CN117844563A - Preparation method and application of refined snake oil extracted by ultrasonic process - Google Patents
Preparation method and application of refined snake oil extracted by ultrasonic process Download PDFInfo
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Abstract
The invention discloses a preparation method for extracting refined snake oil by utilizing an ultrasonic process and application thereof. The invention discloses an agkistrodon acutus snake fat which is prepared into agkistrodon acutus snake oil by adopting an ultrasonic extraction technology, and the specific process comprises the following steps: cleaning Agkistrodon acutus snake fat, pulverizing, adding into ultrasonic extractor, adding water, heating to obtain Agkistrodon acutus snake crude oil, decolorizing and deodorizing to obtain refined snake oil. Crushing dehydrated snake fat into small fat particles for later use; adding pulverized snake fat into an ultrasonic extractor, adding water 1-2 times of snake fat, vacuum-heating, ultrasonic-extracting for 60-120 min to obtain crude snake oil; the crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil. The invention uses ultrasonic wave technology to extract refined snake oil, which can be widely used in food, medicine and cosmetics, and is a human service.
Description
Technical Field
The invention relates to a method for extracting snake oil, belongs to the technical field of animal oil extraction, and in particular relates to a preparation method for extracting refined snake oil by utilizing an ultrasonic process and application thereof.
Background
Agkistrodon acutus oil can be used for treating wind-depressive psychosis, skin sore, scald, burn, skin wrinkle, and chilblain. Has the effects of resisting inflammation, tranquilizing, detumescence, promoting blood circulation, preventing and treating cold injury, reducing blood lipid, and treating dry dermatitis, yellow brown spot, etc.
At present, snake fat is usually decocted in a pot to obtain snake oil, the residue of the snake oil is filtered, and crude oil is applied to products, firstly, the crude oil is easy to oxidize, and has very large fishy smell, so that the products can be used only in a short time, and even if the smell is covered by essence and plant spice, the problem of product storage still cannot be solved. Preventing the application of snake oil products in foods, medicines and cosmetics.
Chinese patent CN201510746864.2 discloses a preparation method of natural snake oil, which comprises the steps of preparing materials, squeezing snake oil at high temperature, filtering, purifying snake oil, extracting rose oil, preparing snake oil, taking fresh rose flowers during preparing materials, removing impurities from the fresh rose flowers, washing and airing; extracting fat tissue of snake, cleaning for several times, and removing impurity such as snake skin and fibre; heating and refining the extracted fat to obtain refined liquid when the snake oil is squeezed at high temperature, and squeezing filter residues for 8-10 min until oil-free exudation is achieved to obtain squeezed liquid; filtering the refined liquid and the squeezed liquid with gauze for 1-2 times until no impurity is visible to the naked eye of the filtrate, and obtaining filtrate and filter residue.
The Chinese patent CN201310449805.X discloses a method for refining snake oil, which takes the fat tissue of the snake as the raw material, heats and refines the refined liquid, filters the refined liquid while the refined liquid is hot to obtain filtrate which is main liquid of the snake oil; squeezing the residue to obtain squeezed liquid, and filtering to obtain filtrate containing snake oil; mixing the main snake oil liquid with the snake oil contained in the filter residue to obtain a crude snake oil product; dissolving crude snake oil in organic solvent for multiple times, extracting under ultrasonic wave, recovering solvent by distillation method, and introducing nitrogen gas to obtain refined snake oil.
To accommodate the wide range of applications and innovative needs, those skilled in the art recognize that there is still a need for further improvements in the two refined snake oil processes described above.
Disclosure of Invention
Aiming at the defects existing in the prior art, the invention aims to provide the preparation method for extracting refined snake oil by utilizing an ultrasonic process, and the prepared agkistrodon acutus oil has good absorption effect on skin, has high absorption speed after being smeared on the surface of the skin, does not generate greasy feeling, and has no irritation to the skin. The snake oil is stable and can be stored for a long time.
