic effect, in the tea set and art of top grade Have wide practical use in porcelain.
Embodiment
Further technical scheme is illustrated below in conjunction with embodiment.
Embodiment 1
A kind of preparation method of spun gold white glaze pottery handicraft, comprises the following steps:
Step 1: Tang's ditch soil 35%, Datong District's soil 35%, camwood knag soil 10%, white arid soil 12% and sodium is taken to grow according to percentage by weight Stone 8%, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 40%, start wet-milling 12 hours, pass through The slurry of wet-milling crosses 200 mesh sieves, takes out and stands 24 hours, standby by obtained slurry through filter mud and after mixing mud;
Step 2: after slurry prepared by step 1 injects base substrate in-mold molding or hand pulled blank forming, molding blank is taken Go out, dry, repair, be put into 800 DEG C of kiln and fire 4 hours after wiping base with water, truce is cooled to room temperature, and the biscuit burnt till takes out It is standby;
Step 3: take 16 parts of nepheline according to parts by weight, burn 25 parts of talcum, 12 parts of feldspar, 6 parts of kaolin, 4 parts of corundum, carbonic acid 3 parts of manganese, 6 parts of actinolite, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material gross weight 32% water, start shooting wet-milling 15 hours, the slurry by wet-milling crossed 300 mesh sieves, takes out and stands 12 hours, the water content of slurry is adjusted into 45%, obtained on earth Glaze, it is standby;
Step 4: according to parts by weight take 30 parts of plant ash, 8 parts of kaolin, Zijin soil 8 parts, 12 parts of talcum, 16 parts of actinolite, 2 parts of 5 parts of corundum, 8 parts of apatite, 2 parts of manganese carbonate, 8 parts of calcite and di-iron trioxide, above-mentioned raw materials are crushed respectively rearmounted Enter ball mill, add the water of raw material gross weight 30%, start wet-milling 16 hours, the slurry by wet-milling crosses 350 mesh sieves, takes out quiet Put 12 hours, the water content of slurry is adjusted to 46%, obtains glaze material, it is standby;
Step 5: wiping base is carried out to biscuit made of step 2 with water, with waddy according to the clockwise or inverse time while wiping base The direction of pin is stirred to ground-coat enamel material made of step 3, during stirring since the center of slurry, and is gradually moved to circumference, Mixing time is 20 minutes, after the completion of stirring, the biscuit after wiping base is put into ground-coat enamel slurry, poured in biscuit outer surface Glaze, after the completion of pouring glaze, after body drying, by way of glaze spraying, glaze material made from step 4 is uniformly imposed on base substrate, Biscuit is obtained after drying;
Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas, open gas tank valve, starting point timing of fighting is opened Begin, it is using the time point as starting point that the following time, which calculates, and pressure is adjusted to 0.01MPa, and rear flashboard pulls open 120cm, and wicket is beaten Open 280cm;2.2 hours are fired, kiln temperature rises to 140 DEG C, and pressure is adjusted to 0.02 MPa;3 hours are fired, kiln temperature rises to 320 ℃;6 hours are fired, kiln temperature rises to 560 DEG C;Fire 5.5 hours, kiln temperature rises to 780 DEG C;Programming rate control is at 3 DEG C/minute afterwards Clock, when kiln temperature is controlled at 900-920 DEG C, with tight flashboard;Fire 6.5 hours afterwards, when kiln temperature rises to 1000 DEG C, pressure is adjusted to 0.03 MPa, start to be incubated;8 hours kiln temperatures are fired afterwards and rise to 1100 DEG C, and into reduction phase, pressure is adjusted to 1.5 MPa;Work as burning 8 hours kiln temperatures of system rise to 1250 DEG C, into strong reduction phase;10 hours kiln temperatures are fired afterwards rises to 1350 DEG C;Kiln temperature control afterwards exists Between 1250 DEG C -1350 DEG C, weak reduction is carried out, is fired 12 hours, it is rear to stop firing, fire and complete.
Embodiment 2:
