CN118078676A

CN118078676A - Hair care peptide essence emulsion and preparation method thereof

Info

Publication number: CN118078676A
Application number: CN202410415700.0A
Authority: CN
Inventors: 陈洁云
Original assignee: Pinko Biotechnology Guangzhou Co ltd
Current assignee: Pinko Biotechnology Guangzhou Co ltd
Priority date: 2024-04-08
Filing date: 2024-04-08
Publication date: 2024-05-28

Abstract

The application relates to the technical field of application of bioactive peptides, and particularly discloses hair care peptide essence emulsion and a preparation method thereof. A hair care peptide essence emulsion is prepared from the following raw materials in parts by weight: 45-65 parts of deionized water; 1-5 parts of an emulsifying agent; 0.1-0.3 part of preservative; oligopeptide-30.5-2.5 parts; 10-12 parts of hair care extract mixture; 0.5-3 parts of glycerol stearate; cetostearyl alcohol polyether-251-5 parts; 0.5-2.5 parts of stearyl trimethyl ammonium chloride; 0.8-1 part of ethanol; 0.05-0.2 part of essence; 0.1-1 part of biotin; 0.1-2 parts of chlorophyll; 0.2-0.6 part of wheat hydrolyzed protein; 4-8 parts of donkey bone collagen peptide; 0.5-2 parts of prinsepia utilis royle oil; 1-3 parts of fermented dendrobium candidum; and (3) fermenting dendrobium candidum to obtain: s1, mixing dendrobium candidum raw materials with distilled water to prepare fermentation stock solution; s2, inoculating mixed bacteria for fermentation after the fermentation raw liquid is treated, adding ganoderan in the fermentation process, and centrifuging to obtain supernatant. The hair care peptide essence emulsion disclosed by the application not only can be suitable for sensitive muscle groups with damaged skin barriers, but also can bring excellent hair care effects.

Description

Hair care peptide essence emulsion and preparation method thereof

Technical Field

The application relates to the technical field of application of bioactive peptides, in particular to hair care peptide essence emulsion and a preparation method thereof.

Background

The hair care peptide is an active peptide which can quickly repair hair in a short time, is derived from keratin, is safe and free of side effects, can not only strengthen the toughness and elasticity of the hair and make the hair smooth and glossy, but also can recover damaged hair from root sources by stabilizing keratin chains to reorganize the hair structure and reapply the vitality of the hair.

At present, the hair care peptide is usually matched with other functional components to prepare a high-efficiency hair care product, such as essence emulsion, which has the excellent characteristic of easy application and no washing, and can be completely absorbed by only taking a proper amount of essence emulsion to be uniformly applied to hair and lightly massaging for 1-3 minutes, so that the hair care peptide is more and more favored by consumers. However, the sensitive muscle group with damaged skin barrier is often limited in the selection of the product, and the sensitive muscle group has poor resistance to external stimulus and weak repair capability, so that the skin is usually in a high reaction state, and once the skin barrier is damaged, the sebum membrane or the stratum corneum of the skin is often damaged, and the substances which can be absorbed by normal groups are treated in a very different way.

In view of the above-mentioned related art, the inventors believe that the essence cream containing hair care peptides on the market at present is not suitable for people with sensitive muscles whose skin barrier is damaged in order to pursue more powerful hair care effects, and is often too weak to cause excessive reactions such as scalp itching and redness of scalp, and causes phenomena of hair dryness and breakage after a large amount of long-term use. Therefore, there is a need to propose a solution to the above technical problems.

Disclosure of Invention

The application provides a hair care peptide essence emulsion and a preparation method thereof, and the hair care peptide essence emulsion is used for obtaining a hair care peptide product which has excellent hair care effect and is suitable for sensitive muscle groups with damaged skin barriers.

In a first aspect, the application provides a hair care peptide essence emulsion, which adopts the following technical scheme:

a hair care peptide essence emulsion is prepared from the following raw materials in parts by weight:

45-65 parts of deionized water;

1-5 parts of an emulsifying agent;

0.1-0.3 part of preservative;

oligopeptide-30.5-2.5 parts;

10-12 parts of hair care extract mixture;

0.5-3 parts of glycerol stearate;

cetostearyl alcohol polyether-251-5 parts;

0.5-2.5 parts of stearyl trimethyl ammonium chloride;

0.8-1 part of ethanol;

0.05-0.2 part of essence;

0.1-1 part of biotin;

0.1-2 parts of chlorophyll;

0.2-0.6 part of wheat hydrolyzed protein;

4-8 parts of donkey bone collagen peptide;