The invention also aims to provide the application of the snake oil prepared by the process of the extraction and purification technology of the snake oil, so that the snake oil can be widely applied to foods, medicines and cosmetics and is used for human services.
The aim and the technical problems of the invention are realized by adopting the following technical proposal. The preparation method for extracting refined snake oil by utilizing ultrasonic technology provided by the invention comprises the following steps:
1) Cleaning the agkistrodon acutus fat wrappage, rinsing the cleaned fat with clear water until no blood water is generated after cleaning, and centrifugally dehydrating for later use;
2) Crushing dehydrated snake fat into fat particles for later use; the Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to be less than 10 meshes;
3) Adding pulverized snake fat into an ultrasonic extractor, adding water 1-3 times of snake fat, vacuum-heating, and ultrasonic extracting for 60-120 min;
vacuum-opening, vacuum-opening at a vacuum degree of more than-0.05 Pa, heating to 70-80deg.C, ultrasonic-opening at 500-600W for 60-120 min, and centrifuging to obtain crude snake oil;
4) Deacidifying, decolorizing and deodorizing crude snake oil to obtain refined snake oil;
the oil activated carbon is powdery activated carbon (wood, shell and coconut shell) with iodine value more than or equal to 800mg/g and moisture less than 10%; the iodine value of the granular activated carbon (fruit shell, coconut shell and coal) is more than or equal to 800mg/g, the strength is more than or equal to 95%, and the pH value is 7-9.
In step 1), the agkistrodon acutus fat coating is cleaned, because the snake fat is embedded in a layer of film, the snake fat needs to be peeled off from the film, the cleaned fat is rinsed with clean water until no blood is generated, baking soda, sodium carbonate and the like are added in the rinsing process to neutralize free acid, and then the free acid is neutralized by acid, and centrifugally dehydrated for later use.
Further, in the step 2), the dehydrated snake fat is crushed into fat particles to make the fat particles uniform in size, and the agkistrodon acutus snake fat comprises snake fat similar to agkistrodon acutus which is crushed into fat particles smaller than 10 meshes; and (5) standby.
In step 3), the crushed snake fat is added into an ultrasonic extractor, water is added to be 1-2 times of the snake fat, vacuum is opened, heating is performed, ultrasonic waves are opened, and the oil is extracted until the whole oil is distilled off, preferably 60-120 minutes.
Further, the vacuum degree of the vacuum is more than-0.05 Pa, preferably-0.05 Pa to 0.1Pa, the heating extraction is preferably carried out at 70 to 80 ℃, the ultrasonic extraction is carried out, preferably 500 to 600W, and the extraction time is 60 to 120 minutes. And (5) centrifuging to obtain crude snake oil.
In step 4), the crude snake oil is deacidified, decolored and deodorized to obtain the refined snake oil.
Furthermore, the oil activated carbon is powdery activated carbon (wood, shell and coconut shell) with an iodine value of more than or equal to 800mg/g and water content of less than 10%. The iodine value of the granular activated carbon (fruit shell, coconut shell and coal) is more than or equal to 800mg/g, the strength is more than or equal to 95%, and the pH value is 7-9. Granular activated carbon husks are preferred.
Furthermore, the invention relates to a preparation method for extracting refined snake oil by utilizing an ultrasonic process, and application of the refined agkistrodon acutus snake oil in preparing foods, medicines and cosmetics.
By means of the technical scheme, the invention has the following advantages and beneficial technical effects:
1) The agkistrodon acutus oil prepared by the invention has good absorption effect on skin, has high absorption speed after being smeared on the surface of the skin, does not generate greasy feeling, and has no irritation to the skin;
2) The medicine snake oil is a very useful natural medicine and is widely applied to traditional Chinese medicines; the snake oil contains abundant proteins, fat, minerals, active substances, vitamins and other components, and has many effects, such as improving skin immunity, relieving arthritis and rheumatic pain, promoting wound healing, improving cardiovascular health, enhancing human immunity and the like.