A kind of preparation method of spun gold white glaze pottery handicraft, comprises the following steps:
Step 1: take Tang's ditch soil 40%, Datong District's soil 30%, camwood knag soil 6%, white arid soil 12% and albite according to percentage by weight 12%, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 40%, start wet-milling 12 hours, pass through The slurry of wet-milling crosses 200 mesh sieves, takes out and stands 24 hours, standby by obtained slurry through filter mud and after mixing mud;
Step 2: after slurry prepared by step 1 injects base substrate in-mold molding or hand pulled blank forming, molding blank is taken Go out, dry, repair, be put into 900 DEG C of kiln and fire 4 hours after wiping base with water, truce is cooled to room temperature, and the biscuit burnt till takes out It is standby;
Step 3: take 16 parts of nepheline according to parts by weight, burn 25 parts of talcum, 12 parts of feldspar, 6 parts of kaolin, 4 parts of corundum, carbonic acid 3 parts of manganese, 6 parts of actinolite, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material gross weight 32% water, start shooting wet-milling 15 hours, the slurry by wet-milling crossed 300 mesh sieves, takes out and stands 12 hours, the water content of slurry is adjusted into 45%, obtained on earth Glaze, it is standby;
Step 4: according to parts by weight take 25 parts of plant ash, 8 parts of kaolin, Zijin soil 6 parts, 10 parts of talcum, 15 parts of actinolite, 5 parts of 6 parts of corundum, 8 parts of apatite, 5 parts of manganese carbonate, 10 parts of calcite and di-iron trioxide, after above-mentioned raw materials are crushed respectively Ball mill is inserted, adds the water of raw material gross weight 30%, start wet-milling 16 hours, the slurry by wet-milling crosses 350 mesh sieves, takes out 12 hours are stood, the water content of slurry is adjusted to 46%, obtains glaze material, it is standby;
Step 5: wiping base is carried out to biscuit made of step 2 with water, with waddy according to the clockwise or inverse time while wiping base The direction of pin is stirred to ground-coat enamel material made of step 3, during stirring since the center of slurry, and is gradually moved to circumference, Mixing time is 20 minutes, after the completion of stirring, the biscuit after wiping base is put into ground-coat enamel slurry, poured in biscuit outer surface Glaze, after the completion of pouring glaze, after body drying, by way of glaze spraying, glaze material made from step 4 is uniformly imposed on base substrate, Biscuit is obtained after drying;
Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas, open gas tank valve, starting point timing of fighting is opened Begin, it is using the time point as starting point that the following time, which calculates, and pressure is adjusted to 0.01MPa, and rear flashboard pulls open 120cm, and wicket is beaten Open 280cm;2.2 hours are fired, kiln temperature rises to 140 DEG C, and pressure is adjusted to 0.02 MPa;3 hours are fired, kiln temperature rises to 320 ℃;6 hours are fired, kiln temperature rises to 560 DEG C;Fire 5.5 hours, kiln temperature rises to 780 DEG C;Programming rate control is at 3 DEG C/minute afterwards Clock, when kiln temperature is controlled at 900-920 DEG C, with tight flashboard;Fire 6.5 hours afterwards, when kiln temperature rises to 1000 DEG C, pressure is adjusted to 0.03 MPa, start to be incubated;8 hours kiln temperatures are fired afterwards and rise to 1100 DEG C, and into reduction phase, pressure is adjusted to 1.5 MPa;Work as burning 8 hours kiln temperatures of system rise to 1250 DEG C, into strong reduction phase;10 hours kiln temperatures are fired afterwards rises to 1350 DEG C;Kiln temperature control afterwards exists Between 1250 DEG C -1350 DEG C, weak reduction is carried out, is fired 12 hours, it is rear to stop firing, fire and complete.
Embodiment 3:
A kind of preparation method of spun gold white glaze pottery handicraft, comprises the following steps:
Step 1: take Tang's ditch soil 36%, Datong District's soil 32%, camwood knag soil 8%, white arid soil 12% and albite according to percentage by weight 12%, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 40%, start wet-milling 12 hours, pass through The slurry of wet-milling crosses 200 mesh sieves, takes out and stands 24 hours, standby by obtained slurry through filter mud and after mixing mud;
Step 2: after slurry prepared by step 1 injects base substrate in-mold molding or hand pulled blank forming, molding blank is taken Go out, dry, repair, be put into 850 DEG C of kiln and fire 3.5 hours after wiping base with water, truce is cooled to room temperature, and the biscuit burnt till takes Go out standby;
Step 3: take 120 parts of nepheline according to parts by weight, burn 30 parts of talcum, 15 parts of feldspar, 6 parts of kaolin, 2 parts of corundum, carbonic acid 3 parts of manganese, 5 parts of actinolite, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material gross weight 32% water, start shooting wet-milling 15 hours, the slurry by wet-milling crossed 300 mesh sieves, takes out and stands 12 hours, the water content of slurry is adjusted into 45%, obtained on earth Glaze, it is standby;
Step 4: take plant ash 35, kaolin 10, Zijin soil 10, talcum 15, actinolite 15, corundum 4, phosphorus according to parts by weight Lime stone 6, manganese carbonate 1, calcite 5 and di-iron trioxide 1, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material The water of gross weight 30%, start wet-milling 16 hours, the slurry by wet-milling crosses 350 mesh sieves, takes out and stands 12 hours, by slurry Water content is adjusted to 46%, obtains glaze material, standby;
Step 5: wiping base is carried out to biscuit made of step 2 with water, with waddy according to the clockwise or inverse time while wiping base The direction of pin is stirred to ground-coat enamel material made of step 3, during stirring since the center of slurry, and is gradually moved to circumference, Mixing time is 20 minutes, after the completion of stirring, the biscuit after wiping base is put into ground-coat enamel slurry, poured in biscuit outer surface Glaze, after the completion of pouring glaze, after body drying, by way of glaze spraying, glaze material made from step 4 is uniformly imposed on base substrate, Biscuit is obtained after drying;
Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas, open gas tank valve, starting point timing of fighting is opened Begin, it is using the time point as starting point that the following time, which calculates, and pressure is adjusted to 0.01MPa, and rear flashboard pulls open 120cm, and wicket is beaten Open 280cm;2.2 hours are fired, kiln temperature rises to 140 DEG C, and pressure is adjusted to 0.02 MPa;3 hours are fired, kiln temperature rises to 320 ℃;6 hours are fired, kiln temperature rises to 560 DEG C;Fire 5.5 hours, kiln temperature rises to 780 DEG C;Programming rate control is at 3 DEG C/minute afterwards Clock, when kiln temperature is controlled at 900-920 DEG C, with tight flashboard;Fire 6.5 hours afterwards, when kiln temperature rises to 1000 DEG C, pressure is adjusted to 0.03 MPa, start to be incubated;8 hours kiln temperatures are fired afterwards and rise to 1100 DEG C, and into reduction phase, pressure is adjusted to 1.5 MPa;Work as burning 8 hours kiln temperatures of system rise to 1250 DEG C, into strong reduction phase;10 hours kiln temperatures are fired afterwards rises to 1350 DEG C;Kiln temperature control afterwards exists Between 1250 DEG C -1350 DEG C, weak reduction is carried out, is fired 12 hours, it is rear to stop firing, fire and complete.
The above described is only a preferred embodiment of the present invention, any formal limitation not is made to the present invention, though So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people Member, without departing from the scope of the present invention, when the technology contents using the disclosure above make out a little change or repair The equivalent embodiment for equivalent variations is adornd, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content Any simple modification, equivalent change and modification made to above example, in the range of still falling within technical solution of the present invention.