0.5-2 parts of prinsepia utilis royle oil;

1-3 parts of fermented dendrobium candidum;

the fermented dendrobium candidum is prepared by the following steps:

S1, crushing dendrobium candidum raw materials, mixing the crushed dendrobium candidum raw materials with distilled water in a ratio of 1 (25-35), extracting at 85-90 ℃ for 2-3 hours, centrifuging, and taking supernatant to obtain fermentation stock solution;

S2, sterilizing the fermentation stock solution at high temperature, cooling, placing the fermentation stock solution in a fermentation container, inoculating 4-7% of mixed bacteria obtained by mixing saccharomycetes and lactobacillus, fermenting for 2-3d at the temperature of 30-35 ℃ and the fermentation rotating speed of 150-170r/min, adding 5-10/L ganoderma lucidum polysaccharide into the fermentation mixture in the fermentation process, centrifuging after the fermentation is finished, and taking the supernatant fluid to obtain the fermented dendrobium candidum.

By adopting the technical scheme, a large number of polar and charged groups are exposed in the oligopeptide-3 molecules, and can be combined with water molecules to form hydrogen bonds, so that the water sample environment of the skin is kept, and the oligopeptide-3 can permeate into the dermis through the stratum corneum of the skin to play a role, so that the effects of resisting aging, promoting collagen metabolism of the skin, whitening, repairing and the like are brought; the hair care extract mixture is prepared from a plurality of natural plant extracts, so that the activity of tyrosinase can be enhanced, the absorption of nutrient substances can be promoted, and further, the effects of promoting the formation of melanin, promoting the growth of hair and blackening and moistening the hair are achieved; biotin can improve hair quality, can reduce hair loss, broken hair and frizziness of hair, and make hair shinier; in the hair care peptide essence emulsion, the matching use of the oligopeptide-3, the hair care extract mixture and the biotin can bring stronger hair care effect.

Meanwhile, in order to enable the hair care peptide essence emulsion to be more suitable for sensitive muscle groups with damaged skin barriers and bring positive hair care effects, the hair care peptide essence emulsion is mainly realized through the cooperation among donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum. The donkey bone collagen peptide has the effects of removing impurities, strengthening proteins and the like, and can promote proliferation and migration of keratinocytes so as to accelerate the repair of an epidermal barrier; the prinsepia utilis royle oil can increase the tight junction protein from the protein level, and can improve the synthesis of lipid by accelerating the expression of intercellular lipid synthase in the skin permeation barrier, thereby bringing the repairing effect of the skin barrier; the fermented dendrobium candidum is obtained by double-bacteria fermentation and stimulation regulation and control by adopting ganoderan in the fermentation process, contains rich sugar, protein, amino acid, fatty acid, polyphenol and other components, and can play an excellent role in balance regulation on a micro-ecological system with complex head skin; the donkey bone collagen peptide, the prinsepia utilis royle oil and the fermented dendrobium candidum are matched, an excellent compound synergistic effect can be achieved among the donkey bone collagen peptide, the prinsepia utilis royle oil and the fermented dendrobium candidum, especially for sensitive muscle groups with damaged skin barriers, a cooperation mechanism for internal repair and external recovery can be formed, the skin barrier function is sound, the skin can be assisted to absorb and convert high-efficiency hair care components, the skin tolerance can be improved in the process, the stimulation effect is reduced, and further the excellent hair care effect can be achieved after the hair care peptide essence emulsion is applied.

Preferably, the fermented dendrobium candidum is prepared by the following steps:

S1, crushing dendrobium candidum raw materials, mixing the crushed dendrobium candidum raw materials with distilled water at a ratio of 1:30, extracting for 2 hours at 90 ℃, centrifuging, and taking supernatant to obtain fermentation stock solution;

S2, sterilizing the fermentation stock solution at high temperature, cooling, placing the fermentation stock solution in a fermentation container, inoculating 5% of mixed bacteria obtained by mixing saccharomycetes and lactobacillus, fermenting for 2d at the temperature of 30 ℃ and the fermentation speed of 150r/min, adding 10/L ganoderan into the fermentation mixture in the fermentation process, centrifuging after the fermentation is finished, and taking the supernatant fluid to obtain the fermented dendrobium candidum.

By adopting the technical scheme, the parameters are adopted for control in the preparation of the fermented dendrobium candidum, and in the process, reducing sugar can be fully decomposed and utilized by microorganisms, macromolecular polysaccharide is decomposed into small molecules, and part of the small molecular polysaccharide is decomposed into diversified monosaccharides; simultaneously, the contents of protein, amino acid, short-chain fatty acid and polyphenol are relatively high; the fermented dendrobium candidum obtained at the moment contains a rich component system, can exert a better self-efficacy effect in the application process, can also have a better coordination effect with donkey collagen peptide and prinsepia utilis royle oil, further has stronger applicability of the finally obtained hair care peptide essence emulsion to sensitive muscle groups with damaged skin barriers, and has better hair care effect.