3) The snake oil has antibacterial, antiinflammatory, skin caring, and pain relieving effects, and can be used for treating skin diseases such as scald, cold injury, skin crack, chronic eczema, tinea pedis, and herpes zoster;
4) The agkistrodon acutus oil prepared by the invention is applied to cosmetics, and the snake oil can permeate deep layers of skin, promote proliferation and renewal of skin cells, moisten, smooth and elastic skin, and eliminate wrinkles, spots, acne marks and the like. Such as a snake oil cream, a snake oil cream hand cream, etc.
Drawings
Fig. 1 is a flow chart of a process for preparing snake oil from agkistrodon acutus snake fat by using an ultrasonic extraction technology.
Detailed Description
The invention discloses a process for preparing snake oil from agkistrodon acutus snake fat by utilizing an ultrasonic extraction technology. Agkistrodon acutus (Deinagkistrodontus) is also known as Agkistrodon, agkistrodon acutus, agkistrodon halys, and Agkistrodon halys. The Agkistrodon acutus snake fat is prepared into Agkistrodon acutus snake oil by ultrasonic extraction technology. Cleaning Agkistrodon acutus snake fat, pulverizing, adding into ultrasonic extractor, adding water, heating to obtain Agkistrodon acutus snake crude oil, decolorizing and deodorizing to obtain refined snake oil.
The invention belongs to the technical field of snake oil processing, relates to a preparation process of agkistrodon acutus snake oil, and in particular relates to the fields of medical preparation and cosmetic preparation.
Wherein, the main components of the agkistrodon acutus snake oil are as follows: 44.68% of oleic acid C18 (1), 10.55% of linoleic acid C18 (2), 19.08% of palm oil C16 and 3.77% of stearic acid C18.
As shown in fig. 1, a process for preparing snake oil from agkistrodon acutus snake fat by using ultrasonic extraction technology comprises the following production process flows:
1) Cleaning the agkistrodon acutus fat wrappage, rinsing the cleaned fat with clear water until the cleaned fat is clean and free of blood, and centrifugally dehydrating for later use;
2) Crushing dehydrated snake fat into fat particles for later use; the Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to be less than 10 meshes;
3) Adding pulverized snake fat into an ultrasonic extractor, adding water 1-2 times of snake fat, vacuum-heating, and ultrasonic extracting for 60-120 min; vacuum is opened, the vacuum degree is more than-0.05 Pa, the temperature is heated to 70-80 ℃, ultrasonic waves are opened for 500-600W, and the extraction time is 60-120 minutes; centrifuging to obtain crude snake oil;
4) Deacidifying, decolorizing and deodorizing crude snake oil to obtain refined snake oil; the oil activated carbon is powdered activated carbon (wood, shell and coconut shell) with iodine value not less than 800mg/g and water content less than 10%.
The iodine value of the granular activated carbon (fruit shell, coconut shell and coal) is more than or equal to 800mg/g, the strength is more than or equal to 95%, and the pH value is 7-9.
The technical scheme of the present invention will be described in further detail with reference to the following specific preferred examples in combination with effect test examples, but the present invention is not limited to the following examples.
Embodiment one:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning an agkistrodon acutus fat wrapper, rinsing the cleaned fat with water, adding baking soda for the first time at the water temperature of preferably about 35 ℃, adjusting the pH value of the water to 8 for the first time, cleaning the cleaned fat wrapper with clean water until no blood water exists, and centrifugally dehydrating the cleaned fat wrapper for later use;
2) Crushing dehydrated snake fat into fat particles for later use; the Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to less than 10 meshes.
3) Adding pulverized snake fat into an ultrasonic extractor, adding water to 2 times of snake fat, vacuum-heating, ultrasonic-extracting for 100 min; firstly, vacuum is opened, the vacuum degree is more than-0.05 Pa, and the temperature is heated to 80 ℃.