Claims (1)

  1. A kind of 1. preparation method of spun gold white glaze pottery handicraft, it is characterised in that:Comprise the following steps:
    Step 1: take Tang's ditch soil 35~40%, Datong District's soil 30~35%, camwood knag soil 6~10%, white arid soil according to percentage by weight 12~16% and albite 8~12%, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 40%, Start wet-milling 12 hours, the slurry by wet-milling crosses 200 mesh sieves, takes out and stands 24 hours, and obtained slurry through filter mud and is mixed It is standby after mud;
    Step 2: after slurry prepared by step 1 injects base substrate in-mold molding or hand pulled blank forming, molding blank is taken Go out, dry, repair, firing 3.5-4 hours in 800-900 DEG C of kiln are put into after wiping base with water, truce is cooled to room temperature, burnt till Biscuit takes out standby;
    Step 3: take nepheline 15-20 parts according to parts by weight, burn talcum 20-30 parts, feldspar 10-15 parts, kaolin 6-8 parts, just Beautiful 2-6 parts, 3 parts of manganese carbonate, actinolite 5-8 parts, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add raw material gross weight 32% water, start wet-milling 15 hours, the slurry by wet-milling crosses 300 mesh sieves, takes out and stands 12 hours, by the water content of slurry 45% is adjusted to, obtains ground-coat enamel material, it is standby;
    Step 4: according to parts by weight take plant ash 25-35 parts, kaolin 8-10 parts, Zijin soil 6-10 parts, talcum 10-15 parts, Actinolite 15-20 parts, corundum 4-6 parts, apatite 6-8 parts, manganese carbonate 1-5 parts, calcite 5-10 parts and di-iron trioxide 1-5 Part, above-mentioned raw materials are crushed respectively it is rearmounted enter ball mill, add the water of raw material gross weight 30%, start wet-milling 16 hours, through overly moist The slurry of mill crosses 350 mesh sieves, takes out and stands 12 hours, the water content of slurry is adjusted into 46%, obtains glaze material, standby;
    Step 5: wiping base is carried out to biscuit made of step 2 with water, with waddy according to the clockwise or inverse time while wiping base The direction of pin is stirred to ground-coat enamel material made of step 3, during stirring since the center of slurry, and is gradually moved to circumference, Mixing time is 20 minutes, after the completion of stirring, the biscuit after wiping base is put into ground-coat enamel slurry, poured in biscuit outer surface Glaze, after the completion of pouring glaze, after body drying, by way of glaze spraying, glaze material made from step 4 is uniformly imposed on base substrate, Biscuit is obtained after drying;
    Step 6: the biscuit of step 5 is put into kiln, burnt using High Temperature Gas, open gas tank valve, starting point timing of fighting is opened Begin, it is using the time point as starting point that the following time, which calculates, and pressure is adjusted to 0.01MPa, and rear flashboard pulls open 120cm, and wicket is beaten Open 280cm;2.2 hours are fired, kiln temperature rises to 140 DEG C, and pressure is adjusted to 0.02 MPa;3 hours are fired, kiln temperature rises to 320 ℃;6 hours are fired, kiln temperature rises to 560 DEG C;Fire 5.5 hours, kiln temperature rises to 780 DEG C;Programming rate control is at 3 DEG C/minute afterwards Clock, when kiln temperature is controlled at 900-920 DEG C, with tight flashboard;Fire 6.5 hours afterwards, when kiln temperature rises to 1000 DEG C, pressure is adjusted to 0.03 MPa, start to be incubated;8 hours kiln temperatures are fired afterwards and rise to 1100 DEG C, and into reduction phase, pressure is adjusted to 1.5 MPa;Work as burning 8 hours kiln temperatures of system rise to 1250 DEG C, into strong reduction phase;10 hours kiln temperatures are fired afterwards rises to 1350 DEG C;Kiln temperature control afterwards exists Between 1250 DEG C -1350 DEG C, weak reduction is carried out, is fired 12 hours, it is rear to stop firing, fire and complete.
CN201711130574.0A 2017-11-15 2017-11-15 A kind of preparation method of spun gold white glaze pottery handicraft Pending CN107892554A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711130574.0A CN107892554A (en) 2017-11-15 2017-11-15 A kind of preparation method of spun gold white glaze pottery handicraft