Preferably, the ratio of the combined fermentation of the yeast and the lactic acid bacteria is 3:7.

By adopting the technical scheme, the proportion of fermentation can be selected to exert better cooperation, the stability of a fermentation system can be increased, the smooth proceeding of the fermentation process is ensured, meanwhile, the mixed bacteria and the added ganoderan have better cooperation effect in the fermentation process, further, the obtained fermented dendrobium candidum has better application quality, and the whole application effect of the hair care peptide essence emulsion is relatively excellent.

Preferably, the weight ratio of the donkey bone collagen peptide to the prinsepia utilis royle oil to the fermented dendrobium candidum is 6:1:1.5.

Through adopting above-mentioned technical scheme, when donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum of above-mentioned weight ratio are joined in marriage, the corresponding effect of performance is comparatively excellent, makes hair care peptide essence emulsion not only more be applicable to skin barrier impaired sensitive muscle crowd, can also demonstrate comparatively excellent hair care effect.

Preferably, 3-5 parts by weight of auxiliary functional auxiliary agents are added into the raw materials of the hair care peptide essence milk, the auxiliary functional auxiliary agents consist of citrus water-soluble pectin, fish gravy and tea bran micropowder, and the weight ratio of the citrus water-soluble pectin, the fish gravy and the tea bran micropowder is (3-5): 1 (0.4-0.7).

By adopting the technical scheme, the citrus water-soluble pectin is a water-soluble colloid gradient extract obtained by mixing citrus peel with water and heating and filtering, and has good emulsion stability and good stability for maintaining the stability of skin mucous membrane; the fish sauce contains rich nutritional ingredients such as protein, amino acid, vitamins, minerals and the like, and can be used as a nutritional supplement; the tea bran micropowder is rich in various antioxidant substances such as tea polyphenol, catechin and the like, and can effectively remove free radicals and prevent oxidation reaction, so that the effects of antioxidation and anti-aging are achieved; when the citrus water-soluble pectin, fish gravy and tea bran micropowder are used as functional auxiliary agents according to a specific weight ratio range, the functional auxiliary agents can maintain the balance of positive and negative charges of skin when functional components are absorbed by sensitive skin with damaged skin barriers, so that better functional component absorption and conversion effects are realized, and abundant substance supply is provided in the process of recovering a microecological system and repairing the skin barriers, cell homeostasis is maintained, and the generation of larger stimulation is avoided, so that donkey collagen peptide, prinsepia utilis royle oil and fermented dendrobium officinale exert more effective effects in the process, and the overall quality of the hair care peptide essence milk is remarkably improved.

Preferably, the weight ratio of the citrus hydrosol to the fish gravy to the tea bran micropowder is 4.5:1:0.5.

By adopting the technical scheme, the auxiliary functional auxiliary agent composed of the citrus hydrosol, the fish gravy and the tea bran micropowder in the weight ratio has better action and effect in application, and the finally obtained hair care peptide essence emulsion has better applicability and hair care effect on sensitive muscle groups with damaged skin barriers.

Preferably, the emulsifier is one or a combination of more of cetostearyl alcohol, polysorbate-20, alkyl polyglucoside, lecithin and stearyl alcohol polyether-6.

Through adopting above-mentioned technical scheme, the preparation of the hair care peptide essence emulsion is all suitable for to above-mentioned kind of emulsifier, can make each component raw materials fully combine and form stable combined state, and the hair care peptide essence emulsion that the application obtained not only texture becomes lighter and finer, also more easily opens and smear even when using.

Preferably, the preservative is one or a combination of more than one of hydroxyacetophenone, phenoxyethanol, octanol, chlorpheniramine and hydroquinone.

By adopting the technical scheme, the preservatives of the types can prevent bacteria from breeding, and the hair care peptide essence emulsion can maintain excellent product stability in the storage process.

Preferably, the hair care extract mixture is a composition of angelica sinensis extract, ganoderma lucidum extract, polygonum multiflorum extract, ginseng extract, black mulberry extract, vine of multiflower knotweed extract, larch extract, tea extract, pseudo-ginseng extract, gallnut extract, ginger root extract, biota orientalis extract, black sesame extract and redseed extract of the annatto.