2) Turning on ultrasonic wave 550W for 100 minutes; and (5) centrifuging to obtain crude snake oil.
4) Deacidifying, decolorizing and deodorizing crude snake oil to obtain refined snake oil; the grease activated carbon is powdered activated carbon and coconut activated carbon, the iodine value is more than or equal to 800mg/g, and the moisture is less than 10%.
The powder of 80-400 meshes of activated carbon is added with the amount of 2%, the oil is heated to 50-80 ℃, the temperature is kept for 30 minutes, and the snake oil is collected by centrifugation.
Continuously decolorizing with coconut shell activated carbon for three times, and stopping adding activated carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
Embodiment two:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning the agkistrodon acutus fat wrapping, rinsing the cleaned fat with water, adding baking soda for the first time at the water temperature of preferably about 35 ℃, adjusting the pH value of the water to 8 for the first time, cleaning with clean water until no blood water exists, and centrifugally dehydrating for later use;
2) Crushing dehydrated snake fat into fat particles for later use; the Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to be less than 10 meshes;
3) Adding pulverized snake fat into an ultrasonic extractor, adding water which is 2 times of snake fat, opening vacuum, heating, opening ultrasonic wave, and extracting for 100 min; firstly, vacuum is opened, the vacuum degree is more than-0.05 Pa, and the temperature is heated to 80 ℃. The ultrasonic wave was turned on at 550W for 100 minutes. Centrifuging to obtain crude snake oil;
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil.
The oil activated carbon is powdered activated carbon and is shell activated carbon, the iodine value is more than or equal to 800mg/g, and the water content is less than 10%. The 80-400 mesh powder of activated carbon is added in an amount of 2%, the oil is heated to 80 ℃, the temperature is kept for 30 minutes, and the snake oil is collected by centrifugation.
Continuously decolorizing with shell activated carbon for three times, and stopping adding activated carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
Embodiment III:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning the agkistrodon acutus fat wrapping, rinsing the cleaned fat with water, adding baking soda for the first time at the water temperature of preferably about 35 ℃, adjusting the pH value of the water to 8 for the first time, cleaning with clean water until no blood water exists, and centrifugally dehydrating for later use;
2) Crushing dehydrated snake fat into fat particles for later use; the Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to be less than 10 meshes;
3) Adding pulverized snake fat into an ultrasonic extractor, adding water which is 2 times of snake fat, opening vacuum, heating, opening ultrasonic wave, and extracting for 100 min; firstly, vacuum is opened, the vacuum degree is more than-0.05 Pa, and the vacuum is opened, and the temperature is heated to 80 ℃;
in step 3), ultrasonic wave 550W was turned on for 100 minutes. Centrifuging to obtain crude snake oil;
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil. The oil activated carbon is powdery activated carbon and is woody activated carbon, the iodine value is more than or equal to 800mg/g, and the water content is less than 10%. The 80-400 mesh powder of activated carbon is added in an amount of 2%, the oil is heated to 80 ℃, the temperature is kept for 30 minutes, and the snake oil is collected by centrifugation.
5) Continuously decolorizing with wood active carbon for three times, and stopping adding active carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
Embodiment four:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning the agkistrodon acutus fat wrapping, rinsing the cleaned fat with water, adding baking soda for the first time at the water temperature of preferably about 35 ℃, adjusting the pH value of the water to 8, cleaning the agkistrodon acutus fat wrapping with clean water until no blood water exists, and centrifugally dehydrating for later use.
2) Crushing the dehydrated snake fat into fat particles for standby. The Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to less than 10 meshes.
3) Adding pulverized snake fat into an ultrasonic extractor, adding water to 2 times of snake fat, vacuum-heating, and ultrasonic extracting for 100 min. Firstly, vacuum is opened with the vacuum degree being more than-0.05 Pa, the temperature is heated to 80 ℃, ultrasonic wave is opened for 550W, and the extraction time is 100 minutes. And (5) centrifuging to obtain crude snake oil.