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711130574.0A CN107892554A (en) 2017-11-15 2017-11-15 A kind of preparation method of spun gold white glaze pottery handicraft

Publications (1)

Publication Number Publication Date
CN107892554A true CN107892554A (en) 2018-04-10

Family

ID=61805387

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711130574.0A Pending CN107892554A (en) 2017-11-15 2017-11-15 A kind of preparation method of spun gold white glaze pottery handicraft

Country Status (1)

Country Link
CN (1) CN107892554A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108675758A (en) * 2018-06-16 2018-10-19 燕俊峰 A kind of production method that Bodhidharma feeds sparrow pottery craftwork
CN108689686A (en) * 2018-06-16 2018-10-23 燕俊峰 A kind of production method that Bodhidharma feeds sparrow pottery craftwork
CN110642614A (en) * 2019-09-25 2020-01-03 张军召 Jun porcelain formed by demolding and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106565092A (en) * 2016-08-31 2017-04-19 福建省德化县臻晖陶瓷有限公司 Lightweight low-temperature fancy golden silk white glazed porcelain and manufacturing process

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106565092A (en) * 2016-08-31 2017-04-19 福建省德化县臻晖陶瓷有限公司 Lightweight low-temperature fancy golden silk white glazed porcelain and manufacturing process

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
刘银: "《无机非金属材料工艺学》", 30 September 2015, 中国科学技术大学出版社 *
徐利华: "《陶瓷坯釉料制备技术》", 31 October 2012, 中国轻工业出版社 *
池至铣: "《釉 釉料及陶瓷颜色配制手册》", 30 November 2015, 中国建材工业出版社 *
皮特森: "《陶瓷工艺与艺术》", 31 July 2009, 武汉理工大学出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108675758A (en) * 2018-06-16 2018-10-19 燕俊峰 A kind of production method that Bodhidharma feeds sparrow pottery craftwork
CN108689686A (en) * 2018-06-16 2018-10-23 燕俊峰 A kind of production method that Bodhidharma feeds sparrow pottery craftwork
CN110642614A (en) * 2019-09-25 2020-01-03 张军召 Jun porcelain formed by demolding and preparation method thereof

Similar Documents

Publication Publication Date Title
CN104030733B (en) Official's Song bluish white brother's kiln porcelain and preparation method thereof
CN106336116B (en) A kind of ceramic glaze and preparation method thereof, the method for utilizing its production ceramics
CN107892554A (en) A kind of preparation method of spun gold white glaze pottery handicraft
CN105777068B (en) Your a kind of pea green porcelain and preparation method thereof
CN105036810A (en) Black-base mottled composite Tang jun glaze and process for preparing jun porcelain through black-base mottled composite Tang jun glaze
CN102898121A (en) Ru-kiln celadon ware and preparation process thereof
CN105036809A (en) Blue background and mottled spot composite Tang jun glaze and technology for preparing jun porcelain through same
CN101624297A (en) Preparation method for tea dust temmoku glaze
CN106186700B (en) Environmentally friendly shell pearl glaze, environmental protection shell pearl glaze ceramic and preparation method thereof made from it
CN110228993B (en) Processing technology of crackle celadon cosmetic bottle with inner non-crackle glaze
CN105237041A (en) Celadon azure secret-color glaze material
CN105776866B (en) Longquan celadon jasper green glaze, the green Longquan celadon of jasper and preparation method thereof
CN111087253B (en) Decoration process on low-water-absorption ceramic surface
CN105175020A (en) Complex Tang-dynasty jun glaze with blue spots in black and process for preparing jun porcelain by use of complex Tang-dynasty jun glaze
CN104446658A (en) Antiqued sky-blue-glaze jade-texture ru porcelain and preparation method thereof
CN112194457A (en) Making process of red rabbit hair cup
CN107098677A (en) Black matrix erythema droplet temmoku glaze ceramics and its preparation technology
CN105294069B (en) A kind of preparation method of dark reddish brown soil pottery
CN103922805B (en) Silver rib puts down making method and the flat de-secret colour ware device of obtained silver-colored rib of de-secret colour ware device
CN104591695A (en) Manufacturing method of large-sized regenerated ceramic
CN107382281A (en) A kind of burning process of emerald green stove an ancient unit of weight
CN107043214A (en) Brownish black floor iron red colored crystalline point ceramic glaze and the method using its preparation ceramics
CN107793123A (en) A kind of manufacture craft of ice-crack-like glaze pottery handicraft
CN109485383A (en) A kind of diamond shape vase pottery art and craft making method
CN103570338B (en) Low-temperature energy-saving manufacture method for once-sintered printed glazed red soil pottery products

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180410

RJ01 Rejection of invention patent application after publication