By adopting the technical scheme, the angelica sinensis extract can increase oxygen and nutrition supply of skin, relieve skin fatigue and improve self-repairing capability of skin; the ganoderma atrum extract contains abundant vitamins and minerals, and can nourish hair and make hair healthier; the Polygoni Multiflori radix extract has effects of promoting melanin synthesis and activating tyrosinase, and can nourish hair and increase melanin; the ginseng extract is rich in various active ingredients, and can provide nutrition components and antioxidation protection required by skin; the black mulberry extract has remarkable effects of promoting hair growth and improving hair quality; the caulis polygoni multiflori extract has a certain skin conditioning effect and can help balance grease secretion; the European larch extract has the effects of moisturizing, relieving and resisting allergy; the tea extract has strong oxygen-proof capability and can promote the generation of collagen; the pseudo-ginseng extract has strong capability of scavenging free radicals, can regulate the immunity of skin, and has good antioxidation effect; the Chinese gall extract has good whitening, astringing, anti-inflammatory, antioxidant and antibacterial effects; the ginger root extract can promote hair growth and has anti-inflammatory effect; the cacumen Platycladi extract can provide sufficient nutrition and control sebum secretion; the black sesame extract can enhance the brightness and softness of hair and provide necessary nutrition for hair roots; the extract of the seed of the carmine in south america can strengthen hair, and resist ultraviolet rays and heat loss; the hair care extract mixture formed by the components is applied to hair care peptide essence emulsion, so that excellent hair care effect can be brought.

In a second aspect, the application provides a preparation method of hair care peptide essence emulsion, which adopts the following technical scheme:

a preparation method of hair care peptide essence emulsion comprises the following steps:

(1) Preparing raw materials comprising deionized water, an emulsifying agent, a preservative, oligopeptide-3, a hair care extraction mixture, glycerol stearate, cetostearyl alcohol polyether-25, stearyl trimethyl ammonium chloride, ethanol, essence, biotin, donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium officinale according to a ratio;

(2) Uniformly stirring and mixing water, an emulsifying agent, oligopeptide-3, a hair care extraction mixture, glycerol stearate and prinsepia utilis royle oil in the step (1) at 65-75 ℃, then homogenizing for 3-5min under vacuum at 5000-7000rpm, cooling to 45-55 ℃, adding cetostearyl alcohol polyether-25, stearyl trimethyl ammonium chloride, donkey bone collagen peptide and fermented dendrobium candidum, uniformly stirring and mixing, cooling to 30-40 ℃, adding ethanol, essence and biotin, uniformly stirring and mixing, and naturally cooling to obtain the hair care peptide essence emulsion.

By adopting the technical scheme, the preparation method is simple to operate, and the hair care peptide essence emulsion with excellent and stable quality can be obtained on the basis of fully mixing and combining the raw materials, so that the large-scale industrial production is facilitated; meanwhile, different addition sequences and temperature changes are adopted on the use of the raw materials, so that the quality control in the production process is facilitated, and the obtained hair care peptide essence emulsion is guaranteed to have higher quality.

In summary, the application has the following beneficial effects:

1. according to the application, donkey collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum are matched, and excellent compound synergism is adopted among the donkey collagen peptide, prinsepia royle oil and fermented dendrobium candidum, so that a cooperation mechanism for internal repair and external recovery can be formed for sensitive muscle groups with damaged skin barriers, the skin barrier function is sound, the skin can be assisted to absorb and convert high-efficiency hair care components, the skin tolerance can be improved and the stimulation effect can be reduced in the process, and the hair care peptide essence emulsion can play an excellent hair care effect;

2. According to the application, the citrus water-soluble pectin, the fish gravy and the tea bran micropowder are formed into the functional auxiliary agent according to a specific weight ratio range, so that the functional auxiliary agent can maintain the positive and negative charge balance of skin when functional components are absorbed by sensitive skin with damaged skin barriers, is beneficial to realizing better functional component absorption and conversion effects, provides rich substance supply, maintains cell homeostasis in the process of recovering a microecological system and repairing the skin barriers, is beneficial to avoiding the generation of larger stimulus, and has stronger applicability to sensitive muscle groups with damaged skin barriers and better hair care effect.

Detailed Description

The present application will be described in further detail with reference to examples.

The raw materials used in each of the preparation examples, examples and comparative examples of the present application are commercially available unless otherwise specified.

Donkey bone collagen peptide is purchased from Gansu Probiotics Biotechnology Co., ltd, has a specification of 80 meshes and a molecular weight of 500 daltons;

Citrus water soluble pectin is purchased from 96% low molecular weight citrus pectin from vanity organisms;

the tea bran micropowder is prepared from Volterras organism by extracting the spray powder from 20:1 raw materials.