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil.
The grease activated carbon is granular activated carbon, the shell activated carbon has an iodine value of more than or equal to 800mg/g, the strength of more than or equal to 95% and the pH value of 7-9. The addition amount of 10-80 mesh particles of activated carbon is 2%, heating oil to 80 ℃, preserving heat for 30 minutes, centrifuging, and collecting snake oil.
Continuously decolorizing with shell activated carbon for three times, and stopping adding activated carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
Fifth embodiment:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning the agkistrodon acutus fat wrapping, rinsing the cleaned fat with water, adding baking soda for the first time at the water temperature of preferably about 35 ℃, adjusting the pH value of the water to 8, cleaning the agkistrodon acutus fat wrapping with clean water until no blood water exists, and centrifugally dehydrating for later use.
2) Crushing the dehydrated snake fat into fat particles for standby. The Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to less than 10 meshes.
3) Adding pulverized snake fat into an ultrasonic extractor, adding water to 2 times of snake fat, vacuum-heating, and ultrasonic extracting for 100 min. Firstly, vacuum is opened with the vacuum degree being more than-0.05 Pa, the temperature is heated to 80 ℃, ultrasonic wave is opened for 550W, and the extraction time is 100 minutes; and (5) centrifuging to obtain crude snake oil.
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil.
The grease activated carbon is granular activated carbon, the iodine value is more than or equal to 800mg/g, the strength is more than or equal to 95%, the pH value is 8, 10-80 mesh particles of activated carbon are added with 2%, the oil is heated to 60 ℃, the temperature is kept for 30 minutes, and the snake oil is collected by centrifugation.
Continuously decolorizing with shell activated carbon for three times, and stopping adding activated carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
Example six:
a process for preparing snake oil from Agkistrodon acutus snake fat by using ultrasonic extraction technology specifically comprises the following steps:
1) Cleaning Agkistrodon acutus fat coating, rinsing clean fat with water, adding baking soda for the first time at about 35deg.C, adjusting pH to 7-9, cleaning with clean water until no blood water exists, and centrifuging for dewatering.
2) Crushing the dehydrated snake fat into fat particles for standby. The Agkistrodon acutus fat comprises fat particles which are similar to the Agkistrodon acutus fat and are crushed to less than 10 meshes.
3) Adding pulverized snake fat into an ultrasonic extractor, adding water to 2 times of snake fat, vacuum-heating, and ultrasonic extracting for 100 min. Firstly, vacuum is opened with the vacuum degree being more than-0.05 Pa, the temperature is heated to 70-80 ℃, ultrasonic wave is opened for 550W, and the extraction time is 100 minutes. And (5) centrifuging to obtain crude snake oil.
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil. The grease activated carbon is granular activated carbon, the iodine value is more than or equal to 800mg/g, the strength is more than or equal to 95%, the pH value is 8, 10-80 mesh particles of activated carbon are added with 2%, the oil is heated to 50-80 ℃, the temperature is kept for 30 minutes, and the snake oil is collected by centrifugation.
Continuously decolorizing with coal activated carbon for three times, and stopping adding activated carbon when the snake oil is colorless and odorless. Filtering the snake oil again until no active carbon exists, collecting the snake oil, checking to be qualified, canning and warehousing for standby.
The following are the contents of the application test examples of the snake oil product of example 1.
Application test example 1
A snake oil ointment containing snake oil prepared from agkistrodon acutus snake fat is prepared from the following components in percentage by mass:
50% of snake oil, 10% of petrolatum, 10% of mineral oil, 6% of beeswax, 5% of macadamia nut (MACADAMIA TERNIFOLIA) seed oil, 5% of squalane, 4% of butter tree (BUTYROSPERMUM PARKII) fruit fat, 2% of safflower (CARTHAMUS TINCTORIUS) flower extract, 2% of lithospermum (LITHOSPERMUM ERYTHRORHIZON) extract, 2% of mugwort (ARTEMISIA ARGYI) leaf extract, 2% of ginger (ZINGIBER OFFICINALE) root extract and 2% of lime (CITRUSAURANTIUM DULCCIS) pericarp oil. The formula can relieve xerosis cutis in autumn and winter, promote skin moisture retention, refine skin, and prevent chapping.
The production process comprises the following steps:
1) Accurately weighing 5kg of snake oil, 10kg of petrolatum, 10kg of mineral oil, 6kg of beeswax, 5kg of macadimia nut (MACADAMIA TERNIFOLIA) seed oil, 4kg of squalane 5kg of butter tree (BUTYROSPERMUM PARKII) fruit oil, 2kg of safflower (CARTHAMUS TINCTORIUS) flower extract, 2kg of lithospermum (LITHOSPERMUM ERYTHRORHIZON) extract, 2kg of mugwort (ARTEMISIAARGYI) leaf extract and 2kg of ginger (ZINGIBER OFFICINALE) root extract for standby;
2) Sequentially adding the accurately weighed steps 1) into a homogenizing pot, stirring and heating to 70 ℃, preserving heat for 30 minutes, cooling to 50 ℃, detecting to be qualified, discharging, and filling.
3) And (5) warehousing and storing.
The product has effects of moistening skin, softening skin, and keeping skin moisture. In particular to the skin repairing of chilblain and chapping, which can close the wound in 24 hours and can recover after 3 days of continuous use.
Application test example two
A snake oil hand-care oil containing snake oil prepared from agkistrodon acutus snake fat is prepared from the following components in percentage by mass:
20% of snake oil, 20% of camellia (CAMELLIA JAPONICA), 20% of coconut (COCOS NUCIFERA) oil, 20% of grape (VITIS VINIFER) seed oil, 10% of squalane, 2% of olive (OLEA EUROPAEA) fruit oil, 2% of shea butter (BUTYROSPERMUM PARKII) fruit fat, 2% of lime (CITRUSAURANTIUM DULCCIS) fruit peel oil, 1% of safflower (CARTHAMUS TINCTORIUS) flower extract, 1% of tocopherol, 1% of mugwort (ARTEMISIAARGYI) leaf extract and 1% of bisabolol. The formula can relieve xerosis cutis in autumn and winter, promote skin moisture retention, refine skin, and prevent chapping. The formula can be used for moisturizing.
The production process comprises the following steps:
1) Accurately weighing 20kg of snake oil, 20kg of camellia (CAMELLIA JAPONICA), 20kg of coconut (coco NUCIFERA) oil, 20kg of grape (VITIS VINIFER) seed oil, 10kg of squalane, 2kg of olive (OLEA EUROPAEA) fruit oil, 2kg of shea butter (BUTYROSPERMUM PARKII) fruit oil, 2kg of lime (CITRUSAURANTIUM DULCCIS) peel oil, 1kg of safflower (CARTHAMUS TINCTORIUS) flower extract, 1kg of tocopherol, 1kg of mugwort (ARTEMISIA ARGYI) leaf extract and 1kg of bisabolol for later use;
2) Sequentially adding the accurately weighed steps 1) into a homogenizing pot, stirring and heating to 70 ℃, preserving heat for 30 minutes, cooling to 50 ℃, detecting to be qualified, discharging, and filling.
3) And (5) warehousing and storing.
The product has effects of moistening skin, softening skin, and keeping skin moisture. Preventing chapped skin, softening skin and protecting skin.
The following are the contents of efficacy test examples.
Efficacy test example 1
Specific product specifications for examples 1-6.
As shown in table 1 below:
from the experimental results of table 1 above, it can be seen that: the fifth embodiment which can reach the index is the embodiment with the least treatment times, the fastest filtration speed and the highest cost control cost performance in the process of treating the snake oil by six activated carbons.
Thus, by the above experimental procedure, experiment case five is preferably carried out as a process scheme for product production.
Efficacy test example two
Skin test was provided:
acute eye irritation/corrosiveness test of skin under the condition of no flushing, the integral value of cornea, iris and conjunctiva is 0 in 24 hours, 48 hours and 72 hours, which indicates that the test object has acute eye irritation to rabbit eyes: is non-irritating under the condition of no flushing.
Acute skin irritation experiments, at 24 hours, 48 hours, and 72 hours, the highest integral mean value of each observation time point is 0, which indicates that the test object has no irritation to the acute skin of the rabbits.
The acute eye irritation/corrosiveness experiment and the acute skin irritation experiment of the rabbit are both non-irritating, so that the skin of a human body is not irritated.
Is more stable than snake oil and can be stored for a long time.
Refined snake oil extracted by ultrasonic wave and common snake oil were subjected to the following high-low temperature and illumination experiments, as shown in the following table 2:
the following high-low temperature and illumination experiments are carried out on the refined snake oil extracted by ultrasonic waves and the common snake oil, and the stability of the snake oil after ultrasonic wave treatment is better than that of the common extracted snake oil under the conditions of 25 ℃, 45 ℃ and illumination. Ultrasonic extraction of snake oil is therefore preferred.
The snake oil extracted by ultrasonic wave has rich oil content, high content of active ingredients in the snake oil, high content of oleic acid and linoleic acid, lighter color of the snake oil, as shown in the following table 3:
| appearance of | Viscosity (Pa, s) | Oleic acid (%) | Linoleic acid (%) | |
| Ultrasonic extraction of snake oil | Clear and transparent | 890 | 42.16 | 9.46 |
| Common snake oil extraction | Semitransparent liquid | 1260 | 38.56 | 8.83 |
The ultrasonic treated snake oil has better transparency, lower viscosity and higher oleic acid and linoleic acid contents than common treated oil. Therefore, the process for extracting the snake oil by using ultrasonic waves is better than the common extraction.
The extraction and purification technology and process of the snake oil can lead the snake oil to be widely applied to foods, for example, the snake oil can be eaten, the snake oil can be fried to prepare cans, in addition, the snake oil (taken) is applicable to preventing arteriosclerosis of middle-aged and elderly people, constipation and the like, has the efficacy of relaxing bowel, and can be taken by using two to three drops of hot water.
In summary, the present invention is not limited to the preferred embodiments, but is capable of being modified, equivalent and altered in various ways without departing from the spirit and scope of the present invention.
Claims (10)
1. A preparation method for extracting refined snake oil by utilizing an ultrasonic process is characterized in that the fat of the agkistrodon acutus is cleaned, crushed, added into an ultrasonic extractor, added with water, heated and extracted to obtain crude oil of the agkistrodon acutus, and the crude oil is decolorized and deodorized to obtain the refined snake oil;
the method specifically comprises the following steps:
1) Firstly, cleaning the Agkistrodon acutus fat to remove blood, and centrifugally dehydrating for later use;
2) Crushing dehydrated snake fat into small fat particles for later use;
3) Adding pulverized snake fat into an ultrasonic extractor, adding water 1-3 times of snake fat, vacuum-heating, ultrasonic-extracting for 60-120 min to obtain crude snake oil;
4) The crude snake oil is deacidified, decolored and deodorized to obtain refined snake oil.
2. The method for preparing refined snake oil by ultrasonic process as claimed in claim 1, wherein: in the step 1), the agkistrodon acutus fat group fabric is used for removing the wrappage on the snake fat, and then the fabric is rinsed for 3 to 4 times by clean water to make the water have no color; and (5) centrifugally dewatering for standby.
3. The method for preparing refined snake oil by ultrasonic process as claimed in claim 1, wherein: in step 2), the agkistrodon acutus fat group fabric is crushed into fat particles smaller than 10 meshes.
4. The method for preparing refined snake oil by ultrasonic process as claimed in claim 1, wherein:
in the step 3), after crushing the agkistrodon acutus fat group fabric, adding the crushed agkistrodon acutus fat group fabric into an ultrasonic extractor, adding water which is more than 2 times of snake fat, and allowing water to be higher than fat;
vacuum is opened, the vacuum degree is more than-0.05 Pa, the temperature is heated to 70-80 ℃, ultrasonic wave is opened for 300-500W, and the extraction time is 60-120 minutes; and (5) centrifuging to obtain crude snake oil.
5. The method for preparing refined snake oil by ultrasonic process as claimed in claim 1, wherein: in the step 4), the crude snake oil is deacidified, decolored and deodorized by grease activated carbon to obtain refined snake oil; deacidifying with oil and active carbon, decolorizing, deodorizing, standing, filtering, and centrifuging to obtain refined Agkistrodon acutus snake oil; inspecting, canning and warehousing;
the adopted activated carbon is powdered activated carbon (wood, shell and coconut shell) with iodine value more than or equal to 800mg/g and water content less than 10%; the iodine value of the granular activated carbon (fruit shell, coconut shell and coal) is more than or equal to 800mg/g, the strength is more than or equal to 95%, and the pH value is 7-9.
6. Use of refined agkistrodon acutus snake oil prepared by the method of any of claims 1-5 in the preparation of food, pharmaceutical and cosmetic products.
7. A snake oil ointment comprising refined snake oil extracted by ultrasonic process as claimed in claim 1, wherein: the composite material is prepared from the following components in percentage by mass:
50% of snake oil, 10% of petrolatum, 10% of mineral oil, 6% of beeswax, 5% of macadamia nut seed oil, 5% of squalane, 4% of shea butter, 2% of safflower extract, 2% of lithospermum extract, 2% of mugwort leaf extract, 2% of ginger root extract and 2% of lime peel oil.
8. The snake oil ointment of claim 7, wherein: the preparation method comprises the following steps:
1) Accurately weighing 5kg of snake oil, 10kg of petrolatum, 10kg of mineral oil, 6kg of beeswax, 5kg of macadimia nut seed oil, 5kg of squalane, 4kg of butter tree fruit fat, 2kg of safflower extract, 2kg of lithospermum extract, 2kg of mugwort leaf extract and 2kg of ginger root extract for standby;
2) Sequentially adding the components accurately weighed in the step 1) into a homogenizing pot, stirring and heating to 70 ℃, preserving heat for 30 minutes, cooling to 50 ℃, detecting to be qualified, discharging, and filling;
3) And (5) warehousing and storing.
9. A snake oil hand oil comprising the refined snake oil extracted by ultrasonic process of claim 1, wherein: the composite material is prepared from the following components in percentage by mass:
20% of snake oil, 20% of camellia oil, 20% of coconut oil, 20% of grape seed oil, 10% of squalane, 2% of olive oil, 2% of shea butter, 2% of lime peel oil, 1% of safflower extract, 1% of tocopherol, 1% of mugwort leaf extract and 1% of bisabolol.
10. The snake oil hand oil of claim 9, wherein: the preparation method comprises the following steps:
1) Accurately weighing 20kg of snake oil, 20kg of camellia oil, 20kg of coconut oil, 20kg of grape seed oil, 10kg of squalane, 2kg of olive oil, 2kg of shea butter, 2kg of lime peel oil, 1kg of safflower extract, 1kg of tocopherol, 1kg of mugwort leaf extract and 1kg of bisabolol for later use;
2) Sequentially putting the accurately weighed steps 1) into a homogenizing pot, stirring and heating to 70 ℃, preserving heat for 30 minutes, cooling to 50 ℃, detecting to be qualified, discharging, and filling;
3) And (5) warehousing and storing.
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