Examples of preparation of starting materials and/or intermediates

Preparation example 1

A fermented dendrobium candidum is prepared by the following steps:

S1, crushing dendrobium candidum raw materials to 800 meshes, mixing the crushed dendrobium candidum raw materials with distilled water at a ratio of 1:30, extracting at 90 ℃ for 2 hours, centrifuging, and taking supernatant to obtain fermentation stock solution;

Note that: in the above operation, the ratio of the combined fermentation of the yeast and the lactic acid bacteria was 3:7.

Preparation example 2

The fermented dendrobium candidum is prepared by the following steps as follows, and is different from the preparation example 1:

S1, crushing dendrobium candidum raw materials to 800 meshes, mixing the crushed dendrobium candidum raw materials with distilled water at a ratio of 1:25, extracting at 85 ℃ for 3 hours, centrifuging, and taking supernatant to obtain fermentation stock solution;

S2, sterilizing the fermentation stock solution at high temperature, cooling, placing the fermentation stock solution in a fermentation container, inoculating 4% of mixed bacteria obtained by mixing saccharomycetes and lactobacillus, fermenting for 3d at 35 ℃ and a fermentation speed of 170r/min, adding 5/L ganoderan into a fermentation mixture in the fermentation process, centrifuging after fermentation is finished, and taking supernatant fluid to obtain the fermented dendrobium candidum.

Preparation example 3

S1, crushing dendrobium candidum raw materials to 800 meshes, mixing the crushed dendrobium candidum raw materials with distilled water at a ratio of 1:35, extracting at 90 ℃ for 2.5 hours, centrifuging, and taking supernatant to obtain fermentation stock solution;

s2, sterilizing the fermentation stock solution at high temperature, cooling, placing the fermentation stock solution in a fermentation container, inoculating 7% of mixed bacteria obtained by mixing saccharomycetes and lactobacillus, fermenting at 30 ℃ at a fermentation speed of 160r/min for 2.5, adding 7.5/L ganoderan into the fermentation mixture in the fermentation process, centrifuging after the fermentation is finished, and taking the supernatant to obtain the fermented dendrobium candidum.

Preparation example 4

A fermented Dendrobium officinale is different from preparation example 1 in that the ratio of the combined fermentation of the saccharomycetes and the lactic acid bacteria is 3.5:7.

Preparation example 5

A fermented Dendrobium officinale is different from preparation example 1 in that the ratio of the combined fermentation of the saccharomycetes and the lactic acid bacteria is 3:7.5.

Preparation example 6

A fermented Dendrobium officinale is different from the preparation example 1 in that only yeast is used in the fermentation process.

Preparation example 7

A fermented Dendrobium officinale is different from preparation example 1 in that only lactic acid bacteria are used in the fermentation process.

Preparation example 8

A fermented Dendrobium officinale is different from preparation 1 in that ganoderan is not added to the fermentation mixture during fermentation.

Examples

Example 1

The hair care peptide essence emulsion is prepared from the following raw materials in parts by weight as shown in table 1:

(2) Uniformly stirring and mixing water, an emulsifying agent, oligopeptide-3, a hair care extraction mixture, glycerol stearate and prinsepia utilis royle oil in the step (1) at 65-75 ℃ (70 ℃ in the embodiment), homogenizing for 3-5min (5 min in the embodiment) at 5000-7000rpm (6000 rpm in the embodiment), cooling to 45-55 ℃ (50 ℃ in the embodiment), adding cetostearyl alcohol polyether-25, stearyl trimethyl ammonium chloride, donkey bone collagen peptide and fermented dendrobium candidum, uniformly stirring and mixing, cooling to 30-40 ℃ (35 ℃ in the embodiment), adding ethanol, essence and biotin, uniformly stirring and mixing, and naturally cooling to obtain the hair care peptide essence emulsion.

Note that: in the above operation, fermented dendrobium candidum was obtained in preparation example 1; biotin is D-biotin; the essence is cinnamaldehyde; the emulsifier is cetostearyl alcohol; the preservative is phenoxyethanol; the hair care extract mixture is a composition of angelica sinensis extract, ganoderma atrum extract, polygonum multiflorum extract, ginseng extract, black mulberry extract, vine of multiflower knotweed extract, larch extract, tea extract, pseudo-ginseng extract, gallnut extract, ginger root extract, biota orientalis extract, black sesame extract and carmine seed extract, and the ratio is 13:7.5:6:5:4.5:3:2:1.5:1:0.8:0.7:0.5:0.3:0.1.

Examples 2 to 3

A hair care peptide essence emulsion is different from example 1 in that the raw materials and the corresponding parts by weight thereof are shown in Table 1.

TABLE 1 raw materials and parts by weight (kg/part) of each of examples 1 to 3

Example 4

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 2.

Example 5

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 3.

Example 6

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 4.

Example 7

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 5.

Example 8

A hair care peptide essence emulsion is different from example 1 in that the total dosage of donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum is unchanged, and the weight ratio of the donkey bone collagen peptide to the prinsepia utilis royle oil to the fermented dendrobium candidum is adjusted to be 6:1:1.5.

Example 9

A hair care peptide essence emulsion is different from the embodiment 1 in that 4 parts by weight of auxiliary functional auxiliary agents are added into the raw materials, the auxiliary functional auxiliary agents consist of citrus water-soluble pectin, fish gravy and tea bran micropowder in a weight ratio of 4.5:1:0.5, and the auxiliary functional auxiliary agents and the fermented dendrobium candidum are added together for use in the preparation process of the hair care peptide essence emulsion.

Example 10

A hair care peptide essence emulsion is different from example 9 in that the auxiliary functional auxiliary agent is added in 3 parts by weight.

Example 11

A hair care peptide essence emulsion is different from example 9 in that 5 parts by weight of auxiliary functional auxiliary agent is added.

Example 12

A hair care peptide essence emulsion is different from example 9 in that the auxiliary functional auxiliary agent consists of citrus water-soluble pectin, fish gravy and tea bran micropowder according to the weight ratio of 3:1:0.4.

Example 13

A hair care peptide essence emulsion is different from example 9 in that the auxiliary functional auxiliary agent consists of citrus water-soluble pectin, fish gravy and tea bran micropowder according to the weight ratio of 5:1:0.7.

Example 14

A hair care peptide essence emulsion is different from example 9 in that the auxiliary functional auxiliary agent consists of citrus water-soluble pectin, fish gravy and tea bran micropowder in a weight ratio of 4:1:0.55.

Example 15

A hair care peptide essence emulsion differs from example 9 in that the raw material does not contain citrus water-soluble pectin.

Example 16

A hair care peptide essence emulsion is different from example 9 in that the raw material does not contain fish gravy.

Example 17

A hair care peptide essence emulsion is different from example 9 in that the raw materials do not contain tea bran micropowder.

Example 18

A hair care peptide essence emulsion is different from example 9 in that the raw materials do not contain citrus water-soluble pectin and fish gravy.

Example 19

A hair care peptide essence emulsion is different from example 9 in that the raw materials do not contain tea bran micropowder and fish gravy.

Example 20

A hair care peptide essence emulsion is different from example 9 in that the raw materials do not contain citrus water-soluble pectin and tea bran micropowder.

Comparative example

Comparative example 1

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 6.

Comparative example 2

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 7.

Comparative example 3

A hair care peptide essence emulsion is different from example 1 in that fermented Dendrobium officinale is obtained in preparation example 8.

Comparative example 4

A hair care peptide essence emulsion is different from example 1 in that the raw material does not contain donkey bone collagen peptide.

Comparative example 5

A hair care peptide essence emulsion is different from example 1 in that prinsepia utilis royle oil is not contained in the raw materials.

Comparative example 6

A hair care peptide essence emulsion is different from example 1 in that the raw materials do not contain fermented dendrobium candidum.

Comparative example 7

A hair care peptide essence emulsion is different from example 1 in that the raw materials do not contain donkey bone collagen peptide and prinsepia utilis royle oil.

Comparative example 8

A hair care peptide essence emulsion is different from example 1 in that the raw materials do not contain donkey bone collagen peptide and fermented dendrobium candidum.

Comparative example 9

A hair care peptide essence emulsion is different from the hair care peptide essence emulsion in that the raw materials do not contain prinsepia utilis royle oil and fermented dendrobium candidum.

Comparative example 10

A hair care peptide essence emulsion is different from example 1 in that the raw materials do not contain donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum.

Performance test

Test sample: the hair care peptide essence milk obtained in examples 1 to 20 was used as test samples 1 to 20, and the hair care peptide essence milk obtained in comparative examples 1 to 10 was used as control samples 1 to 10.

The test method comprises the following steps: 60 sensitive skin groups with damaged skin barriers are selected in the experiment, and subjects aged 18-30 years old are divided into 30 groups, and each of men and women in each group uses test samples 1-20 and control samples 1-10 respectively.

Before use, the head test position area is simply cleaned by clear water, 0.5ml of hair care peptide essence emulsion is used for smearing once, the size of the smearing area is 4cm x 4cm, the head test position area is matched with hand circling type massage for 3 minutes, the head test position area is smeared at the same position area for 5 days, and the following tests are carried out:

(1) The rate of decrease of the percutaneous moisture Loss, which is a physical parameter indicating the normal and continuous diffusion of moisture through the skin horny layer, represents the condition of moisture Loss of the skin horny layer, is a common indicator of the skin barrier function, and when the skin barrier function is impaired, the moisture content of the skin horny layer is decreased and the percutaneous moisture Loss (TRANSEPIDERMAL WATER Loss, TEWL) is increased; the skin test device TEWAMETER TM Hex was used to test the amount of percutaneous water loss before and after the subject used the hair care peptide essence cream, and the rate of decrease in percutaneous water loss = (pre-test value-post-test value)/pre-test value, wherein the higher the rate of decrease in percutaneous water loss, the better the application effect of the hair care peptide essence cream was.

(2) The irritation rating is carried out on the test skin of the subject, whether erythema appears or not is checked, the feeling of the test skin is recorded according to the use process of the subject, the test skin is mainly carried out around stinging, burning and tightening, the test skin is classified into 0-10 grades according to the severity degree, the test skin is negative in 0 grade, and no erythema, stinging, burning and tightening feel are generated; grade 10 is a severe positive reaction, with obvious erythema, stinging, burning and tightness evident, and the reaction exceeded the skin test area; and the test results of each group are averaged over the two person ratings of each group.

(3) Scalp ecological balance evaluation, namely, the micro ecological environment of scalp is critical as the soil for hair growth, the benign ecological system is maintained by three major balances of grease, flora and metabolism, and once the ecological environment is unbalanced, the problems of head oil, head itch and dandruff occur, wherein the head oil is mainly caused by abnormal grease secretion, the head itch is caused by mass propagation of harmful bacteria, and the dandruff is caused by unbalanced metabolism; and (3) carrying out 0-10-point evaluation according to the severity of the head oil, the head itch and the dandruff, wherein 10 is the optimal, 0 is the worst, and the test result of each group is the average value of the evaluation scores of each two people.

(4) A gloss improvement test in which a part of light enters the inside of hair fibers when light is irradiated to the hair; a part of light is reflected or refracted on the surface of the hair crust formed by compact keratin, and healthy hair can always give out stronger luster, so that the effects of hair care, repair, nourishing and the like of the hair care peptide essence emulsion can be evaluated through measuring the glossiness of the hair. The HAIR glossiness is measured by using a HAIR glossiness tester SAMBA HAIR before and after the HAIR care peptide essence emulsion is used by a subject, and the glossiness improvement rate= (post-test value-pre-test value)/pre-test value is obtained, wherein the higher the glossiness improvement rate is, the better the application effect of the HAIR care peptide essence emulsion is.

TABLE 2 application test results for test samples 1-20 and control samples 1-10

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As can be seen by combining example 1 and comparative examples 4-10 and combining table 2, the donkey collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum are matched, so that the hair care peptide essence emulsion is excellent in the reduction rate of percutaneous water loss, the irritation rating, the evaluation of scalp ecological balance and the improvement rate of glossiness after being applied to sensitive muscle groups with damaged skin barriers; if only any one or two of donkey bone collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum are used, the effects are limited, and the effects are simply overlapped, so that the obvious synergistic effect can be brought only when the three are compounded; when the donkey bone collagen peptide, the prinsepia utilis royle oil and the fermented dendrobium candidum are not used, the reduction rate of the percutaneous water loss is found to be negative, which indicates that the skin barrier is greatly damaged, and the stimulation effect is possibly brought to other functional components in the absorption process, and the release effect of any one or two of the donkey bone collagen peptide, the prinsepia royle oil and the fermented dendrobium candidum on the stimulation is extremely limited, so that the prescription can bring a larger action effect in the aspect only when the three components are compounded.

As can be seen by combining example 1 and comparative examples 1-3 and combining table 2, the fermented dendrobium candidum is obtained by double-bacteria fermentation and stimulation regulation and control by using ganoderan in the fermentation process, so that the obtained fermented dendrobium candidum can exert a better matching effect with donkey collagen peptide and prinsepia utilis royle oil after application, and the obtained fermented dendrobium candidum by single-bacteria fermentation or lack of ganoderan for stimulation regulation and control finds that the hair care peptide essence emulsion has obvious loss in the reduction rate of percutaneous water loss, the evaluation of scalp ecological balance and the improvement rate of glossiness; in combination with examples 6-7 and Table 2, it can be seen that the hair care peptide essence emulsion has excellent effect on the application of sensitive muscle groups with damaged skin barrier when the ratio of the combined fermentation of yeast and lactobacillus is 3:7.

As can be seen from the combination of examples 1-3 and 8 and the combination of table 2, when the weight ratio of donkey collagen peptide, prinsepia utilis royle oil and fermented dendrobium candidum is 6:1:1.5, the hair care peptide essence emulsion is more suitable for people with sensitive muscle with damaged skin barrier, and can also show excellent hair care effect.

As can be seen from the combination of examples 1 and 9-14 and the combination of table 2, the application of the functional auxiliary agent comprising the citrus hydrosol, fish gravy and tea bran micropowder in the specific weight ratio ranges to the hair care peptide essence cream can bring forward improvement in the aspects of reduction rate of percutaneous water loss, evaluation of scalp ecological balance and improvement rate of glossiness, wherein the improvement effect brought by the functional auxiliary agent is excellent when the weight ratio of the citrus hydrosol, fish gravy and tea bran micropowder is 4.5:1:0.5. It can be seen from the combination of examples 15 to 20 and table 2 that if only any one or two of the citrus water-soluble pectin, fish gravy and tea bran micropowder is added, the corresponding effects can be simply improved, but the improvement space is limited, and only the simple superposition of the effects is achieved, and only when the three components are used together, the obvious matching effect can be achieved, so that the applicability of the hair care peptide essence emulsion to sensitive muscle groups with damaged skin barriers is high, and the hair care effect is also excellent.

The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.

Claims

1. The hair care peptide essence emulsion is characterized by being prepared from the following raw materials in parts by weight:

45-65 parts of deionized water;

1-5 parts of an emulsifying agent;

0.1-0.3 part of preservative;

oligopeptide-30.5-2.5 parts;

10-12 parts of hair care extract mixture;

0.5-3 parts of glycerol stearate;

cetostearyl alcohol polyether-251-5 parts;

0.5-2.5 parts of stearyl trimethyl ammonium chloride;

0.8-1 part of ethanol;

0.05-0.2 part of essence;

0.1-1 part of biotin;

0.1-2 parts of chlorophyll;

0.2-0.6 part of wheat hydrolyzed protein;

4-8 parts of donkey bone collagen peptide;

0.5-2 parts of prinsepia utilis royle oil;

1-3 parts of fermented dendrobium candidum;

the fermented dendrobium candidum is prepared by the following steps:

2. The hair care peptide essence emulsion according to claim 1, wherein: the fermented dendrobium candidum is prepared by the following steps:

3. The hair care peptide essence emulsion according to claim 1, wherein: the ratio of the combined fermentation of the saccharomycetes and the lactic acid bacteria is 3:7.

4. The hair care peptide essence emulsion according to claim 1, wherein: the weight ratio of the donkey bone collagen peptide to the prinsepia utilis royle oil to the fermented dendrobium candidum is 6:1:1.5.

5. The hair care peptide essence emulsion according to claim 1, wherein: the hair care peptide essence emulsion is characterized in that 3-5 parts by weight of auxiliary functional auxiliary agents are added into the raw materials of the hair care peptide essence emulsion, the auxiliary functional auxiliary agents comprise citrus water-soluble pectin, fish gravy and tea bran micropowder, and the weight ratio of the citrus water-soluble pectin to the fish gravy to the tea bran micropowder is (3-5): 1 (0.4-0.7).

6. The hair care peptide serum of claim 5, wherein: the weight ratio of the citrus hydrosol to the fish gravy to the tea bran micropowder is 4.5:1:0.5.

7. The hair care peptide essence emulsion according to claim 1, wherein: the emulsifier is one or more of cetostearyl alcohol, polysorbate-20, alkyl polyglucoside, lecithin and stearyl alcohol polyether-6.

8. The hair care peptide essence emulsion according to claim 1, wherein: the preservative is one or a combination of more of p-hydroxyacetophenone, phenoxyethanol, octanol, chlorpheniramine and hydroquinone.

9. The hair care peptide essence emulsion according to claim 1, wherein: the hair care extract mixture is a composition of angelica sinensis extract, ganoderma atrum extract, polygonum multiflorum extract, ginseng extract, black mulberry extract, vine of multiflower knotweed extract, larch extract, tea extract, pseudo-ginseng extract, gallnut extract, ginger root extract, biota orientalis extract, black sesame extract and south American carmine seed extract.

10. The method for preparing the hair care peptide essence emulsion according to claim 1, which is characterized in that: the method comprises the following steps: